CN104292931B - A kind of vanilla broad-spectrum antiseptic type multi-effect putty and preparation method - Google Patents

A kind of vanilla broad-spectrum antiseptic type multi-effect putty and preparation method Download PDF

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Publication number
CN104292931B
CN104292931B CN201410411475.XA CN201410411475A CN104292931B CN 104292931 B CN104292931 B CN 104292931B CN 201410411475 A CN201410411475 A CN 201410411475A CN 104292931 B CN104292931 B CN 104292931B
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parts
vanilla
putty
mesh
weight
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CN104292931A (en
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庄可军
庄可香
魏国营
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Hebei Chenyang water paint Co. Ltd.
Hebei Chenyang Industry and Trade Group Co Ltd
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ZHONGSHAN YIZHAN DECORATION ENGINEERING Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/34Filling pastes

Abstract

nullA kind of vanilla broad-spectrum antiseptic type multi-effect putty,Its raw material is made up of the material of following parts by weight: 200 280 parts of water,Heavy calcium carbonate 55 70 parts,Sierozem power 16 25 parts,White cement 10 15 parts,Hydroxypropyl methyl cellulose 2.5 4 parts,36 parts of anion natural mineral matter powder,2 2.5 parts of brightening agent,Fructus Forsythiae 23 parts,Cortex Phellodendri 23 parts,Rhamnus crenata sieb.et zucc. 12 parts,Lavandula angustifolia 1 1.5 parts,Herba Anemones Hupehensis 23 parts,Herba Duchesneae Indicae 0.5 1 parts,Vanilla 0.5 1 parts,Described anion natural mineral matter powder is tourmaline、The mixture of lanthanide rare composite salt and titanium oxide 5:2:3 by weight,Wherein tourmaline is dravite and the mixture of elbaite 3:7 by weight,It is possible not only to discharge for a long time negative aeroion,Also to staphylococcus、Escherichia coli、The multiple pathogenic bacteria such as gram-positive bacteria and fungus have certain suppression、Killing action.

Description

A kind of vanilla broad-spectrum antiseptic type multi-effect putty and preparation method
Technical field
The present invention relates to a kind of building and ornament materials, particularly to a kind of vanilla broad-spectrum antiseptic type multi-effect putty and preparation method.
Background technology
Powder of lacquer putty for use on, it is widely used in construction and decoration as metope packing material, the anti-corrosion material used in traditional putty, also the multiple volatile harmful materials such as formaldehyde, benzene, radon, ammonia are contained in it, pollute room air, and present building generally ventilates the best, for a long time in such room, health for people brings serious threat, destroys the living environment of people;On the other hand, traditional putty paste only serves filling effect, does not possess other function, can not meet the daily demand of people.
Summary of the invention
The deficiency existed for prior art, one of the technical problem to be solved is to provide a kind of Environmental Safety, nontoxic, abnormal smells from the patient is pure and fresh, there is a kind of vanilla broad-spectrum antiseptic type multi-effect putty of health-care effect, it is possible not only to discharge for a long time negative aeroion, purify air, beneficially health;Also the multiple pathogenic bacterias such as staphylococcus, escherichia coli, gram-positive bacteria and fungus are had certain suppression, killing action;Fragrant odour simultaneously, pure and fresh soothes the spirit, pressure of releiving, also can expelling mosquito, human body will not be produced harmful effect, it is adaptable to each age groups.
The two of the technical problem to be solved are to provide the preparation method of a kind of vanilla broad-spectrum antiseptic type multi-effect putty.
It is an object of the invention to be achieved through the following technical solutions:
A kind of vanilla broad-spectrum antiseptic type multi-effect putty, its raw material is made up of the material of following parts by weight: water 200-280 part, heavy calcium carbonate 55-70 part, sierozem power 16-25 part, white cement 10-15 part, hydroxypropyl methyl cellulose 2.5-4 part, anion natural mineral matter powder 3-6 part, brightening agent 2-2.5 part, Fructus Forsythiae 2-3 part, Cortex Phellodendri 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part, lavandula angustifolia 1-1.5 part, Herba Anemones Hupehensis 2-3 part, Herba Duchesneae Indicae 0.5-1 part, vanilla 0.5-1 part, described anion natural mineral matter powder is tourmaline, the mixture of lanthanide rare composite salt and titanium oxide 5:2:3 by weight, wherein tourmaline is dravite and the mixture of elbaite 3:7 by weight.
Specifically, the fineness of described anion natural mineral matter powder is 1000-8000 mesh;The viscosity of described hydroxypropyl methyl cellulose is 80000-100000 mPa•s;The fineness particle diameter of described heavy calcium carbonate is 600-1200 mesh;The fineness particle diameter of described sierozem power is 600-1200 mesh;The fineness particle diameter of described white cement is 500-800 mesh;Described brightening agent uses environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this brightening agent is mainly used in brightening of papermaking, coating, ink and yarn fabric, it utilizes ANSD acid to be initial reactant, synthesize compounding mixed type fluorescent whitening agent, substantially solve pollution problem, expand the range of application of fluorescent whitening agent simultaneously.
The preparation method of a kind of vanilla broad-spectrum antiseptic type multi-effect putty, is made up of following step:
S1, take Fructus Forsythiae 2-3 part, Cortex Phellodendri 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part respectively by above-mentioned each component, lavandula angustifolia 1-1.5 part, Herba Anemones Hupehensis 2-3 part, Herba Duchesneae Indicae 0.5-1 part, vanilla 0.5-1 part, and put into the Chinese medicinal powder being crushed to 800-1200 mesh in super micron mill respectively, standby;
S2, the Chinese medicinal powder in S1 and other raw material are put in large-scale mixing and blending machine, add appropriate water, be sufficiently stirred for mixing well 15-20 minute, get product.
The present invention with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine and verifies repeatedly, and giving full play to each component synergism, the effect brief introduction of the raw material of Chinese medicine employed in it is as follows.
Fructus Forsythiae: heat-clearing and toxic substances removing, dispersing swelling and dissipating binds, dispelling wind and heat pathogens, there is the title of " persons particularly liable to develop skin infection's panacea ", Bacillus typhi, Salmonella paratyphi, escherichia coli, dysentery bacterium, diphtheria corynebacterium and vibrio cholera, staphylococcus, streptococcus etc. can be suppressed.
Cortex Phellodendri: staphylococcus aureus, streptococcus pneumoniae, diphtheria corynebacterium, Streptococcus viridans, dysentery bacterium (except Song Nei Shi), Hemolytic streptococcus, meningococcus, vibrio cholera, anthrax bacillus all effectively or are had stronger inhibitory action;Bacillus subtilis, bordetella pertussis, clostridium tetani also there is inhibitory action.
Rhamnus crenata sieb.et zucc.:: machaka or dungarunga, root bark or Herb are used as medicine, and property is flat, bitter in the mouth, dries, sterilizes, parasite killing.
Lavandula angustifolia: ant can be removed, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, the fragrance of one people that oozes can also be left, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is the main component that lavandula angustifolia is antibacterial, and it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the growth of 10 kinds of funguses.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature, slightly poisonous." [chemical composition] root and herb be containing Anemonin (anemonin) and triterpene soap oleanolic acid-3-O-β-D-ribopyranoside base-(1 → 3)-α-L-rhamnopyranosyl-(1 → 3)-α-L-arabopyranose glycoside, oleanolic acid 3-O-β-D-ribopyranoside base-(1 → 3)-α-L-rhamnopyranosyl-(1 → 2)-β-D-xylopyranose glucoside, and oleanolic acid.[function cures mainly] kills maggot, wriggler, changes long-pending, detumescence, dissipating blood stasis, controls stubborn dermatitis, tinea alba, malaria, infantile malnutrition, dysentery, and carbuncle furuncle swells, scrofula, traumatic injury.
Herba Duchesneae Indicae: " whole nation Chinese herbal medicine compilation " is recorded: perennial herb, Herb has pubescence;Stolon is long, herb hyoscine, has that heat-clearing and toxic substances removing, Huoxue San " be remorse, astringing to arrest bleeding effect, can control again venom, apply and control furuncle etc.;And be used for killing fly larvae, there is the F-I that separates in antibacterial action Herba Duchesneae Indicae, F-II, F-III part in the suppression positive to the growth of staphylococcus aureus and shigella, are the weak positive to bacillus pyocyaneus, are negative sramana paratyphoid fever bacterium.Its F-V part is strong positive Developing restraint to staphylococcus aureus, shigella, bacillus pyocyaneus, its antibacterial activity is present in water-soluble portion and can be dissolved in the part of acetone with not being dissolved in water, additionally, its (more than 0.5g/ml concentration) has inhibitory action (plastic foam infiltration-antibacterial around-France) to diphtheria corynebacterium.
Vanilla: there is special fragrance, there is stimulation, have anti-rot, aid digestion, help hormone secretion, anxiety of releiving and improve the effects such as insomnia.At medical field, Parkinson's disease, urinary system disease, sexually transmitted disease (STD), heart disease, dermatosis etc. there is special efficacy.
Beneficial effects of the present invention:
The present invention is nontoxic, and abnormal smells from the patient is pure and fresh, has health-care effect, beneficially health, and it still is able to keep original intensity and quality after appropriate other function ingredients of interpolation.
1, tourmaline is a kind of silicate mineral, its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it contacts with hydrone under electrostatic field, hydrone just can be ionized into hydrion (H+) and hydroxide ion (OH-), hydroxide ion forms basic hydroxide group anion (H2O OH-) with water molecules, it is " negative aeroion ", scientific research at present proves: anion can not only facilitate human body synthesis and vitamin storage, strengthening and the physiological activity of human activin, the vital movement of human body and other biological there is highly important impact, it is referred to as " air vitamin ".Anion active adsorption indoor harmful substance, such as the construction and decoration harmful substance such as formaldehyde, toluene, not only self does not increase pollution, and Cress room air, it is inherently eliminated construction and decoration syndrome, ensures that health is unaffected, be the decorating and renovating material of a kind of environmental protection.
2, the Chinese medicine ingredients contained in the present invention: Fructus Forsythiae, Cortex Phellodendri, rhamnus crenata sieb.et zucc., lavandula angustifolia, Herba Anemones Hupehensis, Herba Duchesneae Indicae and vanilla, can not only expelling mosquito, also the multiple pathogenic bacterias such as staphylococcus, tubercule bacillus, bacillus pyocyaneus, gram-negative bacteria and gram-positive bacteria and fungus are had certain suppression, killing action, respiratory tract disease can be prevented, strengthen immune function of human body;Can fresh air, and can bacteriostasis and sterilization, simultaneously fragrant odour, character is gentle, pure and fresh soothes the spirit, and helps hormone secretion, and anxiety of releiving is improved the effects such as insomnia, can be helped for sleep, it is adaptable to the decoration of bedroom interior wall.
In addition; adhesive force of the present invention is strong, good leveling property; do not roll up skin, scrubbing resistance, resistance to polishing, do not fall off, do not chap, nontoxic, harmless, "dead"; can effectively protect body of wall; and organically combine with various coating, more it is essential that the life-time service present invention will not produce harmful effect to human body; it is applicable to each age groups, there is application prospect widely.
Detailed description of the invention
Embodiment 1.
A kind of vanilla broad-spectrum antiseptic type multi-effect putty, its raw material is made up of the material of following parts by weight: water 200kg, heavy calcium carbonate 70 kg, sierozem power 16 kg, white cement 15v, hydroxypropyl methyl cellulose 2.5 kg, anion natural mineral matter powder 6 kg, brightening agent 2 kg, Fructus Forsythiae 3 kg, Cortex Phellodendri 2 kg, rhamnus crenata sieb.et zucc. 2 kg, lavandula angustifolia 1.5 kg, Herba Anemones Hupehensis 2 kg, Herba Duchesneae Indicae 0.5kg, vanilla 1 kg, described anion natural mineral matter powder is tourmaline, the mixture of lanthanide rare composite salt and titanium oxide 5:2:3 by weight, wherein tourmaline is dravite and the mixture of elbaite 3:7 by weight.
Specifically, the fineness of described anion natural mineral matter powder is 6000 mesh;The viscosity of described hydroxypropyl methyl cellulose is 80000mPa s;The fineness particle diameter of described heavy calcium carbonate is 700;The fineness particle diameter of described sierozem power is 700 mesh;The fineness particle diameter of described white cement is 600 mesh;Described brightening agent uses environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this brightening agent is mainly used in brightening of papermaking, coating, ink and yarn fabric, it utilizes ANSD acid to be initial reactant, synthesize compounding mixed type fluorescent whitening agent, substantially solve pollution problem, expand the range of application of fluorescent whitening agent simultaneously.
The preparation method of a kind of vanilla broad-spectrum antiseptic type multi-effect putty, is made up of following step:
S1, take Fructus Forsythiae 3 kg, Cortex Phellodendri 2 kg, rhamnus crenata sieb.et zucc. 2 kg, lavandula angustifolia 1.5 kg respectively by above-mentioned each component, Herba Anemones Hupehensis 2 kg, Herba Duchesneae Indicae 0.5kg, vanilla 1 kg, and put into the Chinese medicinal powder being crushed to 1000 mesh in super micron mill respectively, standby;
S2, the Chinese medicinal powder in S1 and other raw material are put in large-scale mixing and blending machine, add the water of 200kg, be sufficiently stirred for mixing well 16 minutes, get product.
Embodiment 2.
A kind of vanilla broad-spectrum antiseptic type multi-effect putty, its raw material is made up of the material of following parts by weight: water 280kg heavy calcium carbonate 55 kg, sierozem power 25 kg, white cement 10 kg, hydroxypropyl methyl cellulose 4 kg, anion natural mineral matter powder 3 kg, brightening agent 2.5 kg, Fructus Forsythiae 2kg, Cortex Phellodendri 3kg, rhamnus crenata sieb.et zucc. 1 kg, lavandula angustifolia 1 kg, Herba Anemones Hupehensis 3 kg, Herba Duchesneae Indicae 1kg, vanilla 0.5 kg, described anion natural mineral matter powder is tourmaline, the mixture of lanthanide rare composite salt and titanium oxide 5:2:3 by weight, wherein tourmaline is dravite and the mixture of elbaite 3:7 by weight.
Specifically, the fineness of described anion natural mineral matter powder is 8000 mesh;The viscosity of described hydroxypropyl methyl cellulose is 100000mPa s;The fineness particle diameter of described heavy calcium carbonate is 1200 mesh;The fineness particle diameter of described sierozem power is 1200 mesh;The fineness particle diameter of described white cement is 800 mesh;Described brightening agent uses environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this brightening agent is mainly used in brightening of papermaking, coating, ink and yarn fabric, it utilizes ANSD acid to be initial reactant, synthesize compounding mixed type fluorescent whitening agent, substantially solve pollution problem, expand the range of application of fluorescent whitening agent simultaneously.
Its further technical scheme is, the preparation method of a kind of vanilla broad-spectrum antiseptic type multi-effect putty, is made up of following step:
S1, take Fructus Forsythiae 2kg respectively by above-mentioned each component, Cortex Phellodendri 3kg, rhamnus crenata sieb.et zucc. 1 kg, lavandula angustifolia 1 kg, Herba Anemones Hupehensis 3 kg, Herba Duchesneae Indicae 1kg vanilla 0.5 kg, and put into the Chinese medicinal powder being crushed to 1200 mesh in super micron mill respectively, standby;
S2, the Chinese medicinal powder in S1 and other raw material are put in large-scale mixing and blending machine, add the water of 280kg, be sufficiently stirred for mixing well 15-20 minute, get product.
Common putty 1.
Heavy calcium carbonate 80kg, sierozem power 25kg, white cement 40kg, HPMC4kg, ultramarine 0.9kg, water 200kg.
Common putty 2.
Sierozem power 20kg, ground calcium carbonate 50 kg, precipitated calcium carbonate 30 kg, Pulvis Talci 100 kg, lithopone 45 kg, titanium dioxide 30 kg, polyvinyl alcohol 10 kg, edible vegetable oil 3.5 kg, machine oil 1.5 kg, 95% industrial alcohol 2 kg, 10% amide solution 1.5 kg, water 380 kg.
The method checking above-mentioned putty is as follows:
(1) putty of embodiment 1 and 2, sampled through Zhongshan city's mass metrology supervisory detection and tested, product of the present invention is carried out the performance tests such as water-fast, alkaline-resisting, antibacterial, Durability of antimicrobial effect, soluble heavy metal content, wherein main performance test is with reference to country JG/T3049---1998 " architecture indoor putty ", antibacterial and mouldproof test is with reference to the requirement of the standard of HG/T3950-2007 " paint film antibacterial and mouldproof method of testing ", and test result asks for an interview table 1.
(2) purifying formaldehyde test:
The standard specified according to JC/T1074-2008 " function of purifying indoor air coating material purifying property " according to the putty in above-described embodiment 1 and embodiment 2 is tested:
At 41 m3The customized chest fully sealed in, being criticized respectively with the putty in embodiment 1 in the present invention and embodiment 2 by common putty scrapes on four faces of chest, treat that putty is dried, spray into 5 ml concentration is the formalin of 36% simultaneously, when formalin is volatilized completely in airtight chest (about 30 minutes), then after 4 hours carry out the content of for the first time sampling and measuring formaldehyde, take sample after 12 hours, after 24 hours respectively and measure the content of formaldehyde in air.
Phenol reagent method is utilized to measure the content of formaldehyde, its principle is: the formaldehyde in air generates piperazine after reacting with phenol reagent, and piperazine is formed glaucous compound, then further according to the depth of color by ferric ion oxidation in an acidic solution, colorimetric carries out quantitatively, to obtain a result.
4 sub-samplings are respectively labeled as A1, A2, A3, A4, and test data ask for an interview table 2.
Conclusion: the putty in Example 1 and Example 2 of the present invention all can play the effect of good purifying formaldehyde, compared with the putty common with on market, the present invention has certain advantage.
(3) anion collecting test.
Being tempered respectively with the putty in Example 1 and Example 2 of the present invention by common putty (common putty 1 and common putty 2) of the prior art, brush is at 20 × 20cm2Plank on, dry, then brush emulsion paint on this plank, then dry, lie on grating type ion collectors, harvester is put into 0.4 m3Closed bin in, carry out follow-on test with still air ion tester, test result shows: in the putty in Example 1 and Example 2 of the present invention, anion average increase is 1617/scm3, contrasting common putty anion average increase is 1180/scm3, and sustained release negative aeroion, it is more beneficial for purifying the air of a room for a long time;And the anion quantity that common putty (common putty 1 and common putty 2) of the prior art is discharged is 0/scm3, it does not possess the function of anion releasing.
Conclusion: the putty in Example 1 and Example 2 of the present invention all can purify the air of a room with sustained release negative aeroion for a long time, compared with common putty (common putty 1 and common putty 2) of the prior art, the present invention has obviously advantage.
(4) repelling effect test.
Carrying out contrast test according to common putty (common putty 1 and common putty 2) of the prior art with the repelling effect of putty in above-described embodiment 1 and embodiment 2, test data ask for an interview table 3.
Conclusion: the putty in Example 1 and Example 2 of the present invention all can play good mosquito-repelling function, compared with the putty common with on market, the present invention has obviously repelling effect.
The foregoing is only presently preferred embodiments of the present invention; not in order to limit the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here without also cannot all of embodiment be given exhaustive; all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. done, within being still included in protection scope of the present invention.

Claims (1)

  1. null1. the preparation method of a vanilla broad-spectrum antiseptic type multi-effect putty,It is characterized in that: this putty raw material is made up of the material of following parts by weight: water 200-280 part,Heavy calcium carbonate 55-70 part,Sierozem power 16-25 part,White cement 10-15 part,Hydroxypropyl methyl cellulose 2.5-4 part,Anion natural mineral matter powder 3-6 part,Brightening agent 2-2.5 part,Fructus Forsythiae 2-3 part,Cortex Phellodendri 2-3 part,Rhamnus crenata sieb.et zucc. 1-2 part,Lavandula angustifolia 1-1.5 part,Herba Anemones Hupehensis 2-3 part,Herba Duchesneae Indicae 0.5-1 part,Vanilla 0.5-1 part,The fineness of described anion natural mineral matter powder is 1000-8000 mesh,Described anion natural mineral matter powder is tourmaline、The mixture of lanthanide rare composite salt and titanium oxide 5:2:3 by weight,Wherein tourmaline is dravite and the mixture of elbaite 3:7 by weight,The viscosity of described hydroxypropyl methyl cellulose is 80000-100000mPa s;The fineness particle diameter of described heavy calcium carbonate is 600-1200 mesh;The fineness particle diameter of described sierozem power is 600-1200 mesh;The fineness particle diameter of described white cement is 500-800 mesh;Described brightening agent uses environment friendly triazine amino stilbene fluorescent bleachng agent, and its preparation method is made up of following step:
    S1, take Fructus Forsythiae 2-3 part, Cortex Phellodendri 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part respectively by above-mentioned each component, lavandula angustifolia 1-1.5 part, Herba Anemones Hupehensis 2-3 part, Herba Duchesneae Indicae 0.5-1 part, vanilla 0.5-1 part, and put into the Chinese medicinal powder being crushed to 800-1200 mesh in super micron mill respectively, standby;
    S2, the Chinese medicinal powder in S1 and other raw material are put in large-scale mixing and blending machine, be sufficiently stirred for mixing well 15-20 minute, get product.
CN201410411475.XA 2014-08-20 2014-08-20 A kind of vanilla broad-spectrum antiseptic type multi-effect putty and preparation method Active CN104292931B (en)

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CN107400400A (en) * 2017-09-23 2017-11-28 江苏昶浩建材有限公司 A kind of negative ion putty powder
CN108530972A (en) * 2018-07-17 2018-09-14 合肥欧仕嘉机电设备有限公司 A kind of preparation method of high-quality exterior wall putty

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CN1908084A (en) * 2006-08-18 2007-02-07 黄华信 Application of phellodendron in coating manufacture
CN101173123A (en) * 2007-11-10 2008-05-07 刘艳臣 Novel water-proof whitening lacquer putty, production method and use method
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CN103725075A (en) * 2013-12-04 2014-04-16 重庆泰睿新型建筑材料有限公司 Interior wall putty powder

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Publication number Priority date Publication date Assignee Title
CN1398933A (en) * 2002-07-08 2003-02-26 北京市建筑涂料厂 Inner wall paint and putty capable of producing negative air ion
CN1908084A (en) * 2006-08-18 2007-02-07 黄华信 Application of phellodendron in coating manufacture
CN101173123A (en) * 2007-11-10 2008-05-07 刘艳臣 Novel water-proof whitening lacquer putty, production method and use method
CN102910874A (en) * 2012-11-13 2013-02-06 辽宁啄木鸟漆业发展有限公司 Negative ion putty powder
CN103725075A (en) * 2013-12-04 2014-04-16 重庆泰睿新型建筑材料有限公司 Interior wall putty powder

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