CN104292931A - Vanillan broad-spectrum antibiosis-type multiple-effect putty and preparation method thereof - Google Patents
Vanillan broad-spectrum antibiosis-type multiple-effect putty and preparation method thereof Download PDFInfo
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- CN104292931A CN104292931A CN201410411475.XA CN201410411475A CN104292931A CN 104292931 A CN104292931 A CN 104292931A CN 201410411475 A CN201410411475 A CN 201410411475A CN 104292931 A CN104292931 A CN 104292931A
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- putty
- negative ion
- vanilla
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention relates to a vanillan broad-spectrum antibiosis-type multiple-effect putty, which comprises the following raw materials by weight part: 200-280 parts of water, 55-70 parts of heavy calcium carbonate powder, 16-25 parts of calcium powder, 10-15 parts of white cement, 2.5-4 parts of hydroxypropyl methyl cellulose, 3-6 parts of negative ion natural mineral matter powder, 2-2.5 parts of brightening agent, 2-3 parts of fructus forsythia, 2-3 parts of phellodendron, 1-2 parts of Rhamnus crenata, 1-1.5 parts of lavender, 2-3 parts of Anemone hupehensis, 0.5-1 part of Duchesnea indica and 0.5-1 part of vanillan; the negative ion natural mineral matter powder is a mixture of tourmalinite, lanthanide rare earth composite salt and titanium oxide according to weight ratio being 5: 2: 3, and tourmalinite is a mixture of dravite and elbaite according to weight ratio of 3: 7. The multiple-effect putty can release air negative ion for long-term, and has certain inhibition and killing effects for a plurality of pathogen and fungi such as staphylococcus, escherichia coli and gram positive bacteria.
Description
Technical field
The present invention relates to a kind of building and ornament materials, particularly a kind of vanilla broad-spectrum antimicrobial type multi-effect putty and preparation method.
Background technology
Putty powder, it is widely used in construction and decoration as metope packing material, the impregnating material used in traditional putty, also containing multiple volatile harmful materials such as formaldehyde, benzene, radon, ammonia in it, pollute room air, and present building generally ventilates, for a long time in such room not good, health for people brings serious threat, destroys the living environment of people; On the other hand, traditional putty paste only plays filling effect, does not possess other function, can not meet the daily demand of people.
Summary of the invention
For the deficiency that prior art exists, one of technical problem to be solved by this invention is to provide a kind of Environmental Safety, nontoxic, smell is pure and fresh, there is a kind of vanilla broad-spectrum antimicrobial type multi-effect putty of health-care effect, not only can release air negative ion for a long time, purify air, be beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, be applicable to each age groups to human body.
Two of technical problem to be solved by this invention is to provide a kind of preparation method of vanilla broad-spectrum antimicrobial type multi-effect putty.
The object of the invention is to be achieved through the following technical solutions:
A kind of vanilla broad-spectrum antimicrobial type multi-effect putty, its raw material is made up of the material of following parts by weight: water 200-280 part, heavy calcium carbonate 55-70 part, sierozem power 16-25 part, white cement 10-15 part, Vltra tears 2.5-4 part, negative ion natural mineral matter powder 3-6 part, whitening agent 2-2.5 part, capsule of weeping forsythia 2-3 part, golden cypress 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part, lavandula angustifolia 1-1.5 part, Hupeh Anemone Herb 2-3 part, mock-strawberry 0.5-1 part, vanilla 0.5-1 part, described negative ion natural mineral matter powder is tourmalinite, lanthanide rare composite salt and titanium oxide are by weight the mixture of 5:2:3, wherein tourmalinite is dravite and the elbaite mixture by weight 3:7.
Specifically, the fineness of described negative ion natural mineral matter powder is 1000-8000 order; The viscosity of described Vltra tears is 80000-100000 mPas; The fineness particle diameter of described heavy calcium carbonate is 600-1200 order; The fineness particle diameter of described sierozem power is 600-1200 order; The fineness particle diameter of described white cement is 500-800 order; Described whitening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this whitening agent is mainly used in papermaking, coating, the brightening of ink and yarn fabric, it utilizes ANSD acid to be initial reactant, synthesize composite mixed type white dyes, substantially solve pollution problem, expand the range of application of white dyes simultaneously.
A preparation method for vanilla broad-spectrum antimicrobial type multi-effect putty, is made up of following step:
S1, get capsule of weeping forsythia 2-3 part respectively by above-mentioned each component, golden cypress 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part, lavandula angustifolia 1-1.5 part, Hupeh Anemone Herb 2-3 part, mock-strawberry 0.5-1 part, vanilla 0.5-1 part, and drop in supper micron mill respectively and be crushed to 800-1200 object herb powder, for subsequent use;
S2, the herb powder in S1 and other raw material to be dropped in large-scale mixing and blending machine, add appropriate water, fully stir and mix well 15-20 minute, get product.
The present invention is with reference to modern Chinese herbal medicine pharmacological research, and from the drug screening of existing Chinese medicine with repeatedly verify, give full play to each component and act synergistically, the effect brief introduction of wherein adopted Chinese medicine material is as follows.
The capsule of weeping forsythia: clearing heat and detoxicating, dispersing swelling and dissipating binds, dispelling wind and heat pathogens, have the title of " persons particularly liable to develop skin infection's panacea ", can suppress Corynebacterium diphtheriae, paratyphosum Bacterium, intestinal bacteria, dysentery bacterium, diphtheria corynebacterium and vibrio cholerae, staphylococcus, suis etc.
Golden cypress: to streptococcus aureus, streptococcus pneumoniae, diphtheria corynebacterium, Streptococcus viridans, dysentery bacterium (except Song Nei Shi), Hemolytic streptococcus, meningococcus, vibrio cholerae, anthrax bacillus all effectively or have stronger restraining effect; Also restraining effect is had to Bacillus subtilus, bordetella pertussis, tetanus bacillus.
Rhamnus crenata sieb.et zucc.:: machaka or dungarunga, Gen Pi or complete stool are used as medicine, and property is flat, bitter, dry, sterilization, desinsection.
Lavandula angustifolia: ant can be removed, except roach, except mite, when being placed under wardrobe, pillow, not only mothball can be replaced, the fragrance of one people that oozes can also be left, research finds, lavandula angustifolia has obvious anti-microbial effect, and the phantol contained in lavandula angustifolia is the antibacterial main component of lavandula angustifolia, and it can suppress the growth of 17 kinds of bacteriums (comprising gram-negative bacteria and gram-positive bacteria), 10 kinds of fungies.
Hupeh Anemone Herb: 1. " Shaanxi herbal medicine ": " bitter, cool, slightly poisonous." 2. " herbal medicine is commonly used in Sichuan ": " and toil, temperature, slightly poisonous." [chemical composition] root and herb are containing Pulsatilla camphor (anemonin) and triterpene soap Oleanolic Acid-3-O-β-D-ribopyranose base-(1 → 3)-α-L-rhamnopyranosyl-(1 → 3)-α-L-arabopyranose glucoside, Oleanolic Acid 3-O-β-D-ribopyranose base-(1 → 3)-α-L-rhamnopyranosyl-(1 → 2)-β-D-xylopyranose glucoside, and Oleanolic Acid.[function cures mainly] kills maggot, wriggler, eliminate indigestion, detumescence, and the loose stasis of blood, controls stubborn dermatitis, the favus of the scalp, malaria, infantile malnutrition, dysentery, and carbuncle furuncle sore swells, scrofula, wound.
Mock-strawberry: " national herbal medicine compilation " is recorded: perennial herb, and complete stool has pubescence; Stolon is long, herb hyoscine, have clearing heat and detoxicating, Huoxue San " is remorse, astringing to arrest bleeding effect, can control venomous snake bite again, apply control furunculosis etc.; And for killing fly maggot, there is F-I, the F-II, F-III part that are separated in anti-microbial effect mock-strawberry the growth of streptococcus aureus and shigella, in suppressing positive, is the weak positive to Pseudomonas aeruginosa, is negative to sramana's paratyphoid bacterium.Its F-V part is strong positive Developing restraint to streptococcus aureus, shigella, Pseudomonas aeruginosa, its anti-microbial activity is present in water-soluble portion and can not be water-soluble but can be dissolved in the part of acetone, in addition, its (more than 0.5g/ml concentration) has restraining effect (plastic foam infiltration-antibacterial around-France) to diphtheria corynebacterium.
Vanilla: there is special fragrance, there is hormesis, have anti-rotten, aid digestion, help hormone secretion, the effect such as anxiety of releiving and improvement insomnia.At medical field, there is special efficacy to parkinsonism, urinary system disease, venereal disease, heart trouble, tetter etc.
Beneficial effect of the present invention:
The present invention is nontoxic, and smell is pure and fresh, has health-care effect, is conducive to HUMAN HEALTH, and it still can keep original intensity and quality after appropriate other function ingredients of interpolation.
1, tourmalinite is a kind of silicate minerals, its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it contacts with water molecules under electrostatic field, just water molecules can be ionized into hydrogen ion (H+) and hydroxide ion (OH-), hydroxide ion and water molecules form basic hydroxide group negative ion (H2OOH-), be " negative aeroion ", current scientific research proves: negative ion can not only facilitate human body to synthesize and vitamin storage, the physiological activity of strengthening and human activin, very important impact is had on the vital movement of human body and other biological, be called as " air VITAMIN ".The indoor objectionable impurities of negative ion active adsorption, as the construction and decoration such as formaldehyde, toluene objectionable impurities, not only self does not increase pollution, and Cress room air, fundamentally eliminate construction and decoration syndromes, ensureing that HUMAN HEALTH is unaffected, is a kind of decorating and renovating material of environmental protection.
2, the traditional Chinese medicine ingredients contained in the present invention: the capsule of weeping forsythia, golden cypress, rhamnus crenata sieb.et zucc., lavandula angustifolia, Hupeh Anemone Herb, mock-strawberry and vanilla, can not only expelling mosquito, also there are certain suppression, killing action to the multiple germs such as staphylococcus, tubercule bacillus, Pseudomonas aeruginosa, gram-negative bacteria and gram-positive bacteria and fungi, can respiratory tract disease be prevented, strengthen immune function of human body; Can fresh air, and can restraining and sterilizing bacteria, simultaneously fragrant odour, character is gentle, pure and freshly soothes the spirit, and helps hormone secretion, anxiety of releiving, improves the effects such as insomnia, can help for sleep, be applicable to the decoration of bedroom interior wall.
In addition; strong adhesion of the present invention, good leveling property; do not roll up skin, scrubbing resistance, resistance to polishing, do not come off, do not chap, nontoxic, harmless, "dead"; effectively can protect body of wall; and organically combine with various coating, more crucially, life-time service the present invention can not produce detrimentally affect to human body; be applicable to each age groups, there is application prospect widely.
Embodiment
Embodiment 1.
A kind of vanilla broad-spectrum antimicrobial type multi-effect putty, its raw material is made up of the material of following parts by weight: water 200kg, heavy calcium carbonate 70 kg, sierozem power 16 kg, white cement 15v, Vltra tears 2.5 kg, negative ion natural mineral matter powder 6 kg, whitening agent 2 kg, the capsule of weeping forsythia 3 kg, golden cypress 2 kg, rhamnus crenata sieb.et zucc. 2 kg, lavandula angustifolia 1.5 kg, Hupeh Anemone Herb 2 kg, mock-strawberry 0.5kg, vanilla 1 kg, described negative ion natural mineral matter powder is tourmalinite, lanthanide rare composite salt and titanium oxide are by weight the mixture of 5:2:3, wherein tourmalinite is dravite and the elbaite mixture by weight 3:7.
Specifically, the fineness of described negative ion natural mineral matter powder is 6000 orders; The viscosity of described Vltra tears is 80000mPas; The fineness particle diameter of described heavy calcium carbonate is 700; The fineness particle diameter of described sierozem power is 700 orders; The fineness particle diameter of described white cement is 600 orders; Described whitening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this whitening agent is mainly used in papermaking, coating, the brightening of ink and yarn fabric, it utilizes ANSD acid to be initial reactant, synthesize composite mixed type white dyes, substantially solve pollution problem, expand the range of application of white dyes simultaneously.
A preparation method for vanilla broad-spectrum antimicrobial type multi-effect putty, is made up of following step:
S1, get the capsule of weeping forsythia 3 kg respectively by above-mentioned each component, golden cypress 2 kg, rhamnus crenata sieb.et zucc. 2 kg, lavandula angustifolia 1.5 kg, Hupeh Anemone Herb 2 kg, mock-strawberry 0.5kg, vanilla 1 kg, and drop in supper micron mill respectively and be crushed to 1000 object herb powders, for subsequent use;
S2, the herb powder in S1 and other raw material to be dropped in large-scale mixing and blending machine, add the water of 200kg, fully stir and mix well 16 minutes, get product.
Embodiment 2.
A kind of vanilla broad-spectrum antimicrobial type multi-effect putty, its raw material is made up of the material of following parts by weight: water 280kg heavy calcium carbonate 55 kg, sierozem power 25 kg, white cement 10 kg, Vltra tears 4 kg, negative ion natural mineral matter powder 3 kg, whitening agent 2.5 kg, capsule of weeping forsythia 2kg, golden cypress 3kg, rhamnus crenata sieb.et zucc. 1 kg, lavandula angustifolia 1 kg, Hupeh Anemone Herb 3 kg, mock-strawberry 1kg, vanilla 0.5 kg, described negative ion natural mineral matter powder is tourmalinite, lanthanide rare composite salt and titanium oxide are by weight the mixture of 5:2:3, wherein tourmalinite is dravite and the elbaite mixture by weight 3:7.
Specifically, the fineness of described negative ion natural mineral matter powder is 8000 orders; The viscosity of described Vltra tears is 100000mPas; The fineness particle diameter of described heavy calcium carbonate is 1200 orders; The fineness particle diameter of described sierozem power is 1200 orders; The fineness particle diameter of described white cement is 800 orders; Described whitening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this whitening agent is mainly used in papermaking, coating, the brightening of ink and yarn fabric, it utilizes ANSD acid to be initial reactant, synthesize composite mixed type white dyes, substantially solve pollution problem, expand the range of application of white dyes simultaneously.
Its further technical scheme is, a kind of preparation method of vanilla broad-spectrum antimicrobial type multi-effect putty, is made up of following step:
S1, get capsule of weeping forsythia 2kg respectively by above-mentioned each component, golden cypress 3kg, rhamnus crenata sieb.et zucc. 1 kg, lavandula angustifolia 1 kg, Hupeh Anemone Herb 3 kg, mock-strawberry 1kg vanilla 0.5 kg, and drop in supper micron mill respectively and be crushed to 1200 object herb powders, for subsequent use;
S2, the herb powder in S1 and other raw material to be dropped in large-scale mixing and blending machine, add the water of 280kg, fully stir and mix well 15-20 minute, get product.
Common putty 1.
Heavy calcium carbonate 80kg, sierozem power 25kg, white cement 40kg, HPMC4kg, ultramarine 0.9kg, water 200kg.
Common putty 2.
Sierozem power 20kg, water-ground limestone 50 kg, light calcium carbonate 30 kg, talcum powder 100 kg, zinc sulfide white 45 kg, titanium dioxide 30 kg, polyvinyl alcohol 10 kg, edible vegetable oil 3.5 kg, machine oil 1.5 kg, 95% industrial spirit 2 kg, 10% amide solution 1.5 kg, water 380 kg.
Check the method for above-mentioned putty as follows:
(1) putty of embodiment 1 and 2, sample through Zhongshan city's mass metrology supervisory detection and test, water-fast, alkaline-resisting, antibacterial, the performance test such as Durability of antimicrobial effect, soluble heavy metal content is carried out to product of the present invention, wherein salient features test is with reference to national JG/T3049---1998 " architecture indoor putty ", antibacterial and mouldproof test is with reference to the requirement of the standard of HG/T3950-2007 " paint film antibacterial and mouldproof testing method ", and test result asks for an interview table 1.
(2) purifying formaldehyde test:
Test according to JC/T1074-2008 " function of purifying indoor air coating material purifying property " specified standards according to the putty in above-described embodiment 1 and embodiment 2:
At 41 m
3complete hermetic chest customized in, putty in embodiment 1 in common putty and the present invention and embodiment 2 is criticized respectively and scrapes on four faces of chest, after putty drying, spray into 5 ml concentration is the formaldehyde solution of 36% simultaneously, when formaldehyde solution is volatilized completely in airtight chest (about 30 minutes), then after 4 hours carry out the content of first time sampling and measuring formaldehyde, after 12 hours, after 24 hours, get the content that sample measures formaldehyde in air respectively.
Phenol reagent method is utilized to measure the content of formaldehyde, its principle is: generate piperazine after the formaldehyde in air and phenol reagent react, and piperazine is formed glaucous compound by ferric ion oxidation in an acidic solution, and then according to the depth of color, colorimetric is carried out quantitatively, to obtain a result.
4 sub-samplings are labeled as A1, A2, A3, A4 respectively, and test data asks for an interview table 2.
Conclusion: the putty in the embodiment of the present invention 1 and embodiment 2 all can play the effect of good purifying formaldehyde, and compared with putty common on market, the present invention has certain advantage.
(3) negative ion collecting test.
Common putty of the prior art (common putty 1 and common putty 2) and the putty in the embodiment of the present invention 1 and embodiment 2 are tempered respectively, brushes at 20 × 20cm
2plank on, dry, then brush emulsion paint on this plank, then dry, lie on grating ion collectors, collector is put into 0.4 m
3closed bin in, carry out continuously tested with still air ion tester, test result shows: in the putty in the embodiment of the present invention 1 and embodiment 2, negative ion average increase is 1617/scm
3, contrasting common putty negative ion average increase is 1180/scm
3, and sustained release negative aeroion, be more conducive to purifying the air of a room for a long time; And the negative ion quantity that common putty of the prior art (common putty 1 and common putty 2) discharges is 0/scm
3, it does not possess the function of anion releasing.
Conclusion: the putty in the embodiment of the present invention 1 and embodiment 2 all can sustained release negative aeroion, and purify the air of a room for a long time, compare with common putty of the prior art (common putty 1 and common putty 2), the present invention has obviously advantage.
(4) repelling effect test.
Carry out contrast test according to common putty of the prior art (common putty 1 and common putty 2) and the repelling effect of putty in above-described embodiment 1 and embodiment 2, test data asks for an interview table 3.
Conclusion: the putty in the embodiment of the present invention 1 and embodiment 2 all can play good mosquito-repelling function, and compared with putty common on market, the present invention has obviously repelling effect.
The foregoing is only preferred embodiment of the present invention; not in order to limit the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here exhaustive without the need to also giving all embodiments; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., be still included within protection scope of the present invention.
Claims (3)
1. a vanilla broad-spectrum antimicrobial type multi-effect putty, it is characterized in that: its raw material is made up of the material of following parts by weight: water 200-280 part, heavy calcium carbonate 55-70 part, sierozem power 16-25 part, white cement 10-15 part, Vltra tears 2.5-4 part, negative ion natural mineral matter powder 3-6 part, whitening agent 2-2.5 part, capsule of weeping forsythia 2-3 part, golden cypress 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part, lavandula angustifolia 1-1.5 part, Hupeh Anemone Herb 2-3 part, mock-strawberry 0.5-1 part, vanilla 0.5-1 part, the fineness of described negative ion natural mineral matter powder is 1000-8000 order, described negative ion natural mineral matter powder is tourmalinite, lanthanide rare composite salt and titanium oxide are by weight the mixture of 5:2:3, wherein tourmalinite is dravite and the elbaite mixture by weight 3:7.
2. a kind of vanilla broad-spectrum antimicrobial type multi-effect putty as claimed in claim 1, is characterized in that: the viscosity of described Vltra tears is 80000-100000mPas; The fineness particle diameter of described heavy calcium carbonate is 600-1200 order; The fineness particle diameter of described sierozem power is 600-1200 order; The fineness particle diameter of described white cement is 500-800 order; Described whitening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent.
3. a preparation method for vanilla broad-spectrum antimicrobial type multi-effect putty, is characterized in that: be made up of following step:
S1, get capsule of weeping forsythia 2-3 part respectively by above-mentioned each component, golden cypress 2-3 part, rhamnus crenata sieb.et zucc. 1-2 part, lavandula angustifolia 1-1.5 part, Hupeh Anemone Herb 2-3 part, mock-strawberry 0.5-1 part, vanilla 0.5-1 part, and drop in supper micron mill respectively and be crushed to 800-1200 object herb powder, for subsequent use;
S2, the herb powder in S1 and other raw material to be dropped in large-scale mixing and blending machine, add appropriate water, fully stir and mix well 15-20 minute, get product.
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