CN104211481A - Compound fertilizer containing tigogenin extracted residue - Google Patents

Compound fertilizer containing tigogenin extracted residue Download PDF

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Publication number
CN104211481A
CN104211481A CN201410490033.9A CN201410490033A CN104211481A CN 104211481 A CN104211481 A CN 104211481A CN 201410490033 A CN201410490033 A CN 201410490033A CN 104211481 A CN104211481 A CN 104211481A
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Prior art keywords
tigogenin
waste residue
fertilizer
extracts
dry
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CN201410490033.9A
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CN104211481B (en
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覃佑康
李华锋
秦高雄
廖青
黄尚顺
王俊
宋燕芳
覃国炼
黄转香
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GUANGXI ZHONGYI BIOLOGICAL SCIENCE & TECHNOLOGY Co Ltd
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GUANGXI ZHONGYI BIOLOGICAL SCIENCE & TECHNOLOGY Co Ltd
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Abstract

The invention discloses a compound fertilizer containing tigogenin extracted residue. The fertilizer is prepared by mixing an inorganic fertilizer and an organic fertilizer and is composed of the following raw materials by weight: 200-700 parts of tigogenin extracted residue, 100-300 parts of monoammonium phosphate, 80-150 parts of potassium chloride and 80-120 parts of urea. The compound fertilizer solves the problem of pollution caused by the existing tigogenin production, and comprehensively utilizes the residue generated after extraction of the tigogenin as the organic raw material. Compared with the existing compound fertilizer, the compound fertilizer has a synergistic interaction effect, turns waste into wealth, and is favorable for industrial production and popularization.

Description

A kind of composite fertilizer that contains tigogenin extraction waste residue
Technical field
The present invention relates to Chemical Mixed Fertilizer field, relate in particular to a kind of composite fertilizer that tigogenin extracts waste residue that contains.
Background technology
Tigogenin production technique comparative maturity, but the processing of the waste residue producing in production process is but a troubling problem.Existing is to adopt the land-fill method of digging pit to process to the processing of waste residue substantially, and this mode pollutes soil, and resource can not be fully used, and has caused waste.
Tigogenin extraction waste residue is that the fermented product fiber crops cream of sisal hemp fiber crops water obtains through acidolysis, can be considered a kind of plant and makes compost.Saponin, after organic solvent lixiviate, still contains the organic matters such as a large amount of starch, sugar, wax in waste residue, organic content reaches 32%~40%, can be used as natural organic fertilizer and uses.Organic-inorganic complex fertilizer is to process by fermentation with organic materialss such as feces of livestock and poultry, plant and animal residues, processing of farm products tankage, adds mineral manure and makes.It is sisal hemp plant fermentation thing that tigogenin extracts waste residue, as the organic composition of organic-inorganic complex fertilizer, is feasible.
Summary of the invention
The object of the present invention is to provide a kind of composite fertilizer that tigogenin extracts waste residue that contains, the invention solves existing tigogenin and produce the pollution problem existing, the waste residue producing after comprehensive utilization tigogenin extracts is as organic matter material, this fertilizer is with respect to existing composite fertilizer, there is synergistic function, turn waste into wealth, be beneficial to suitability for industrialized production and popularization.
For achieving the above object, technical scheme of the present invention is as follows:
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 200-700 weight part extracts waste residue, the monoammonium phosphate of 100-300 weight part, the urea of the Repone K of 80-150 weight part, 80-120 weight part.
The compound L-glutamic acid that also comprises 150-400 weight part.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 10-15 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Advantage of the present invention is:
The invention provides a kind of novel organic-inorganic compound mixed fertilizer, in this fertilizer, utilized tigogenin to extract this traditional polluting waste of waste residue, coordinate mineral manure, form whole fertilizer formula, by tigogenin, extract coordinating of waste residue and common mineral manure, not only solve the direct as fertilizer sources of tigogenin extraction waste residue and used the injury to soil and plant, and by this cooperation, produced the synergism of fertilizer, contriver finds through test, based on the organic-inorganic compound mixed fertilizer that extracts waste residue containing tigogenin of the present invention in actual using, fertilising efficiency than conventional composite fertilizer is in the market higher, fertility is stronger, promoter action to plant-growth is larger.As the experimental verification in the embodiment of the present invention shows, take sugarcane as example, its stem is high, stem footpath, single stem heavy and number of productive tiller is all better than the result that other fertilizer are processed.
The Chemical Mixed Fertilizer that contains tigogenin extraction waste residue of the present invention, its organic matter material using extracts waste residue for tigogenin, organic content is high, its use had both solved the waste residue difficult treatment occurring in production of saponin and the environmental problem causing, rationally utilized again this waste residue as organic matter material, produce new value, turned waste into wealth, increased economic benefit.The present invention can be generalized to all tigogenin producers, can be used as industry and processes standard or the forerunner that tigogenin extracts waste residue.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 200 weight parts extracts waste residue, the monoammonium phosphate of 100 weight parts, the urea of the Repone K of 80 weight parts, 80 weight parts.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 10 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Embodiment 2
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 300 weight parts extracts waste residue, the monoammonium phosphate of 150 weight parts, the urea of the Repone K of 90 weight parts, 90 weight parts.
The compound L-glutamic acid that also comprises 150 weight parts.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 11 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Embodiment 3
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 400 weight parts extracts waste residue, the monoammonium phosphate of 200 weight parts, the urea of the Repone K of 100 weight parts, 100 weight parts.
The compound L-glutamic acid that also comprises 200 weight parts.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 12 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Embodiment 4
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 500 weight parts extracts waste residue, the monoammonium phosphate of 250 weight parts, the urea of the Repone K of 110 weight parts, 110 weight parts.
The compound L-glutamic acid that also comprises 250 weight parts.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 13 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Embodiment 5
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 600 weight parts extracts waste residue, the monoammonium phosphate of 300 weight parts, the urea of the Repone K of 130 weight parts, 120 weight parts.
The compound L-glutamic acid that also comprises 300 weight parts.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 14 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Embodiment 6
The composite fertilizer that contains tigogenin extraction waste residue of the present invention, by mineral manure and organic fertilizer, mix and make, by comprising that following raw material forms: the tigogenin of 700 weight parts extracts waste residue, the monoammonium phosphate of 300 weight parts, the urea of the Repone K of 150 weight parts, 120 weight parts.
The compound L-glutamic acid that also comprises 400 weight parts.
The described composite fertilizer that contains tigogenin extraction waste residue, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
The preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 15 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment; After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
Embodiment 7
Embodiment 1~6 formula and detected result are as shown in the table:
Table 1 compound fertilizer formula and detected result
Sugarcane field fertilizer efficiency
1, test site and time: San Ha village, Qu Li town, Fusui County, in February, 2013-2013 year December.
2, for examination fertilizer: patent of the present invention is produced organic-inorganic complex fertilizer (embodiment 3 and embodiment 5 formulas), commercially available 16% organic-inorganic complex fertilizer (organic matter: 15%, N:8%, P:12%, K:7%, Guangxi Chemical Inst. produces), commercially available 45% composite fertilizer (N:16%, P:7%, K:22%, Guangxi Chemical Inst. produces), conventional fertilizer: 46% urea, 18% fused(calcium magnesium)phosphate, 60% Repone K.
3, test design: establish 5 processing.Respectively to process A (organic-inorganic complex fertilizer that the embodiment of the present invention 3 formulas are produced), treatments B (organic-inorganic complex fertilizer that the embodiment of the present invention 5 formulas are produced), process C (16% organic-inorganic complex fertilizer), process D (45% composite fertilizer), process E (conventional fertilizer application).Adopt plot experiment, experimental plot line-spacing 1m, the long 20m of every row, every community 10 row, each community area 200m 2, test total area 1000m 2.Every mu of (667m 2) amount of sowing 7000 buds.
4, fertilizing method: process A, treatments B, processing C and process D: base manure 20kg/ mu, tillering phase, 35Kg/ mu, extended jointing stage 50Kg/ mu; Process E: base manure: urea 10Kg/ mu, fused(calcium magnesium)phosphate 100Kg/ mu, Repone K 10Kg/ mu; Tillering phase: urea 15Kg/ mu, Repone K 10Kg/ mu; Extend the jointing stage: urea 25Kg/ mu.
5, sugarcane Agronomic
The sugarcane Agronomic of table 2 different fertilization
As can be seen from Table 2, the cane stalk of processing A and treatments B is high, stem footpath, single stem is heavy and number of productive tiller is all better than other fertilizer and processes, and shows that tigogenin that the present invention produces extracts waste residue organic-inorganic complex fertilizer and have stronger advantage in Sugarcane Fertilization application.And tigogenin extracts waste residue and is waste material, cheap, greatly reduce the cost of organic raw material, economic benefits.

Claims (4)

1. one kind contains the composite fertilizer that tigogenin extracts waste residue, by mineral manure and organic fertilizer, mix and make, it is characterized in that by comprising that following raw material forms: the tigogenin of 200-700 weight part extracts waste residue, the monoammonium phosphate of 100-300 weight part, the urea of the Repone K of 80-150 weight part, 80-120 weight part.
2. the composite fertilizer that contains tigogenin extraction waste residue as claimed in claim 1, is characterized in that: the compound L-glutamic acid that also comprises 150-400 weight part.
3. the composite fertilizer that contains tigogenin extraction waste residue as claimed in claim 1, is characterized in that, its preparation method comprises the following steps:
A, that tigogenin is extracted to waste residue is dry, controls moisture in 10%, pulverizes standby;
B, monoammonium phosphate, Repone K are pulverized, are extracted waste residue powder mixing granulation with tigogenin, by spray granulating after urea melting, dry after and get final product.
4. as claim 1-3 contains the composite fertilizer that tigogenin extracts waste residue as described in any one, the preparation method that described tigogenin extracts waste residue comprises the following steps:
Take that to remove the sisal hemp crushed material of fiber be raw material, through squeezing, take out numb juice, numb juice spontaneous fermentation sedimentation, after 10-15 days, is got the dry sisal hemp fiber crops cream that to obtain of sediment;
After the hydrolysis of sisal hemp fiber crops cream, make hydrolyzate, after hydrolyzate extracts, the throw out of filtration is tigogenin and extracts waste residue.
CN201410490033.9A 2014-09-24 2014-09-24 Compound fertilizer containing tigogenin extracted residue Active CN104211481B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104620931A (en) * 2015-01-27 2015-05-20 广西华劲竹林发展有限公司 Method for preparing dendrocalamus minor light matrix through agave sisalana waste residues
CN105294338A (en) * 2015-10-30 2016-02-03 大新县生产力促进中心 Zenia insigins Chun. special fertilizer and production method thereof

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CN101684049A (en) * 2008-09-22 2010-03-31 新疆富沃药业有限公司 Method for preparing biological fertilizer and the biological fertilizer by the method
CN102174399A (en) * 2010-12-31 2011-09-07 广西赛尔纸业有限公司 Method for preparing herbal biological fiber and biological paper pulp
CN102320879A (en) * 2011-09-06 2012-01-18 李子先 High nutrient compound selenium fertilizer and preparation method thereof
CN103087143A (en) * 2013-01-09 2013-05-08 广西南剑生物科技有限公司 Method for extracting tigogenin from squeezed juice of sisal residue
CN104030818A (en) * 2014-06-16 2014-09-10 合肥江氏农业科技有限公司 Pocket-size mushroom cultivation medium and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101684049A (en) * 2008-09-22 2010-03-31 新疆富沃药业有限公司 Method for preparing biological fertilizer and the biological fertilizer by the method
CN101560240A (en) * 2009-05-18 2009-10-21 广西福园剑麻股份有限公司 Extracting method of ticogenin with high yield
CN102174399A (en) * 2010-12-31 2011-09-07 广西赛尔纸业有限公司 Method for preparing herbal biological fiber and biological paper pulp
CN102320879A (en) * 2011-09-06 2012-01-18 李子先 High nutrient compound selenium fertilizer and preparation method thereof
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CN104030818A (en) * 2014-06-16 2014-09-10 合肥江氏农业科技有限公司 Pocket-size mushroom cultivation medium and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104620931A (en) * 2015-01-27 2015-05-20 广西华劲竹林发展有限公司 Method for preparing dendrocalamus minor light matrix through agave sisalana waste residues
CN104620931B (en) * 2015-01-27 2017-05-31 广西华劲竹林发展有限公司 The method that hang spring bamboo Light media is prepared using sisal hemp waste residue
CN105294338A (en) * 2015-10-30 2016-02-03 大新县生产力促进中心 Zenia insigins Chun. special fertilizer and production method thereof

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