CN104263550A - Makeup solution glass bottle detergent - Google Patents
Makeup solution glass bottle detergent Download PDFInfo
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- CN104263550A CN104263550A CN201410462165.0A CN201410462165A CN104263550A CN 104263550 A CN104263550 A CN 104263550A CN 201410462165 A CN201410462165 A CN 201410462165A CN 104263550 A CN104263550 A CN 104263550A
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Abstract
The invention relates to a makeup solution glass bottle detergent, belonging to the technical field of cleaning supplies. The makeup solution glass bottle detergent is prepared from water, 2-methyl-5-oxo-cyclopentano-1-enol propionate, 3,5-di-tert-butyl-4-hydroxy-benzyl alcohol, 3,7-dimethyl-9-(2,6,6-trimethylcyclohexenyl)-2,4,6,8-all-trans-nona-tetraenoic acid, sodium 4-methyl-2-oxo-valerate, 2-methyl-2-propyl-1,3-propanediol dicarbamate, potassium 1,2,3,6-tetrahydro-2,6-dioxopyrimidyl-4-carboxylate and the like. The makeup solution glass bottle detergent has favorable impurity removal effect on the glass material by utilizing the interaction and mutual influence among the related chemical components. The makeup solution glass bottle detergent contains safe and non-irritating materials, can remove organic impurities harmful to the skin in the makeup solution glass bottle, is non-irritating for the skin, and effectively ensures the use effect of the makeup solution.
Description
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Technical field
The present invention relates to skin lotion vial sanitising agent, belong to cleaning supplies technical field.
background technology
Be called as the Chinese Cosmetic Market of " beautiful economic ", through the fast development of more than 20 years, achieve unprecedented achievement now, and skin lotion has widely used in female group as a kind of care compositions wherein, its good soothing effect obtains the consistent approval of numerous women.And as face protection product, the quality of skin lotion quality directly affects the image appearance of user, the daily life quality of extreme influence user, thus, while the quality of guarantee skin lotion own, also need to keep a close eye on the clean of cosmetics containers that can affect its using character, namely cosmetics containers are necessary to carry out safely cleaning targetedly to it before use.
Summary of the invention
The object of the present invention is to provide a kind of cleaning capacity strong and skin lotion vial sanitising agent to no skin irritation.
Technical problem of the present invention, is achieved by following technical proposals:
Skin lotion vial sanitising agent, special character is to be prepared from by the raw material of following weight: 75 parts, water, 2-methyl-5-oxo ring penta-1-enol propionic ester 22-24 part, 3, 5-di-t-butyl-4-hydroxy-benzyl alcohol 26-28 part, 3, 7-dimethyl-9-(2, 6, 6-trimethyl cyclohexene)-2, 4, 6, 8-alltrans nona tetraenoic acid 16-18 part, 4-methyl-2-oxo-pentanoic acid sodium salt 16-18 part, 2-methyl-2-propyl-1, ammediol diurethanes 12-15 part, 1, 2, 3, 6-tetrahydrochysene-2, 6-dioxo pyrimidine-4-carboxylic acid potassium salt 10-12 part, methylpentanolone 6-8 part, 4-urocanic acid 4-6 part.
Preparation method of the present invention: by deionized water, 2-methyl-5-oxo ring penta-1-enol propionic ester, 3, 5-di-t-butyl-4-hydroxy-benzyl alcohol, 3, 7-dimethyl-9-(2, 6, 6-trimethyl cyclohexene)-2, 4, 6, 8-alltrans nona tetraenoic acid, 4-methyl-2-oxo-pentanoic acid sodium salt to add in reactor 1 stirring and dissolving at 40-50 DEG C, by 2-methyl-2-propyl-1, ammediol diurethanes, 1, 2, 3, 6-tetrahydrochysene-2, 6-dioxo pyrimidine-4-carboxylic acid potassium salt, methylpentanolone, 4-urocanic acid stirring and dissolving at 50-60 DEG C in reactor 2, mixture in reactor 2 is joined gradually in reactor 1, fully 15-25 minute is stirred in 45 DEG C of waters bath with thermostatic control, leave standstill 1-2 hour, namely required skin lotion vial sanitising agent is obtained.
This skin lotion vial sanitising agent, utilizes the interaction between related chemical constituents, influences each other, and has good Impurity removal effect to glass material.In addition, its material itself is safe and non-stimulating, can not only remove organic impurity harmful to skin in skin lotion vial, and itself to skin without any pungency, effectively ensure the result of use of skin lotion.
Embodiment
Below provide the specific embodiment of the present invention, be used for being further described the present invention.In the present invention, if no special instructions, each raw material all in working substance content for 100%.
In following examples and comparative example, raw material introduction:
2-methyl-5-oxo ring penta-1-enol propionic ester, CAS accession number is: 87-55-8;
3,5-di-t-butyl-4-hydroxy-benzyl alcohol, CAS accession number is: 88-26-6;
3,7-dimethyl-9-(2,6,6-trimethyl cyclohexene)-2,4,6,8-alltrans nona tetraenoic acid, CAS accession number is: 302-79-4;
4-methyl-2-oxo-pentanoic acid sodium salt, CAS accession number is: 4502-00-5;
2-methyl-2-propyl-1,3-PD diurethanes, CAS accession number is: 57-53-4;
1,2,3,6-tetrahydrochysene-2,6-dioxo pyrimidine-4-carboxylic acid potassium salt, CAS accession number is: 24598-73-0;
Methylpentanolone, CAS accession number is: 123-42-2;
4-urocanic acid, CAS accession number is: 104-98-3.
Embodiment 1
Weigh: water 75kg, 2-methyl-5-oxo ring penta-1-enol propionic ester 22kg, 3,5-di-t-butyl-4-hydroxy-benzyl alcohol 27kg, 3,7-dimethyl-9-(2,6,6-trimethyl cyclohexene)-2,4,6,8-alltrans nona tetraenoic acid 18kg, 4-methyl-2-oxo-pentanoic acid sodium salt 17kg, 2-methyl-2-propyl-1,3-PD diurethanes 12kg, 1,2,3,6-tetrahydrochysene-2,6-dioxo pyrimidine-4-carboxylic acid potassium salt 11kg, methylpentanolone 8kg, 4-urocanic acid 5kg.
The preparation method of this embodiment skin lotion vial sanitising agent: by deionized water, 2-methyl-5-oxo ring penta-1-enol propionic ester, 3, 5-di-t-butyl-4-hydroxy-benzyl alcohol, 3, 7-dimethyl-9-(2, 6, 6-trimethyl cyclohexene)-2, 4, 6, 8-alltrans nona tetraenoic acid, 4-methyl-2-oxo-pentanoic acid sodium salt to add in reactor 1 stirring and dissolving at 40-50 DEG C, by 2-methyl-2-propyl-1, ammediol diurethanes, 1, 2, 3, 6-tetrahydrochysene-2, 6-dioxo pyrimidine-4-carboxylic acid potassium salt, methylpentanolone, 4-urocanic acid stirring and dissolving at 50-60 DEG C in reactor 2, mixture in reactor 2 is joined gradually in reactor 1, fully 15-25 minute is stirred in 45 DEG C of waters bath with thermostatic control, leave standstill 1-2 hour, namely required skin lotion vial sanitising agent is obtained.
Embodiment 2
Weigh: water 75kg, 2-methyl-5-oxo ring penta-1-enol propionic ester 24kg, 3,5-di-t-butyl-4-hydroxy-benzyl alcohol 28kg, 3,7-dimethyl-9-(2,6,6-trimethyl cyclohexene)-2,4,6,8-alltrans nona tetraenoic acid 17kg, 4-methyl-2-oxo-pentanoic acid sodium salt 18kg, 2-methyl-2-propyl-1,3-PD diurethanes 13kg, 1,2,3,6-tetrahydrochysene-2,6-dioxo pyrimidine-4-carboxylic acid potassium salt 12kg, methylpentanolone 7kg, 4-urocanic acid 6kg.
The preparation method of this embodiment skin lotion vial sanitising agent is with embodiment 1.
Embodiment 3
Weigh: water 75kg, 2-methyl-5-oxo ring penta-1-enol propionic ester 23kg, 3,5-di-t-butyl-4-hydroxy-benzyl alcohol 26kg, 3,7-dimethyl-9-(2,6,6-trimethyl cyclohexene)-2,4,6,8-alltrans nona tetraenoic acid 16kg, 4-methyl-2-oxo-pentanoic acid sodium salt 16kg, 2-methyl-2-propyl-1,3-PD diurethanes 15kg, 1,2,3,6-tetrahydrochysene-2,6-dioxo pyrimidine-4-carboxylic acid potassium salt 10kg, methylpentanolone 6kg, 4-urocanic acid 4kg.
The preparation method of this embodiment skin lotion vial sanitising agent is with embodiment 1.
Comparative example 1
Weigh: water 75kg, 2-methyl-5-oxo ring penta-1-enol propionic ester 22kg, 7-dimethyl-9-(2,6,6-trimethyl cyclohexene)-2,4,6,8-alltrans nona tetraenoic acid 18kg, 4-methyl-2-oxo-pentanoic acid sodium salt 17kg, 1,2,3,6-tetrahydrochysene-2,6-dioxo pyrimidine-4-carboxylic acid potassium salt 11kg, methylpentanolone 8kg, 4-urocanic acid 5kg.
The preparation method of this comparative example skin lotion vial sanitising agent: by deionized water, 2-methyl-5-oxo ring penta-1-enol propionic ester, 3, 7-dimethyl-9-(2, 6, 6-trimethyl cyclohexene)-2, 4, 6, 8-alltrans nona tetraenoic acid, 4-methyl-2-oxo-pentanoic acid sodium salt to add in reactor 1 stirring and dissolving at 40-50 DEG C, by 1, 2, 3, 6-tetrahydrochysene-2, 6-dioxo pyrimidine-4-carboxylic acid potassium salt, methylpentanolone, 4-urocanic acid stirring and dissolving at 50-60 DEG C in reactor 2, mixture in reactor 2 is joined gradually in reactor 1, fully 15-25 minute is stirred in 45 DEG C of waters bath with thermostatic control, leave standstill 1-2 hour, namely the skin lotion vial sanitising agent of this comparative example is obtained.
Comparative example 2
Weigh: water 75kg, 3,5-di-t-butyl-4-hydroxy-benzyl alcohol 27kg, 3,7-dimethyl-9-(2,6,6-trimethyl cyclohexene)-2,4,6,8-alltrans nona tetraenoic acid 18kg, 4-methyl-2-oxo-pentanoic acid sodium salt 17kg, 2-methyl-2-propyl-1,3-PD diurethanes 12kg, methylpentanolone 8kg, 4-urocanic acid 5kg.
The preparation method of this comparative example skin lotion vial sanitising agent: by deionized water, 3, 5-di-t-butyl-4-hydroxy-benzyl alcohol, 3, 7-dimethyl-9-(2, 6, 6-trimethyl cyclohexene)-2, 4, 6, 8-alltrans nona tetraenoic acid, 4-methyl-2-oxo-pentanoic acid sodium salt to add in reactor 1 stirring and dissolving at 40-50 DEG C, by 2-methyl-2-propyl-1, ammediol diurethanes, methylpentanolone, 4-urocanic acid stirring and dissolving at 50-60 DEG C in reactor 2, mixture in reactor 2 is joined gradually in reactor 1, fully 15-25 minute is stirred in 45 DEG C of waters bath with thermostatic control, leave standstill 1-2 hour, namely the skin lotion vial sanitising agent of this comparative example is obtained.
(1), detergency test is carried out with embodiment 1-3 and comparative example 1-2 gained finished product
1) preparation of artificial dirt
Mixing oil is filled a prescription: configure for 0.5:1:0.5:1 with butter, lard, vegetables oil, polymeric impurities mass ratio, and add the glyceryl monostearate of its total mass 5%, this is artificial dirt.
Artificial dirt is put on electric furnace and be heated to 300 DEG C, stir and keep this temperature 15min, beaker is moved to magnetic stirrer, naturally cools to temperature required for subsequent use.To defile temperature reference: when room temperature is 20 DEG C, need oil temperature 80 DEG C; When room temperature is 25 DEG C, need oil temperature 45 DEG C; When room temperature is lower than 17 DEG C or higher than 27 DEG C, test should not be carried out, and needs to carry out under the environment of proper temperature.The Terg-O-Tometer of attached freezing plant should be used if desired.
2) defile
The skin lotion vial of cleaning is one group with five put on weighing frame, is accurately weighed as W0 with balance, the skin lotion vial after weighing is placed on rack one by one.
When greasy dirt remains in stable temperature, one by one skin lotion vial is got on to take off from rack, all immerse in greasy dirt and keep 2-3s, slowly take out, after lower of greasy dirt slows, put back to original rack, prepare dirty skin lotion vial successively.After the greasy dirt of skin lotion vial inside and outside wall solidifies, skin lotion vial is taken off and with filter paper or absorbent cotton, corner or the unnecessary greasy dirt of side is wiped.After left at room temperature 4h, weighing frame is W1 with balance accurate weighing.
3) testing sequence
The skin lotion vial of known greasy dirt amount is inserted in corresponding wash stand and prepare washing.
Switched on power by spotter, wash temperature is set to 32 DEG C, and velocity of rotation is set to 150r/min, and washing time is set to 5min.
Take 5.0g sample to be tested in 2500ml hard water, after shaking up, measure 800ml test solution respectively in five washing becks of Terg-O-Tometer, when test solution temperature rises to 32 DEG C, rapidly the skin lotion vial of known weight is put into washing beck accordingly together with wash stand, start to count soak time after washing beck put into by last skin lotion vial, simultaneously rapid agitator to be installed, when soaking 1min, start spotter, start washing, during 5min, machine auto stop, rapidly agitator is taken off, take out wash stand, rear skin lotion vial will be washed be placed in one by one on rack, after leaving standstill 3h, skin lotion vial is placed on corresponding weighing frame and weighs as W2.
Test result is as shown in the table:
Soil removal efficiency=[(W1-W2)/(W1-W0)] * 100%
| ? | Soil removal efficiency, % |
| Embodiment 1 | 99.2 |
| Embodiment 2 | 98.6 |
| Embodiment 3 | 98.9 |
| Comparative example 1 | 77.8 |
| Comparative example 2 | 56.3 |
(2), pungency test is carried out with embodiment 1-3 and comparative example 1-2 gained finished product
Simulation irritant experiment carries out in laboratory, and experimenter (each 5 people of men and women) is clean in the aqueous detergent solution of 1wt%, and water temperature 23-27 DEG C, water used is deionized water, washs 2 every day, each 3 hours, continuous 1 week.Average after marking according to the standard of following table for the pungency of wrist-watch skin, mark higher, pungency is less again.
| Judge project | Completely unchanged | Flat epidermis has wrinkle | Micro-erythema | Obvious erythema | Edema | Crowfoot cracks |
| Scoring | 100 | 80 | 60 | 40 | 20 | 0 |
Pungency test data table
| ? | Scoring |
| Embodiment 1 | 100 |
| Embodiment 2 | 100 |
| Embodiment 3 | 100 |
| Comparative example 1 | 60 |
| Comparative example 2 | 20 |
Claims (1)
1. skin lotion vial sanitising agent, it is characterized in that being prepared from by the raw material of following weight: 75 parts, water, 2-methyl-5-oxo ring penta-1-enol propionic ester 22-24 part, 3, 5-di-t-butyl-4-hydroxy-benzyl alcohol 26-28 part, 3, 7-dimethyl-9-(2, 6, 6-trimethyl cyclohexene)-2, 4, 6, 8-alltrans nona tetraenoic acid 16-18 part, 4-methyl-2-oxo-pentanoic acid sodium salt 16-18 part, 2-methyl-2-propyl-1, ammediol diurethanes 12-15 part, 1, 2, 3, 6-tetrahydrochysene-2, 6-dioxo pyrimidine-4-carboxylic acid potassium salt 10-12 part, methylpentanolone 6-8 part, 4-urocanic acid 4-6 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410462165.0A CN104263550A (en) | 2014-09-11 | 2014-09-11 | Makeup solution glass bottle detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410462165.0A CN104263550A (en) | 2014-09-11 | 2014-09-11 | Makeup solution glass bottle detergent |
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| Publication Number | Publication Date |
|---|---|
| CN104263550A true CN104263550A (en) | 2015-01-07 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410462165.0A Pending CN104263550A (en) | 2014-09-11 | 2014-09-11 | Makeup solution glass bottle detergent |
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| Country | Link |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252990A (en) * | 1998-10-13 | 2000-05-17 | 强生消费者公司 | Vitamin A stable cleaning composition |
| CN101605538A (en) * | 2006-10-17 | 2009-12-16 | 雷内笛卡尔巴黎第五大学 | Citrulline is used for the treatment of the purposes of undernutrition conditions |
| CN103540429A (en) * | 2012-07-11 | 2014-01-29 | 上海和黄白猫有限公司 | Hand-protecting and nail-protecting liquid detergent |
-
2014
- 2014-09-11 CN CN201410462165.0A patent/CN104263550A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252990A (en) * | 1998-10-13 | 2000-05-17 | 强生消费者公司 | Vitamin A stable cleaning composition |
| CN101605538A (en) * | 2006-10-17 | 2009-12-16 | 雷内笛卡尔巴黎第五大学 | Citrulline is used for the treatment of the purposes of undernutrition conditions |
| CN103540429A (en) * | 2012-07-11 | 2014-01-29 | 上海和黄白猫有限公司 | Hand-protecting and nail-protecting liquid detergent |
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Application publication date: 20150107 |