CN104305178B - A kind of Folium Eriobotryae extracting solution high pressure vacuum dipping prepares, with microwave vacuum drying, the method that Citrus sinensis Osbeck does bubble sheet - Google Patents
A kind of Folium Eriobotryae extracting solution high pressure vacuum dipping prepares, with microwave vacuum drying, the method that Citrus sinensis Osbeck does bubble sheet Download PDFInfo
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- CN104305178B CN104305178B CN201410519957.7A CN201410519957A CN104305178B CN 104305178 B CN104305178 B CN 104305178B CN 201410519957 A CN201410519957 A CN 201410519957A CN 104305178 B CN104305178 B CN 104305178B
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- citrus sinensis
- sinensis osbeck
- folium eriobotryae
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- sheet
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- 238000007598 dipping method Methods 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims abstract description 30
- 238000001291 vacuum drying Methods 0.000 title claims abstract description 13
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 49
- 239000000834 fixative Substances 0.000 claims abstract description 17
- 238000005516 engineering process Methods 0.000 claims abstract description 16
- 239000012043 crude product Substances 0.000 claims abstract description 15
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims abstract description 11
- 239000001527 calcium lactate Substances 0.000 claims abstract description 11
- 235000011086 calcium lactate Nutrition 0.000 claims abstract description 11
- WHMDKBIGKVEYHS-IYEMJOQQSA-L Zinc gluconate Chemical compound [Zn+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O WHMDKBIGKVEYHS-IYEMJOQQSA-L 0.000 claims abstract description 10
- 239000011670 zinc gluconate Substances 0.000 claims abstract description 10
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- 229960000306 zinc gluconate Drugs 0.000 claims abstract description 10
- 235000021433 fructose syrup Nutrition 0.000 claims abstract description 9
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
- 239000007788 liquid Substances 0.000 claims description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 230000008569 process Effects 0.000 claims description 14
- 239000006228 supernatant Substances 0.000 claims description 12
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 10
- 239000011347 resin Substances 0.000 claims description 9
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- IKIIZLYTISPENI-ZFORQUDYSA-N baicalin Chemical compound O1[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IKIIZLYTISPENI-ZFORQUDYSA-N 0.000 claims description 5
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- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 5
- 235000019165 vitamin E Nutrition 0.000 claims description 5
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- 238000002360 preparation method Methods 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 238000005660 chlorination reaction Methods 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
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- 238000002372 labelling Methods 0.000 abstract description 12
- 235000016709 nutrition Nutrition 0.000 abstract description 12
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- 229940041131 calcium lactate gluconate Drugs 0.000 abstract description 5
- 235000008935 nutritious Nutrition 0.000 abstract description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 235000013312 flour Nutrition 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 5
- 244000248349 Citrus limon Species 0.000 description 4
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- 239000011780 sodium chloride Substances 0.000 description 4
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- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 3
- 241001092070 Eriobotrya Species 0.000 description 3
- 235000009008 Eriobotrya japonica Nutrition 0.000 description 3
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- 239000011575 calcium Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
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- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
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- 229930003451 Vitamin B1 Natural products 0.000 description 1
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- RSMUVYRMZCOLBH-UHFFFAOYSA-N metsulfuron methyl Chemical compound COC(=O)C1=CC=CC=C1S(=O)(=O)NC(=O)NC1=NC(C)=NC(OC)=N1 RSMUVYRMZCOLBH-UHFFFAOYSA-N 0.000 description 1
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- 235000019605 sweet taste sensations Nutrition 0.000 description 1
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- 229960003495 thiamine Drugs 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
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- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
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- 235000019154 vitamin C Nutrition 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/10—General methods of cooking foods, e.g. by roasting or frying
- A23L5/15—General methods of cooking foods, e.g. by roasting or frying using wave energy, irradiation, electrical means or magnetic fields, e.g. oven cooking or roasting using radiant dry heat
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Inorganic Chemistry (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention provides a kind of Folium Eriobotryae extracting solution high pressure vacuum dipping and prepare, with microwave vacuum drying, the method that Citrus sinensis Osbeck does bubble sheet, comprise the following steps: a) carry out Folium Eriobotryae successively squeezing the juice and desolventing technology, obtaining Folium Eriobotryae juice, then adding mass fraction in gained Folium Eriobotryae juice is 15%～the crystal sugar of 17%, 10%～14%, 5%～8%, 5%～10%, 0.02%～0.04%, Mel, high fructose syrup, calcium lactate and zinc gluconate；B) carry out Citrus sinensis Osbeck successively cutting into slices, color fixative and pre-dried, obtain Citrus sinensis Osbeck sheet crude product；C) described Citrus sinensis Osbeck sheet crude product is carried out in described Folium Eriobotryae juice normal temperature high voltage vacuum moment dipping, after having impregnated, is dried to obtain Citrus sinensis Osbeck dry bubble sheet；Between described step a) and step b), order does not limits.The Citrus sinensis Osbeck that the present invention provides is done bubble sheet and is had the nutritional labeling of Citrus sinensis Osbeck and Folium Eriobotryae simultaneously, the most nutritious, and has good health-care effect.
Description
Technical field
The invention belongs to field of food, particularly relate to a kind of Folium Eriobotryae extracting solution high pressure vacuum dipping true with microwave
Empty being dried prepares the method that Citrus sinensis Osbeck does bubble sheet.
Background technology
Folium Eriobotryae is the leaf of rosaceous plant Folium Eriobotryae, and property is put down, and bitter in the mouth enters lung, stomach warp, the most just
It is taken as medical material to use, is traditional relieving cough and asthma Chinese medicine, have preventing phlegm from forming and stopping coughing, regulating the stomach and sending down the abnormal ascending QI, dysentery relieving diuresis
Effect, neuralgia, arthritis, pain in the lumbar region and cancer etc. are also had certain curative effect.Containing tens in Folium Eriobotryae
Plant triterpenoids, be the principle active component of Folium Eriobotryae；Additionally, Folium Eriobotryae also containing saponins material,
Organic acid substance, tannin, vitamin B, vitamin C etc..
Citrus sinensis Osbeck contains abundant vitamin, sugar, acid, cellulose, carotene, vitamin B1, vitamin
The multiple nutrients compositions such as B2, protein, fat, calcium, phosphorus, ferrum, have blood circulation promoting and new old generation
Thank, regain one's strength, health invigorating, the effect kept fit, often eat Citrus sinensis Osbeck, contribute to prevention of arterial blood vessel
Hardening, reduce cholesterol, reduce fat, drain non-ferrous metal, radioelement and internal surplus thing,
Desirably prevent the diseases such as cancer.
Summary of the invention
It is an object of the invention to provide a kind of Folium Eriobotryae extracting solution high pressure vacuum dipping and microwave vacuum drying system
The method that standby Citrus sinensis Osbeck does bubble sheet, the Citrus sinensis Osbeck that the present invention provides is done bubble sheet and is impregnated with the effective ingredient of Folium Eriobotryae, no
The most nutritious, and there is good health-care effect.
The invention provides a kind of Folium Eriobotryae extracting solution high pressure vacuum dipping and microwave vacuum drying is prepared Citrus sinensis Osbeck and done
The method of bubble sheet, comprises the following steps:
A) carry out Folium Eriobotryae successively squeezing the juice and desolventing technology, obtain Folium Eriobotryae juice, then to gained Folium Eriobotryae
Adding mass fraction in juice is 15%～17%, 10%～14%, 5%～8%, 5%～10%, 0.02%～0.04%
Crystal sugar, Mel, high fructose syrup, calcium lactate and zinc gluconate；
B) carry out Citrus sinensis Osbeck successively cutting into slices, color fixative and pre-dried, obtain Citrus sinensis Osbeck sheet crude product；
C) described Citrus sinensis Osbeck sheet crude product is carried out in described Folium Eriobotryae juice normal temperature high voltage vacuum moment dipping, first
Carrying out high pressure dipping, pressure is 0.85MPa～0.95MPa, and the time is 5min～8min, then carries out true
Empty moment dipping, vacuum is 75mbar～85mbar, time 5min～15min, then carry out high pressure long time
Between impregnate, pressure is 0.80MPa～0.85MPa, and the time is 50min～65min, finally carry out vacuum long time
Between impregnate, vacuum is 72mbar～83mbar, and time 60min～70min is dried to obtain after having impregnated
Citrus sinensis Osbeck dry bubble sheet；
Between described step a) and step b), order does not limits.
Preferably, described step a) specifically includes:
A1) mix with water after Folium Eriobotryae being pulverized, after microwave treatment, carry out centrifugal treating, obtain supernatant
Liquid；
A2) described supernatant is carried out desolventing technology by decolorizing resin, obtain Folium Eriobotryae juice.
Preferably, described step a1) in, described Folium Eriobotryae is 1:1～3 with the mass ratio of water.
Preferably, described step a1) in, the power of described microwave is 480W～560W, at described microwave
The time of reason is 5min～7min.
Preferably, described step a1) in, the mode of described microwave treatment is that batch (-type) processes, microwave treatment
1min suspends 30s.
Preferably, described step b) particularly as follows:
B1) in colour-keeping liquid, color fixative is carried out after being cut into slices by Citrus sinensis Osbeck；
B2) the Citrus sinensis Osbeck sheet after color fixative is carried out microwave vacuum predrying.
Preferably, described step b1) in, described colour-keeping liquid includes: mass ratio is
The water of 100:1～2:0.2～0.4:0.4～1:0.3, sodium chloride, citric acid, vitamin E and baicalin.
Preferably, described step b2) in, described predrying temperature is 50 DEG C～60 DEG C, and microwave power is
20kW～40kW, vacuum is 2.4Pa～2.6Pa.
Preferably, in described step c), described being dried as microwave vacuum drying, the power of described microwave is
20kW～40kW, vacuum is 2.4Pa～2.6Pa, dry temperature 70-80 DEG C.
The Citrus sinensis Osbeck that a kind of method described in technique scheme that present invention also offers prepares dry bubble sheet.
Compared with prior art, Folium Eriobotryae is carried out squeezing the juice and desolventing technology by the present invention successively, obtains Folium Eriobotryae
Juice, then in gained Folium Eriobotryae juice add mass fraction be 15%～17%, 10%～14%, 5%～8%,
5%～the crystal sugar of 10%, 0.02%～0.04%, Mel, high fructose syrup, calcium lactate and zinc gluconate；By umbilicus
Orange carries out cutting into slices successively, color fixative and pre-dried, obtains Citrus sinensis Osbeck sheet crude product；Described Citrus sinensis Osbeck sheet crude product is existed
Carrying out normal temperature high voltage vacuum moment dipping in described Folium Eriobotryae juice, first carry out high pressure dipping, pressure is
0.85MPa～0.95MPa, the time is 5min～8min, then carries out vacuum moment dipping, and vacuum is
75mbar～85mbar, time 5min～15min, then carry out high pressure and impregnate for a long time, and pressure is
0.80MPa～0.85MPa, the time is 50min～65min, finally carries out vacuum and impregnates for a long time, vacuum
For 72mbar～83mbar, time 60min～70min, after having impregnated, it is dried to obtain Citrus sinensis Osbeck dry bubble sheet.This
The antioxidant inventing the interpolation of the color retention to lemon tablet is natural extract polyphenoils, can not only be good
Preventing the oxidation of lemon tablet, this colour fixative is to human body without fanout free region simultaneously, can relieved eat.Loquat juice adds
Add calcium lactate and two kinds of materials of zinc gluconate, can effectively make up the ZD problem of calcium in Citrus sinensis Osbeck so that
The nutritional labeling that the Citrus sinensis Osbeck prepared with this invention does bubble sheet is more perfect, all-ages.Dipping uses
Vacuum impregnation technology can more effectively make nutritional labeling in Folium Eriobotryae juice penetrate in Citrus sinensis Osbeck sheet, dry run is adopted
With low-temperature vacuum drying, low temperature can make the nutritional labeling in Citrus sinensis Osbeck sheet retain to greatest extent.The dry bubble of this Citrus sinensis Osbeck
Sheet has the nutritional labeling of Citrus sinensis Osbeck and Folium Eriobotryae simultaneously, the most nutritious, and has good health care merit
Effect.Further, the present invention takes the mode of microwave to be squeezed the juice by Folium Eriobotryae, and complete saves Folium Eriobotryae
Effective ingredient in leaf so as to get Citrus sinensis Osbeck dry bubble sheet health-care effect more preferable.The dry bubble of Citrus sinensis Osbeck prepared by the present invention
Sheet can directly eat, and has advantage easy to carry.It addition, the present invention can using Folium Eriobotryae as raw material,
Decrease the generation of Folium Eriobotryae fallen leaves, thus decrease the waste of resource and the pollution of environment.
Detailed description of the invention
The invention provides a kind of Folium Eriobotryae extracting solution high pressure vacuum dipping and microwave vacuum drying is prepared Citrus sinensis Osbeck and done
The method of bubble sheet, comprises the following steps:
A) carry out Folium Eriobotryae successively squeezing the juice and desolventing technology, obtain Folium Eriobotryae juice, then to gained Folium Eriobotryae
Adding mass fraction in juice is 15%～17%, 10%～14%, 5%～8%, 5%～10%, 0.02%～0.04%
Crystal sugar, Mel, high fructose syrup, calcium lactate and zinc gluconate；
B) carry out Citrus sinensis Osbeck successively cutting into slices, color fixative and pre-dried, obtain Citrus sinensis Osbeck sheet crude product；
C) described Citrus sinensis Osbeck sheet crude product is carried out in described Folium Eriobotryae juice normal temperature high voltage vacuum moment dipping, first
Carrying out high pressure dipping, pressure is 0.85MPa～0.95MPa, and the time is 5min～8min, then carries out true
Empty moment dipping, vacuum is 75mbar～85mbar, time 5min～15min, then carry out high pressure long time
Between impregnate, pressure is 0.80MPa～0.85MPa, and the time is 50min～65min, finally carry out vacuum long time
Between impregnate, vacuum is 72mbar～83mbar, and time 60min～70min is dried to obtain after having impregnated
Citrus sinensis Osbeck dry bubble sheet；
Between described step a) and step b), order does not limits.
Citrus sinensis Osbeck sheet is carried out vacuum impregnation in Folium Eriobotryae juice by the present invention, makes the nutritional labeling in Folium Eriobotryae juice ooze
Enter in Citrus sinensis Osbeck sheet, through i.e. can get after drying Citrus sinensis Osbeck dry bubble sheet, this Citrus sinensis Osbeck dry bubble sheet have simultaneously Citrus sinensis Osbeck and
The nutritional labeling of Folium Eriobotryae, the most nutritious, and there is good health-care effect.
It, using Folium Eriobotryae as raw material, is carried out squeezing the juice and after desolventing technology, obtains Folium Eriobotryae by the present invention successively
Juice.Specifically, Folium Eriobotryae juice is prepared in accordance with the following methods:
A1) mix with water after Folium Eriobotryae being pulverized, after microwave treatment, carry out centrifugal treating, obtain supernatant
Liquid；
A2) described supernatant is carried out desolventing technology by decolorizing resin, obtain Folium Eriobotryae juice.
First Folium Eriobotryae is pulverized by the present invention, and preferred powder is broken to the flour of 40 mesh, then that Folium Eriobotryae is broken
Powder mixes with water and carries out microwave treatment and squeeze the juice.The mass ratio of Folium Eriobotryae flour and water is preferably 1:1～3, more preferably
For 1:2.During described microwave treatment, the power of microwave is preferably 480W～560W, more preferably
500W～550W；The time of microwave is preferably 5min～7min, more preferably 6min.Present invention preferably employs
Intermittent type microwave processes, and preferably microwave treatment 1min suspends 30s, and recurrence interval processes to total microwave treatment time
Reach the predetermined time.
Before being pulverized by Folium Eriobotryae, the present invention preferably carries out pretreatment to described Folium Eriobotryae, specifically wraps
Include:
Being soaked in clear water by Folium Eriobotryae, brush off the fine hair on its surface, clear water is cleaned.
Folium Eriobotryae is soaked in clear water, by Impurity removals such as the dusts on its surface；Then Pi is brushed off with hairbrush
Fine hair on rake leaf, rinses well with clear water.
In microwave processing process, the effective ingredient in Folium Eriobotryae is dissolved in the water, and obtains Folium Eriobotryae juice.Microwave
After being disposed, it is centrifuged the mixture obtained processing, collects supernatant.
After obtaining supernatant, it is carried out desolventing technology.The present invention preferably by described supernatant by decolouring tree
Fat carries out desolventing technology, and described decolorizing resin is preferably equal hole decolorizing resin, such as XDA-7 equal hole decolouring tree
Fat, during desolventing technology, the flow velocity of described supernatant is 1.5 times of amount of resin/h.Described desolventing technology repeatable enter
OK, the present invention there is no particular restriction to this.
After decolouring, add in the Folium Eriobotryae juice obtained mass fraction be 15%～17%, 10%～14%,
5%～the crystal sugar of 8%, 5%～10%, 0.02%～0.04%, Mel, high fructose syrup, calcium lactate and glucose
Acid zinc.The mass fraction of described crystal sugar, Mel, high fructose syrup, calcium lactate and zinc gluconate is more preferably
15%, 10%, 5%, 5% and 0.02%.Loquat juice with the addition of calcium lactate and two kinds of materials of zinc gluconate,
Can effectively make up the ZD problem of calcium in Citrus sinensis Osbeck so that the Citrus sinensis Osbeck prepared with this invention does the battalion of bubble sheet
Form point more perfect, all-ages.
It, with Citrus sinensis Osbeck as raw material, is carried out cutting into slices, color fixative and pre-dried by the present invention successively, obtains Citrus sinensis Osbeck
Sheet crude product.Specifically, described Citrus sinensis Osbeck sheet crude product is prepared in accordance with the following methods:
B1) in colour-keeping liquid, color fixative is carried out after being cut into slices by Citrus sinensis Osbeck；
B2) the Citrus sinensis Osbeck sheet after color fixative is carried out microwave vacuum predrying.
First Citrus sinensis Osbeck is cut into slices by the present invention, uses microtome.The thickness of described Citrus sinensis Osbeck sheet is preferably
2mm～4mm, more preferably 3mm.Before being cut into slices by Citrus sinensis Osbeck, the present invention is preferably by clear for Citrus sinensis Osbeck clear water
Wash clean.
After Citrus sinensis Osbeck is cut into slices, it is placed in colour-keeping liquid and carries out color retention.Described colour-keeping liquid is preferably quality
Than water, sodium chloride, citric acid, vitamin E and baicalin for 100:1:0.2:0.4:0.3, Citrus sinensis Osbeck sheet is soaked
In colour-keeping liquid, the color retention to Citrus sinensis Osbeck sheet can be completed.The time of described color fixative is preferably
40min～60min, more preferably 45min～55min.After immersion, Citrus sinensis Osbeck sheet is pulled out and drains.This
The antioxidant that the bright color retention to lemon tablet adds is natural extract polyphenoils, can not only well prevent
The only oxidation of lemon tablet, this colour fixative is to human body without fanout free region simultaneously, can relieved eat.
Carrying out predrying by the Citrus sinensis Osbeck sheet after color fixative, it is predrying that the present invention preferably carries out microwave vacuum to it, can
To carry out in microwave vacuum dryer.In the present invention, described pre-dried temperature is preferably 50 DEG C～60
DEG C, the power of microwave is preferably 20kW～40kW, and vacuum is preferably 2.4Pa～2.6Pa, predrying to Citrus sinensis Osbeck
The moisture content of sheet is 10%～20%.Carry out predrying under these conditions so that the nutritional labeling of Citrus sinensis Osbeck sheet obtains
To farthest retaining.
After predrying, obtain Citrus sinensis Osbeck sheet crude product, described Citrus sinensis Osbeck sheet crude product is carried out very in Folium Eriobotryae juice
Empty dipping, makes the nutritional labeling in Folium Eriobotryae juice and beneficiating ingredient penetrate in Citrus sinensis Osbeck sheet, the most available
Citrus sinensis Osbeck dry bubble sheet.First the present invention carries out high pressure dipping to it, and pressure is 0.85MPa～0.95MPa,
Time is 5min～8min, then carries out vacuum moment dipping, and vacuum is 75mbar～85mbar, the time
5min～15min, then carries out high pressure and impregnates for a long time, and pressure is 0.80MPa～0.85MPa, and the time is
50min～65min, finally carries out vacuum and impregnates for a long time, and vacuum is 72mbar～83mbar, the time
60min～70min, is dried to obtain Citrus sinensis Osbeck dry bubble sheet after having impregnated.The present invention to described Citrus sinensis Osbeck sheet crude product with
The ratio of described Folium Eriobotryae juice is not particularly limited, it is possible to by Citrus sinensis Osbeck sheet submergence.
After immersion, Citrus sinensis Osbeck sheet is dried, i.e. can get Citrus sinensis Osbeck dry bubble sheet.In the present invention, institute
Stating to be dried and be preferably microwave vacuum drying, the power of described microwave is preferably 20kW～40kW, and vacuum is excellent
Elect 2.4Pa～2.6Pa, preferred 70-80 DEG C of dry temperature as.The present invention is preferably dried to Citrus sinensis Osbeck sheet moisture content
It is less than 8%.
The Citrus sinensis Osbeck that a kind of method described in technique scheme that present invention also offers prepares dry bubble sheet, its
There is the nutritional labeling of Citrus sinensis Osbeck and Folium Eriobotryae.
The Citrus sinensis Osbeck that the present invention provides dry bubble sheet can use as leisure food, not only has a sweet taste good to eat, and
And it is easy to carry.The present invention provide Citrus sinensis Osbeck sheet can also as health food eat, have preventing phlegm from forming and stopping coughing,
Diuresis, effect of raising immunity.The Citrus sinensis Osbeck that the present invention provides dry bubble sheet can be drunk after soaked.
Citrus sinensis Osbeck sheet is carried out vacuum impregnation in Folium Eriobotryae juice by the present invention, makes the nutritional labeling in Folium Eriobotryae juice ooze
Enter in Citrus sinensis Osbeck sheet, through i.e. can get after drying Citrus sinensis Osbeck dry bubble sheet, this Citrus sinensis Osbeck dry bubble sheet have simultaneously Citrus sinensis Osbeck and
The nutritional labeling of Folium Eriobotryae, the most nutritious, and there is good health-care effect.Further, originally
Invention takes the mode of microwave to be squeezed the juice by Folium Eriobotryae, the complete effective ingredient saved in Folium Eriobotryae,
Make the Citrus sinensis Osbeck dry bubble sheet health-care effect obtained more preferable.Citrus sinensis Osbeck prepared by the present invention dry bubble sheet can directly eat,
There is advantage easy to carry.It addition, the present invention can decrease Folium Eriobotryae fallen leaves using Folium Eriobotryae as raw material
Produce, thus decrease the waste of resource and the pollution of environment.
For further illustrating the present invention, the Folium Eriobotryae extracting solution high pressure present invention provided below in conjunction with embodiment
Vacuum impregnation and microwave vacuum drying prepare Citrus sinensis Osbeck do bubble sheet method be described in detail.
Embodiment 1
(1) pretreatment of Folium Eriobotryae: select fresh Folium Eriobotryae and first soak several minutes with clear water, then use hairbrush brush
Fall the fine hair of residual on Folium Eriobotryae, rinse well with clear water, standby.
(2) microwave of Folium Eriobotryae is squeezed the juice: first pulverized with pulverizer by the Folium Eriobotryae cleaned in (1), flour
Cross 40 mesh sieves, the flour obtained is put in glass container, be that 1:1 adds pure water by solid-liquid ratio, use microwave
Process time 7min, power is 500W, within the time set, often processes 1min and suspends 30s, with this type of
Pushing away, recurrence interval processes and reaches to test stipulated time, after having processed, high speed centrifugation to the time always processed,
Collect supernatant, seal and preserve, standby.
The decolouring of Folium Eriobotryae juice: be 1.5 times amount (resins) by flow velocity by the Folium Eriobotryae juice obtained in (2)
/ enter XDA-7 equal hole decolorizing resin per hour and carry out desolventing technology, it is repeated 3 times, obtains Folium Eriobotryae juice, so
Being separately added into mass fraction in backward gained Folium Eriobotryae juice is: 15%, the ice of 10%, 5%, 5%, 0.02%
Sugar, Mel, high fructose syrup, calcium lactate, zinc gluconate.
The pretreatment of Citrus sinensis Osbeck: select intact Citrus sinensis Osbeck, cleans with clear water, standby.
Citrus sinensis Osbeck is cut into slices: Citrus sinensis Osbeck microtome orientation cleaned in (4) is cut into the thin slice of 3mm, standby.
The color fixative of Citrus sinensis Osbeck sheet: the Citrus sinensis Osbeck sheet cut is put into and soaks 60min, the composition of colour-keeping liquid in colour-keeping liquid
It is the water of 100:1:0.2:0.4:0.3, sodium chloride, citric acid, vitamin E and baicalin preparation for mass ratio
Aqueous solution, floods Citrus sinensis Osbeck sheet with colour-keeping liquid and is advisable, and is pulled out by Citrus sinensis Osbeck sheet and drain after having soaked.
The low-temperature microwave vacuum of Citrus sinensis Osbeck sheet is predrying: be dried by the Citrus sinensis Osbeck sheet microwave vacuum dryer in (6)
Carrying out predrying, baking temperature is 50 DEG C, and microwave power is 30KW, and vacuum is 2.4Pa, be dried to
The moisture content of Citrus sinensis Osbeck sheet is 15%.
Citrus sinensis Osbeck sheet after (6) process is put into normal temperature high voltage vacuum moment dipping in the solution in (3),
First carrying out high pressure dipping, pressure is 0.88MPa, and the time is 6min, then carries out vacuum moment dipping,
Vacuum is 80mbar, time 7min, then carries out high pressure and impregnates for a long time, and pressure is 0.84MPa, time
Between be 62min, finally impregnate for a long time by vacuum, vacuum is 75mbar, and time 63min has impregnated
Redrying process is carried out after one-tenth.
The redrying of Citrus sinensis Osbeck sheet: the Citrus sinensis Osbeck sheet in (7) carries out second time microwave drying, and microwave power is
30KW, vacuum is 2.5Pa, and baking temperature is 70 DEG C, is dried to Citrus sinensis Osbeck sheet moisture and is down to 8% discharging.
Detecting the Citrus sinensis Osbeck obtained dry bubble sheet, result is as shown in table 1:
Table 1 Citrus sinensis Osbeck does the indices of bubble sheet
Embodiment 2
(1) pretreatment of Folium Eriobotryae: select fresh Folium Eriobotryae and first soak several minutes with clear water, then use hairbrush brush
Fall the fine hair of residual on Folium Eriobotryae, rinse well with clear water, standby.
(2) microwave of Folium Eriobotryae is squeezed the juice: first pulverized with pulverizer by the Folium Eriobotryae cleaned in (1), flour
Cross 40 mesh sieves, the flour obtained is put in glass container, be that 1:2 adds pure water by solid-liquid ratio, use microwave
Processing 6min, power is 560W, within the time set, and often process 1min time-out 30s, by that analogy,
Recurrence interval processes to reaching experiment stipulated time, after having processed, high speed centrifugation total processing time, collects
Supernatant, seals and preserves, standby.
(3) decolouring of Folium Eriobotryae juice: by the Folium Eriobotryae juice obtained in (2) by flow velocity be 1.5 times amount (tree
Fat)/enter XDA-7 equal hole decolorizing resin per hour and carry out desolventing technology, it is repeated 3 times, obtains Folium Eriobotryae juice,
Then being separately added into mass fraction in gained loquat juice is: 17%, the ice of 14%, 8%, 10%, 0.04%
Sugar, Mel, high fructose syrup, calcium lactate, zinc gluconate.
(4) pretreatment of Citrus sinensis Osbeck: select intact Citrus sinensis Osbeck, cleans with clear water, standby.
(5) Citrus sinensis Osbeck section: Citrus sinensis Osbeck microtome orientation cleaned in (4) is cut into the thin slice of 3mm,
Standby.
The color fixative of Citrus sinensis Osbeck sheet: the Citrus sinensis Osbeck sheet cut is put into and soaks 60min, the composition of colour-keeping liquid in colour-keeping liquid
It is the water of 100:1:0.4:1:0.3, sodium chloride, citric acid, vitamin E and baicalin preparation for mass ratio
Aqueous solution, floods Citrus sinensis Osbeck sheet with colour-keeping liquid and is advisable, and is pulled out by Citrus sinensis Osbeck sheet and drain after having soaked.
(6) the low-temperature microwave vacuum of Citrus sinensis Osbeck sheet is predrying: by the Citrus sinensis Osbeck sheet microwave vacuum drying in (6)
Machine is dried and carries out predrying, and baking temperature is 60 DEG C, and microwave power is 30KW, and vacuum is 2.4Pa, dry
The dry moisture content to Citrus sinensis Osbeck sheet is 15%.
(7) the high pressure vacuum dipping of Citrus sinensis Osbeck sheet: the Citrus sinensis Osbeck sheet after (6) process is put in (3)
Carrying out normal temperature high voltage vacuum moment dipping in solution, first carry out high pressure dipping, pressure is 0.85MPa,
Time is 8min, then carries out vacuum moment dipping, and vacuum is 85mbar, time 5min, then carries out height
The long-time dipping of pressure, pressure is 0.84MPa, and the time is 52min, finally carries out vacuum and impregnates for a long time, very
Reciprocal of duty cycle is 80mbar, and time 63min carries out redrying process after having impregnated.
(8) redrying of Citrus sinensis Osbeck sheet: the Citrus sinensis Osbeck sheet in (7) is carried out second time microwave drying, microwave
Power is 30KW, and vacuum is 2.5Pa, and baking temperature is 80 DEG C and is dried to Citrus sinensis Osbeck sheet moisture and is down to 8% discharging.
Detecting the Citrus sinensis Osbeck obtained dry bubble sheet, result is as shown in table 1:
Table 2 Citrus sinensis Osbeck does the indices of bubble sheet
The above is only the preferred embodiment of the present invention, it is noted that common for the art
For technical staff, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications,
These improvements and modifications also should be regarded as protection scope of the present invention.
Claims (4)
1. Folium Eriobotryae extracting solution high pressure vacuum dipping and microwave vacuum drying are prepared Citrus sinensis Osbeck and are done the side of bubble sheet
Method, comprises the following steps:
A) mix with water after Folium Eriobotryae being pulverized, after microwave treatment, carry out centrifugal treating, obtain supernatant
Liquid；Described supernatant is carried out desolventing technology by decolorizing resin, obtains Folium Eriobotryae juice；Then to gained
In Folium Eriobotryae juice add mass fraction be 15%～17%, 10%～14%, 5%～8%, 5%～10%,
Crystal sugar, Mel, high fructose syrup, calcium lactate and the zinc gluconate of 0.02%～0.04%；The merit of described microwave
Rate is 480W～560W, and the time of described microwave treatment is 5min～7min；
B) it is the water of 100:1～2:0.2～0.4:0.4～1:0.3, chlorination at mass ratio after Citrus sinensis Osbeck being cut into slices
The colour-keeping liquid of sodium, citric acid, vitamin E and baicalin carries out color fixative, the Citrus sinensis Osbeck sheet after color fixative is entered
Row microwave vacuum is predrying, obtains Citrus sinensis Osbeck sheet crude product；Described predrying temperature is 50 DEG C～60 DEG C, microwave merit
Rate is 20kW～40kW, and vacuum is 2.4Pa～2.6Pa；
C) described Citrus sinensis Osbeck sheet crude product is carried out in described Folium Eriobotryae juice normal temperature high voltage vacuum moment dipping, first
Advanced horizontal high voltage dipping, pressure is 0.85MPa～0.95MPa, and the time is 5min～8min, then enters
Row vacuum moment impregnates, and vacuum is 75mbar～85mbar, and time 5min～15min then carries out height
The long-time dipping of pressure, pressure is 0.80MPa～0.85MPa, and the time is 50min～65min, finally carries out
Vacuum impregnates for a long time, and vacuum is 72mbar～83mbar, and time 60min～70min, after having impregnated
It is dried to obtain Citrus sinensis Osbeck dry bubble sheet；Described being dried as microwave vacuum drying, the power of described microwave is
20kW～40kW, vacuum is 2.4Pa～2.6Pa, and dry temperature is 70-80 DEG C；
Between described step a) and step b), order does not limits.
Preparation method the most according to claim 1, it is characterised in that in described step a), institute
The mass ratio stating Folium Eriobotryae and water is 1:1～3.
Preparation method the most according to claim 1, it is characterised in that in described step a), institute
The mode stating microwave treatment is that batch (-type) processes, and microwave treatment 1min suspends 30s.
4. the Citrus sinensis Osbeck that the method described in a claims 1 to 3 any one prepares dry bubble sheet.
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| WO2012078798A1 (en) * | 2010-12-07 | 2012-06-14 | Bananalogix, Inc. | Methods of processing organic matter and compositions thereof |
| CN102919743A (en) * | 2012-10-10 | 2013-02-13 | 广东省农业科学院蚕业与农产品加工研究所 | Preparation method of natural lemon slice and fruit powder |
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| CN102919743A (en) * | 2012-10-10 | 2013-02-13 | 广东省农业科学院蚕业与农产品加工研究所 | Preparation method of natural lemon slice and fruit powder |
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