CN104230267A - Thermal-insulation moisture-proof floor tile and preparation method thereof - Google Patents

Thermal-insulation moisture-proof floor tile and preparation method thereof Download PDF

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Publication number
CN104230267A
CN104230267A CN201410455192.5A CN201410455192A CN104230267A CN 104230267 A CN104230267 A CN 104230267A CN 201410455192 A CN201410455192 A CN 201410455192A CN 104230267 A CN104230267 A CN 104230267A
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floor tile
heat
thermal
raw material
insulation
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CN104230267B (en
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陈剑
钟安祯
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Puding Yinfeng Agricultural Science & Technology Development Co Ltd
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Puding Yinfeng Agricultural Science & Technology Development Co Ltd
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Abstract

The invention relates to the technical field of building floor tiles and particularly relates to a thermal-insulation moisture-proof floor tile and a preparation method thereof. The preparation method of the thermal-insulation moisture-proof floor tile comprises the following steps: combining and matching raw materials such as white cement, quartz sand, cellulose, ceramic powder, glass particles, natural color sand, iron oxide and copper oxide; and combining a raw material treating step, a raw material mixing step, a cast pouring step, a punch forming step and a maintaining step in a preparation process to prepare the thermal-insulation moisture-proof floor tile. According to the preparation method, the durable performances of the prepared thermal-insulation moisture-proof floor tile are improved to a great extent, the preparation process is simple and the preparation cost is low; and moreover, compared with the conventional thermal-insulation building material, the thermal-insulation moisture-proof floor tile has the advantages that the thermal insulation effect of the thermal-insulation moisture-proof floor tile is improved by over 50%, the thermal-insulation time of the thermal-insulation moisture-proof floor tile is prolonged by 5-6 times in comparison with that of the conventional thermal-insulation moisture-proof floor tile, and the thermal-insulation effects of the thermal-insulation moisture-proof floor tile are greatly strengthened. Meanwhile, the moisture-proof effects of the thermal-insulation moisture-proof floor tile are improved to a great extent.

Description

A kind of heat-holding dampproof floor tile and preparation method thereof
Technical field
The present invention relates to floor tile technical field for building, especially a kind of heat-holding dampproof floor tile and preparation method thereof.
Background technology
Floor tile, obtain on the decoration of bottom surface at present and apply largely, its main purpose solves the coarse technical problem in bottom surface, simultaneously, also conveniently in people's life process, reduce dust, improve the quality of living environment, certainly also play certain insulation, sound insulation, moistureproof effect, and it is also more to the research of floor tile in the prior art, mainly to the pattern of floor tile, the durable of floor tile, the shape of floor tile and smooth finish make research, and then improve the quality of indoor environment; Certainly also have certain research for technical problems such as protection against the tide, insulation, sound insulations, but the effect of its research is comparatively undesirable.
For this reason, this researchist is by long-term research and discovery, and guaranteeing that floor tile is durable, pattern is beautiful, smooth finish is preferably under prerequisite, and study the insulation of floor tile, protection against the tide, sound insulation technology, the processing for floor tile provides a kind of new approaches.
Summary of the invention
In order to solve the above-mentioned technical problem existed in prior art, the invention provides a kind of heat-holding dampproof floor tile, have durable easy-to-use, learn in its cavity be made in hexahedron by test, pouring air themperature is after 50 DEG C, it is after 10-13h, it is being detected, 43-44.63 DEG C can also be reached, and after traditional floor tile carries out being made into same hexahedron cavity, pour the air of 50 DEG C, after 2-4h, its temperature is maintained normal temperature, visible, the heat insulation effect of this heat-holding dampproof floor tile is better, and there is good moisture effect, compared with traditional floor tile, its humidity resistance exceeds the feature of more than 50%.
Meanwhile, the present invention also provides a kind of preparation method of heat-holding dampproof floor tile.
Be achieved particular by following technical scheme:
A kind of heat-holding dampproof floor tile, its raw material composition comprises white cement 8-11 part, quartz sand 6-7 part, Mierocrystalline cellulose 3-7 part, ceramics powder 4-6 part, glass particle 3-5 part, natural colour sand 6-9 part, ferric oxide 1-3 part, cupric oxide 0.5-1.5 part.
Described raw material composition comprises white cement 10 parts, quartz sand 7 parts, Mierocrystalline cellulose 5 parts, ceramics powder 5 parts, glass particle 4 parts, natural colour sand 7 parts, ferric oxide 2 parts, cupric oxide 1 part.
Described Mierocrystalline cellulose is Walocel MT 20.000PV.
Described quartz sand is 130-170 order.
Described ceramics powder is 110-130 order.
Described glass particle is 120-140 order.
Described natural colour sand is 130-150 order.
Described ferric oxide is molten state.
Described cupric oxide is molten state.
The preparation method of this heat-holding dampproof floor tile, comprises the following steps:
(1) raw material prepares: after quartz sand powder being broken to 130-170 order, after adopting the clarification liming immersion treatment 30-70min of quartz sand gross weight 1-2%, be placed on again in baking box, heat-up rate is adopted to be after 10-13 DEG C/min is warming up to 60 DEG C, isothermal holding 1h, after again it being cooled to normal temperature in 20-60s, stand-by; After ceramics powder being crushed to 110-130 order, then to be placed on concentration be 1-3% weight is after ceramics powder 1-3 salt solution doubly soaks 40-50min, after stirring 10min, stand-by; After glass particle being crushed to 120-140 order, then to be placed on temperature be in 100-180 DEG C, and after heat treatment 1-4h, constant temperature is stand-by; After natural colour sand being crushed to 130-150 order, then to be placed in temperature be that after 200-270 DEG C of heat treated 1-2h, constant temperature is stand-by; Ferric oxide is placed in smelting furnace, is smelted into molten state stand-by; Cupric oxide is placed in smelting furnace, is smelted into molten state stand-by.
(2) raw material mixing: according to said ratio part, by step 1) get out stand-by raw material, according to quartz sand, ceramics powder, glass particle, natural colour sand, ferric oxide, the order of cupric oxide is add mixing successively in 180-200 DEG C in envrionment temperature, and employing stirring speed is 180-230r/min stir process, after process 1-3h to be mixed, add Mierocrystalline cellulose wherein again, and reduce temperature to 80-100 DEG C, the stirring velocity of adjustment stirrer is 90-100r/min, after stir process 30-50min, add cement wherein again, and reduce temperature to 50-70 DEG C, adjustment stirring velocity is 300-500r/min, after stir process 3-4h, stand-by,
(3) mould is filled with: by step 2) raw material that mix is filling in ground brick shaping mould, and filling thickness is 10-15cm, and sprays the admixture combined by rosin 18kg, peregal 4kg of raw material gross weight 1-3%, standing 1-3h, stand-by;
(4) impact briquetting: by step 3) to fill with the raw material that completes of mould and adopt pneumatic press impact briquetting, the pressure of punching press is 4.51-5.13MPa, and the thickness after punching press completes is 4-6cm, can obtain heat-holding dampproof floor tile just finished product.
(5) maintenance: by step 4) the heat-holding dampproof floor tile that obtains just finished product be placed in physical environment, according to sprinkling water every day 2 times, carrying out natural curing 12-30 days, the moistureproof floor tile of finished product thermal insulation can be obtained.
Compared with prior art, technique effect of the present invention is embodied in:
1. white cement is passed through, quartz sand, Mierocrystalline cellulose, ceramics powder, glass particle, natural colour sand, ferric oxide, the combination of the raw materials such as cupric oxide and collocation, and in conjunction with in preparation technology, Feedstock treating, raw material mixes, fill with mould, impact briquetting and curing step, the durability of the heat-holding dampproof floor tile made is improved largely, its manufacture craft is simple, cost of manufacture is cheap, and obtain heat-holding dampproof floor tile relative to traditional heat-insulating construction material, its heat insulation effect improves more than 50%, insulation time expand is traditional 5-6 times, greatly strengthen the heat insulation effect of floor tile, simultaneously, its moisture effect is also improved largely.
2. by preparation method, Feedstock treating step processes raw material, the performance of various raw material is improved largely, ensure that the improvement of the performance of the heat-holding dampproof floor tile made, and in conjunction with in raw material mixing step, to control and the adjustment of the order that raw material adds, further ensure that the micro-variations occurred between brother's raw material is controlled, make the heat-holding dampproof successful of the heat-holding dampproof floor tile prepared.
Embodiment
Below in conjunction with concrete embodiment, further restriction is done to technical scheme of the present invention, but claimed scope is not only confined to done description.
Embodiment 1
A kind of heat-holding dampproof floor tile, its raw material composition comprises white cement 8kg, quartz sand 6kg, Mierocrystalline cellulose 3kg, ceramics powder 4kg, glass particle 3kg, natural colour sand 6kg, ferric oxide 1kg, cupric oxide 0.5kg.
Described Mierocrystalline cellulose is Walocel MT 20.000PV.
Described quartz sand is 130 orders.
Described ceramics powder is 110 orders.
Described glass particle is 120 orders.
Described natural colour sand is 130 orders.
Described ferric oxide is molten state.
Described cupric oxide is molten state.
The preparation method of this heat-holding dampproof floor tile, comprises the following steps:
(1) raw material prepares: after quartz sand powder being broken to 130 orders, after adopting the clarification liming immersion treatment 30min of quartz sand gross weight 1%, be placed on again in baking box, heat-up rate is adopted to be after 10 DEG C/min is warming up to 60 DEG C, isothermal holding 1h, after again it being cooled to normal temperature in 20s, stand-by; After ceramics powder being crushed to 110 orders, then to be placed on concentration be 1% weight is after the salt solution of ceramics powder 1 times soaks 40min, after stirring 10min, stand-by; After glass particle being crushed to 120 orders, then to be placed on temperature be in 100 DEG C, and after heat treatment 1h, constant temperature is stand-by; After natural colour sand being crushed to 130 orders, then to be placed in temperature be that after 200 DEG C of heat treated 1h, constant temperature is stand-by; Ferric oxide is placed in smelting furnace, is smelted into molten state stand-by; Cupric oxide is placed in smelting furnace, is smelted into molten state stand-by.
(2) raw material mixing: according to said ratio part, by step 1) get out stand-by raw material, according to quartz sand, ceramics powder, glass particle, natural colour sand, ferric oxide, the order of cupric oxide is add mixing successively in 180 DEG C in envrionment temperature, and employing stirring speed is 180r/min stir process, after process 1h to be mixed, add Mierocrystalline cellulose wherein again, and reduce temperature to 80 DEG C, the stirring velocity of adjustment stirrer is 90r/min, after stir process 30min, add cement wherein again, and reduce temperature to 50 DEG C, adjustment stirring velocity is 300r/min, after stir process 3h, stand-by,
(3) mould is filled with: by step 2) raw material that mix is filling in ground brick shaping mould, and filling thickness is 10cm, and sprays the admixture combined by rosin 18kg, peregal 4kg of raw material gross weight 1%, standing 1h, stand-by;
(4) impact briquetting: by step 3) to fill with the raw material that completes of mould and adopt pneumatic press impact briquetting, the pressure of punching press is 4.51MPa, and the thickness after punching press completes is 4cm, can obtain heat-holding dampproof floor tile just finished product.
(5) maintenance: by step 4) the heat-holding dampproof floor tile that obtains just finished product be placed in physical environment, according to sprinkling water every day 2 times, carrying out natural curing 12 days, the moistureproof floor tile of finished product thermal insulation can be obtained.
Embodiment 2
On the basis of embodiment 1, a kind of heat-holding dampproof floor tile, its raw material composition comprises white cement 11kg, quartz sand 7kg, Mierocrystalline cellulose 7kg, ceramics powder 6kg, glass particle 5kg, natural colour sand 9kg, ferric oxide 3kg, cupric oxide 1.5kg.
Described quartz sand is 170 orders.
Described ceramics powder is 130 orders.
Described glass particle is 140 orders.
Described natural colour sand is 150 orders.
The preparation method of this heat-holding dampproof floor tile, comprises the following steps:
(1) raw material prepares: after quartz sand powder being broken to 170 orders, after adopting the clarification liming immersion treatment 70min of quartz sand gross weight 2%, be placed on again in baking box, heat-up rate is adopted to be after 13 DEG C/min is warming up to 60 DEG C, isothermal holding 1h, after again it being cooled to normal temperature in 60s, stand-by; After ceramics powder being crushed to 130 orders, then to be placed on concentration be 3% weight is after the salt solution of ceramics powder 3 times soaks 50min, after stirring 10min, stand-by; After glass particle being crushed to 140 orders, then to be placed on temperature be in 180 DEG C, and after heat treatment 4h, constant temperature is stand-by; After natural colour sand being crushed to 150 orders, then to be placed in temperature be that after 270 DEG C of heat treated 2h, constant temperature is stand-by; Ferric oxide is placed in smelting furnace, is smelted into molten state stand-by; Cupric oxide is placed in smelting furnace, is smelted into molten state stand-by.
(2) raw material mixing: according to said ratio part, by step 1) get out stand-by raw material, according to quartz sand, ceramics powder, glass particle, natural colour sand, ferric oxide, the order of cupric oxide is add mixing successively in 200 DEG C in envrionment temperature, and employing stirring speed is 230r/min stir process, after process 3h to be mixed, add Mierocrystalline cellulose wherein again, and reduce temperature to 100 DEG C, the stirring velocity of adjustment stirrer is 100r/min, after stir process 50min, add cement wherein again, and reduce temperature to 70 DEG C, adjustment stirring velocity is 500r/min, after stir process 4h, stand-by,
(3) mould is filled with: by step 2) raw material that mix is filling in ground brick shaping mould, and filling thickness is 15cm, and sprays the admixture combined by rosin 18kg, peregal 4kg of raw material gross weight 3%, standing 3h, stand-by;
(4) impact briquetting: by step 3) to fill with the raw material that completes of mould and adopt pneumatic press impact briquetting, the pressure of punching press is 5.13MPa, and the thickness after punching press completes is 6cm, can obtain heat-holding dampproof floor tile just finished product.
(5) maintenance: by step 4) the heat-holding dampproof floor tile that obtains just finished product be placed in physical environment, according to sprinkling water every day 2 times, carrying out natural curing 30 days, the moistureproof floor tile of finished product thermal insulation can be obtained.
Embodiment 3
On the basis of embodiment 1, a kind of heat-holding dampproof floor tile, its raw material composition comprises white cement 10kg, quartz sand 7kg, Mierocrystalline cellulose 5kg, ceramics powder 5kg, glass particle 4kg, natural colour sand 7kg, ferric oxide 2kg, cupric oxide 1kg.
Described quartz sand is 140 orders.
Described ceramics powder is 120 orders.
Described glass particle is 130 orders.
Described natural colour sand is 140 orders.
The preparation method of this heat-holding dampproof floor tile, comprises the following steps:
(1) raw material prepares: after quartz sand powder being broken to 140 orders, after adopting the clarification liming immersion treatment 55min of quartz sand gross weight 1.5%, be placed on again in baking box, heat-up rate is adopted to be after 11 DEG C/min is warming up to 60 DEG C, isothermal holding 1h, after again it being cooled to normal temperature in 50s, stand-by; After ceramics powder being crushed to 120 orders, then to be placed on concentration be 2% weight is after the salt solution of ceramics powder 2 times soaks 45min, after stirring 10min, stand-by; After glass particle being crushed to 130 orders, then to be placed on temperature be in 160 DEG C, and after heat treatment 3h, constant temperature is stand-by; After natural colour sand being crushed to 140 orders, then to be placed in temperature be that after 230 DEG C of heat treated 1.5h, constant temperature is stand-by; Ferric oxide is placed in smelting furnace, is smelted into molten state stand-by; Cupric oxide is placed in smelting furnace, is smelted into molten state stand-by.
(2) raw material mixing: according to said ratio part, by step 1) get out stand-by raw material, according to quartz sand, ceramics powder, glass particle, natural colour sand, ferric oxide, the order of cupric oxide is add mixing successively in 190 DEG C in envrionment temperature, and employing stirring speed is 210r/min stir process, after process 2h to be mixed, add Mierocrystalline cellulose wherein again, and reduce temperature to 90 DEG C, the stirring velocity of adjustment stirrer is 95r/min, after stir process 40min, add cement wherein again, and reduce temperature to 60 DEG C, adjustment stirring velocity is 400r/min, after stir process 3.5h, stand-by,
(3) mould is filled with: by step 2) raw material that mix is filling in ground brick shaping mould, and filling thickness is 11cm, and sprays the admixture combined by rosin 18kg, peregal 4kg of raw material gross weight 2%, standing 2h, stand-by;
(4) impact briquetting: by step 3) to fill with the raw material that completes of mould and adopt pneumatic press impact briquetting, the pressure of punching press is 4.97MPa, and the thickness after punching press completes is 5cm, can obtain heat-holding dampproof floor tile just finished product.
(5) maintenance: by step 4) the heat-holding dampproof floor tile that obtains just finished product be placed in physical environment, according to sprinkling water every day 2 times, carrying out natural curing 18 days, the moistureproof floor tile of finished product thermal insulation can be obtained.
It is important to point out at this; above embodiment is only limitted to understanding of the present invention and elaboration; be not limitation of the present invention, the non-protruding essential characteristics that those skilled in the art make on this basis and the improvement of non-significant progress, all belong to protection category of the present invention.

Claims (10)

1. a heat-holding dampproof floor tile, is characterized in that, its raw material composition comprises white cement 8-11 part, quartz sand 6-7 part, Mierocrystalline cellulose 3-7 part, ceramics powder 4-6 part, glass particle 3-5 part, natural colour sand 6-9 part, ferric oxide 1-3 part, cupric oxide 0.5-1.5 part.
2. heat-holding dampproof floor tile as claimed in claim 1, it is characterized in that, described raw material composition comprises white cement 10 parts, quartz sand 7 parts, Mierocrystalline cellulose 5 parts, ceramics powder 5 parts, glass particle 4 parts, natural colour sand 7 parts, ferric oxide 2 parts, cupric oxide 1 part.
3. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described Mierocrystalline cellulose is Walocel MT 20.000PV.
4. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described quartz sand is 130-170 order.
5. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described ceramics powder is 110-130 order.
6. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described glass particle is 120-140 order.
7. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described natural colour sand is 130-150 order.
8. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described ferric oxide is molten state.
9. heat-holding dampproof floor tile as claimed in claim 1 or 2, it is characterized in that, described cupric oxide is molten state.
10. the preparation method of the heat-holding dampproof floor tile as described in any one of claim 1-9, is characterized in that, comprise the following steps:
(1) raw material prepares: after quartz sand powder being broken to 130-170 order, after adopting the clarification liming immersion treatment 30-70min of quartz sand gross weight 1-2%, be placed on again in baking box, heat-up rate is adopted to be after 10-13 DEG C/min is warming up to 60 DEG C, isothermal holding 1h, after again it being cooled to normal temperature in 20-60s, stand-by; After ceramics powder being crushed to 110-130 order, then to be placed on concentration be 1-3% weight is after ceramics powder 1-3 salt solution doubly soaks 40-50min, after stirring 10min, stand-by; After glass particle being crushed to 120-140 order, then to be placed on temperature be in 100-180 DEG C, and after heat treatment 1-4h, constant temperature is stand-by; After natural colour sand being crushed to 130-150 order, then to be placed in temperature be that after 200-270 DEG C of heat treated 1-2h, constant temperature is stand-by; Ferric oxide is placed in smelting furnace, is smelted into molten state stand-by; Cupric oxide is placed in smelting furnace, is smelted into molten state stand-by.
(2) raw material mixing: according to said ratio part, by step 1) get out stand-by raw material, according to quartz sand, ceramics powder, glass particle, natural colour sand, ferric oxide, the order of cupric oxide is add mixing successively in 180-200 DEG C in envrionment temperature, and employing stirring speed is 180-230r/min stir process, after process 1-3h to be mixed, add Mierocrystalline cellulose wherein again, and reduce temperature to 80-100 DEG C, the stirring velocity of adjustment stirrer is 90-100r/min, after stir process 30-50min, add cement wherein again, and reduce temperature to 50-70 DEG C, adjustment stirring velocity is 300-500r/min, after stir process 3-4h, stand-by,
(3) mould is filled with: by step 2) raw material that mix is filling in ground brick shaping mould, and filling thickness is 10-15cm, and sprays the admixture combined by rosin 18kg, peregal 4kg of raw material gross weight 1-3%, standing 1-3h, stand-by;
(4) impact briquetting: by step 3) to fill with the raw material that completes of mould and adopt pneumatic press impact briquetting, the pressure of punching press is 4.51-5.13MPa, and the thickness after punching press completes is 4-6cm, can obtain heat-holding dampproof floor tile just finished product.
(5) maintenance: by step 4) the heat-holding dampproof floor tile that obtains just finished product be placed in physical environment, according to sprinkling water every day 2 times, carrying out natural curing 12-30 days, the moistureproof floor tile of finished product thermal insulation can be obtained.
CN201410455192.5A 2014-09-09 2014-09-09 A kind of heat-holding dampproof floor tile and preparation method thereof Expired - Fee Related CN104230267B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104761240B (en) * 2015-04-01 2016-08-24 程林 A kind of preparation method of moistureproof floor tile
CN110066648A (en) * 2018-01-23 2019-07-30 中石化石油工程技术服务有限公司 A kind of anti-strength retrogression oil well cement additive and methods for making and using same

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Publication number Priority date Publication date Assignee Title
CN101298378A (en) * 2008-04-11 2008-11-05 北京迪百斯特科技发展有限公司 Flexible ceramic-like tile and production process thereof
CN102417341A (en) * 2011-07-22 2012-04-18 广州市建筑科学研究院有限公司 Novel unfired inorganic ceramic tile and preparation method thereof
CN102875186A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Fluorite slag aerated brick and preparation method thereof
CN103011717A (en) * 2012-10-28 2013-04-03 赵延波 Building section bar

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101298378A (en) * 2008-04-11 2008-11-05 北京迪百斯特科技发展有限公司 Flexible ceramic-like tile and production process thereof
CN102417341A (en) * 2011-07-22 2012-04-18 广州市建筑科学研究院有限公司 Novel unfired inorganic ceramic tile and preparation method thereof
CN102875186A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Fluorite slag aerated brick and preparation method thereof
CN103011717A (en) * 2012-10-28 2013-04-03 赵延波 Building section bar

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104761240B (en) * 2015-04-01 2016-08-24 程林 A kind of preparation method of moistureproof floor tile
CN110066648A (en) * 2018-01-23 2019-07-30 中石化石油工程技术服务有限公司 A kind of anti-strength retrogression oil well cement additive and methods for making and using same

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