CN104151092B - A kind of production method of organic water soluble Liquid Fertilizer - Google Patents

A kind of production method of organic water soluble Liquid Fertilizer Download PDF

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Publication number
CN104151092B
CN104151092B CN201410403137.1A CN201410403137A CN104151092B CN 104151092 B CN104151092 B CN 104151092B CN 201410403137 A CN201410403137 A CN 201410403137A CN 104151092 B CN104151092 B CN 104151092B
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fertilizer
liquid
production method
water soluble
stock solution
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CN104151092A (en
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曾凡强
刘付东
梁敏锐
曾松清
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ZHONGSHAN CHENGMING AGRICULTURE TECHNOLOGY DEVELOPMENT CO., LTD.
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ZHONGSHAN BASIDE AGRICULTURAL SCIENCE AND TECHNOLOGY Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Abstract

The invention discloses the production method of a kind of organic water soluble Liquid Fertilizer, belong to agricultural liquid fertilizer technology field.After the method carries out anaerobic fermentation to fertilizer stock solution under the existence mixed yeast and lactic acid bacteria of biological filler material, add Bacillus licheniformis, and add arsenic determination, boron fertilizer, zinc fertilizer and molydbenum fertilizer, then aeration, liquid chitin is added, after stirring after carrying out aerobic fermentation.The present invention makes larger molecular organics acidolysis in anaerobic fermentation stage become small organic molecule, it is prone to chelate with other chemicals under good oxygen condition, promote the effect of each element, relatively other be simply mixed made by Liquid Fertilizer out, be greatly improved effect;Production technology of the present invention is simple, does not has operational complexity, and set multiple efficacies is, easy to use.

Description

A kind of production method of organic water soluble Liquid Fertilizer
[technical field]
The present invention relates to the production method of a kind of organic water soluble Liquid Fertilizer, belong to agricultural liquid fertile Technical field.
[background technology]
The straw water (blackstrap, pitchy) in sugar refinery, the yeast waste liquor (pitchy) of yeast factory Deng containing organic matter, humic acids, the soluble ingredient of nutrient, it is that one is kept under strict control refuse, how to go Process it, there has been the entrance in this respect of many units, the most typical system that turns waste into wealth exactly Be made for fertilizer or ethanol or other, and at fertilizer here, usage amount should be that tool is big, but Owing to manufacturing technology is low, causing product DeGrain, usage amount is the highest, finally Cause these raw materials still cannot turn waste into wealth and the environment that depollutes, the most unfortunately.
And the development of Liquid Fertilizer is quickly, it is processed into Liquid Fertilizer especially with garbage, such as " a kind of method utilizing waste molasses of sugar plant to produce biological foliage fertilizer " (200810088386), just It is that the blackstrap utilizing sugar refinery is processed, utilizes the foliage fertilizer fermenting out to be applied to crop On, it is possible to add certain chemical fertilizer and be mixed with using;" the liquid that molasses alcohol waste liquid manufactures Fertilizer and method " (CN02134669), use P2O5Or H3PO4And HNO3Make digestion agent, Turn down waste liquid pH value≤1.5, clear up at high temperature under high pressure, then adjust with ammonia and CaO Joint pH value be 6.0~7.0 liquid fertilizer.
But above invention has some problems, such as in Water soluble fertilizer: above first invention, Its market acceptance level is poor, and fertilizer is functional the most common, it is impossible to meet the demand of peasant household, the Two inventions relate to strong acid, and manufacturing process is excessively dangerous and has the possibility polluting environment.The most once had Similar liquid production is fertile containing humic acid liquid by producer, has certain effect, but generally Also being that market acceptance level is poor, fertilizer is functional the most common, it is impossible to meet the demand of peasant household.
In order to solve that environmental pollution, fertilizer effect be more single, fertilizer manufacturing technology is low this A little problems, Liquid Fertilizer should be processed to high-tech, strengthens using effect, meet user to use The hobby of the multi-direction demand of effect, thus reach benign cycle: it is dirty that terminal requirements solves environment Dye problem.Such as develop one and can prevent and treat soil pathogenic bacteria virus, hestening rooting, conditioned soil The fertilizer of the effects such as earth, raising crop anti-adversity, supplementary crop element, if but allowing user buy Several things return use just reach above effect if, just can only increase on foot manually to become with the time This.There is producer also to carry out this studying, but fertilizer is simple mixture, utilization of being far from being Production technology in terms of biochemistry, so product effect is also the most general.
[summary of the invention]
The invention aims to overcome the defect of prior art, it is provided that one can prevent and treat soil Earth pathogenic bacteria virus, hestening rooting, improvement soil, raising crop anti-adversity, supplementary crop element The production method of the organic water soluble Liquid Fertilizer of effect, the method mainly utilizes biochemical processes The using effect making Liquid Fertilizer is more excellent.
The present invention for achieving the above object, by the following technical solutions:
The production method of a kind of organic water soluble Liquid Fertilizer, it is characterised in that include walking in detail below Rapid:
A, by yeast and lactic acid bacteria respectively by 100,000,000/cm3The index of liquid joins fertilizer Stock solution mix homogeneously, then carry out anaerobic fermentation at least 48 in the presence of biological filler material Hour;
By 1,000,000,000/cm in b, fertilizer stock solution after anaerobic fermentation3The index of liquid adds ground Clothing bacillus cereus, and add arsenic determination, boron fertilizer, zinc fertilizer and molydbenum fertilizer, then aeration, Carry out aerobic fermentation at least 24 hours;
C, fertilizer stock solution after aerobic fermentation press 20Kg/m3The amount of liquid adds liquid first Shell element, after stirring.
The biological filler bed of material in the present invention is bar brush, arranges two-layer, is respectively placed in fertilizer former 1/5 and 1/2 eminence of liquid place container, microorganism can be sufficiently adhering to the breeding of biological filler material, This container can be reactor, it is also possible to be reaction tank.
The present invention is placed with immersible pump bottom anaerobic fermentation stage, fertilizer stock solution, every 12 little Shi Kaidong once, each half an hour.The outlet of this immersible pump is parallel with at the bottom of pond, starts latent During water pump, the liquid in rotation flowing of bottom can be made, to reach the purpose stirred, make part The liquid on upper strata can enter in lower floor.
Present invention addition of arsenic determination in the aerobic fermentation stage is 3Kg/m3Liquid Body.
Boron fertilizer in the present invention is Borax, and addition is 2Kg/m3Liquid, zinc fertilizer is seven water sulfur Acid zinc, addition is 0.5Kg/m3Liquid, molydbenum fertilizer is ammonium molybdate, and addition is 0.2Kg/m3 Liquid.
Arsenic determination in the present invention, boron fertilizer, zinc fertilizer and molydbenum fertilizer first add with after water dissolution again Enter in fertilizer stock solution.
The present invention in the aerobic fermentation stage of step b, every aeration 4 hours the most static 2 Hour until aerobic fermentation is complete.
In the present invention, the chitin of the liquid chitin that agitation phases after aerobic fermentation adds contains Amount is 1wt%.
Fertilizer stock solution mainly includes that the straw water in sugar refinery and/or the yeast waste liquor of yeast factory etc. are containing organic Matter, humic acids, the soluble ingredient of nutrient, wherein the straw water in sugar refinery refers to the blackstrap of pitchy, The yeast mixture of yeast factory is pitchy.
The present invention compared with prior art, has the advantage that
(1) during production process uses anaerobic fermentation process, the bottom in fertilizer stock solution (i.e. reacts appearance Device or the bottom of reaction tank) anaerobic fermentation stirring facility setting strip brush biological filler thing is set Mode, exposes aerobe fermentation mode during aerobic fermentation, make stock solution carry out anaerobism and aerobic good ferment, Larger molecular organics acidolysis in anaerobic fermentation stage is easily made to become small organic molecule, it is easy to Chelate with other chemicals under good oxygen condition, promote the effect of each element, relatively other letters Liquid Fertilizer out made by single mixing, is greatly improved effect;
(2) production technology is simple, does not has operational complexity;
(3) aerobic fermentation have employed the Bacillus licheniformis of double oxide growth breeding, and it can disliked Forming spore under bad environment thus preserve life, this just can be allowed to be applied in soil effectively, Reach the effect of growth promotion and disease prevention;
(4) interpolation of chitin, also makes fertilizer be provided with and presses down nematicide, controlling disease, raising The effect of crop anti-adversity;
(5) interpolation of nitric acid rare earth, itself and the aminoacid in fertilizer, humic acid chelating, effect More preferably, make fertilizer more have the function significantly promoting growth, and improve the product of agricultural product Matter;
(6) composition of this Liquid Fertilizer can effectively prevent and treat soil pathogenic bacteria virus, and have hestening rooting, The effects such as improvement soil, raising crop anti-adversity, supplementary crop element.
[detailed description of the invention]
The production method of the present invention a kind of organic water soluble Liquid Fertilizer, including step in detail below:
A, by yeast and lactic acid bacteria respectively by 100,000,000/cm3The index of liquid joins fertilizer Stock solution mix homogeneously, then carry out anaerobic fermentation at least 48 in the presence of biological filler material Hour;
By 1,000,000,000/cm in b, fertilizer stock solution after anaerobic fermentation3The index of liquid adds ground Clothing bacillus cereus, and add arsenic determination, boron fertilizer, zinc fertilizer and molydbenum fertilizer, then aeration, Carry out aerobic fermentation at least 24 hours;
C, fertilizer stock solution after aerobic fermentation press 20Kg/m3The amount of liquid adds chitin Content is the liquid chitin of 1wt%, after stirring.
Wherein the biological filler material in step a is bar brush, conspires to create one layer side by side, arranges two altogether Layer, is respectively placed in 1/5 and 1/2 eminence of fertilizer stock solution place container, at anaerobic fermentation stage, It is placed with immersible pump bottom fertilizer stock solution, within every 12 hours, starts once, each half an hour.
Wherein in step b, the addition of arsenic determination is 3Kg/m3Liquid, boron fertilizer is boron Sand, addition is 2Kg/m3Liquid, zinc fertilizer is zinc sulphate heptahydrate, and addition is 0.5Kg/m3 Liquid, molydbenum fertilizer is ammonium molybdate, and addition is 0.2Kg/m3Liquid, during aerobic fermentation, every aeration 4 Individual hour the most static 2 hours until aerobic fermentation is complete.
Describe the present invention below in conjunction with specific embodiment:
Design a stock solution storage pool, anaerobic pond, Aerobic Pond, stirring pool, One finished product storage pool, these objects combine together the most successively, form one completely Production technology system.
Containing straw liquid manure material stock solution in stock solution storage pool, its discharging opening is at the bottom of by pipeline and anaerobic pond Portion communicates, fertilizer stock solution can controllable flow rate put into bottom anaerobic pond, anaerobic pond pond is high 1/5 and 1/2 eminence, is respectively provided with one layer of biological filler material, is provided with immersible pump bottom anaerobic pond, After piling fertilizer stock solution in anaerobic pond, by 100,000,000/cm3The index of liquid is separately added into yeast Bacterium and lactic acid bacteria, after starting immersible pump mix homogeneously, start immersible pump and enter for the most every 12 hours Row mixing dispersion, starts half an hour every time, and circulation carries out anaerobic fermentation 48 hours.
The discharging opening of anaerobic pond is positioned at top, and its discharging opening is by phase bottom pipeline and Aerobic Pond Logical, after anaerobic fermentation, put into new fertilizer stock solution, the top anaerobism that can squeeze out respective amount is sent out The fertilizer solution of ferment enters Aerobic Pond, and so transfer fertilizer solution introduces too much prevented also from anaerobic pond Oxygen affects anaerobic fermentation, and the amount putting into new fertilizer stock solution to discharge the liquid of anaerobic pond 60% is Reference standard.
After fertilizer solution enters Aerobic Pond, by 1,000,000,000/cm3The index of liquid adds lichens spore Bacillus, adds arsenic determination 3Kg/m3Liquid, Borax 2Kg/m3Liquid, seven water sulphuric acid Zinc 0.5Kg/m3Liquid, ammonium molybdate 0.2Kg/m3Liquid, first with water-soluble before chemical fertilizer addition Solving, then aeration carries out aerobic fermentation, and every aeration 4 hours is the most static 2 hours, until 24 hours, then by bottom Aerobic Pond by fertilizer solution suction stirring pool, stirring is lower presses 20Kg/m3 The amount of liquid adds the liquid chitin that chitin content is 1wt%, by stirring after stirring Suction finished product storage pool bottom pond, the fertilizer solution prepared is also in finished product storage pool Stirring, prevents precipitate asymmetric suspension in liquid, finally carries out packing.
Fertilizer out made by the present invention meets the technical specification that organic water soluble is fertile.
Fertilizer solution prepared by the present invention can be used for land for growing field crops and irrigates, and concentration during foliage-spray is 300 times, usage amount is 50mL, and namely this fertilizer of 50mL converts 15Kg water to dilute use; Consumption is irrigated in land for growing field crops: this Liquid Fertilizer of 10Kg is used for 1 mu of ground, converts the dilution of at least 100L water and makes With, even can be better than the effect of 100L water more than the water-reducible effect of 100L, but not surpass Crossing 500L water, too much water adds, may result in the loss of fertilizer.
Comparative example: by fertilizer stock solution, zymocyte and the chemical fertilizer identical with the present invention without appointing What fermentation is simply simply mixed.
By fertile for the fluid present invention land for growing field crops Brassica campestris L. ssp.chinensis plantation being respectively applied to the same terms with comparative example, Find that fluid present invention fertilizer increases production 22.3% than comparative example, sickness rate relative reduction 56.2%;
By fertile for the fluid present invention corn planting being respectively applied to the same terms with comparative example, find Fluid present invention fertilizer increases production 24.1% than comparative example, sickness rate relative reduction 50.3%;
By fertile for the fluid present invention Brassica campestris L. ssp.chinensis soilless culture being respectively applied to the same terms with comparative example (water planting), finds that fluid present invention fertilizer increases production 35.2% than comparative example, and sickness rate drops relatively Low by 80.2%.

Claims (9)

1. the production method of an organic water soluble Liquid Fertilizer, it is characterised in that include following tool Body step:
A, by yeast and lactic acid bacteria respectively by 100,000,000/cm3The index of liquid joins fertilizer Stock solution mix homogeneously, then carry out anaerobic fermentation at least 48 in the presence of biological filler material Hour;
By 1,000,000,000/cm in b, fertilizer stock solution after anaerobic fermentation3The index of liquid adds ground Clothing bacillus cereus, and add arsenic determination, boron fertilizer, zinc fertilizer and molydbenum fertilizer, then aeration, Carry out aerobic fermentation at least 24 hours;
C, fertilizer stock solution after aerobic fermentation press 20Kg/m3The amount of liquid adds liquid carapace Element, after stirring;
Described biological filler material is bar brush, arranges two-layer, is respectively placed in described fertilizer stock solution 1/5 and 1/2 eminence of place container.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, It is characterized in that at anaerobic fermentation stage, bottom fertilizer stock solution, be equipped with immersible pump, every 12 hours Start once, each half an hour.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, It is characterized in that in the aerobic fermentation stage, the addition of arsenic determination is 3Kg/m3Liquid.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, It is characterized in that described boron fertilizer is Borax, addition is 2Kg/m3Liquid, described zinc fertilizer is Zinc sulphate heptahydrate, addition is 0.5Kg/m3Liquid, described molydbenum fertilizer is ammonium molybdate, addition For 0.2Kg/m3Liquid.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, It is characterized in that described arsenic determination, boron fertilizer, zinc fertilizer and molydbenum fertilizer first with after water dissolution again Add in fertilizer stock solution.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, It is characterized in that in the aerobic fermentation stage of step b, every aeration 4 hours the most static 2 Hour until aerobic fermentation is complete.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, The chitin content that it is characterized in that described liquid chitin is 1wt%.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 1, It is characterized in that described fertilizer stock solution includes that the straw water in sugar refinery and/or the yeast of yeast factory give up Liquid.
The production method of a kind of organic water soluble Liquid Fertilizer the most according to claim 8, It is characterized in that described sugar refinery straw water is pitchy blackstrap, the yeast waste liquor of described yeast factory For pitchy.
CN201410403137.1A 2014-08-15 2014-08-15 A kind of production method of organic water soluble Liquid Fertilizer Active CN104151092B (en)

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CN105801186A (en) * 2014-12-31 2016-07-27 哈尔滨市企效生物科技有限公司 Method for rapidly processing night soil into feeds and fertilizers through using ecologic active liquid
CN105777215A (en) * 2016-02-01 2016-07-20 江西菲蓝生物工程有限公司 Composite water-soluble bio-organic fertilizer and production method thereof
CN105837263A (en) * 2016-03-17 2016-08-10 哈尔滨市企效生物科技有限公司 Process for producing organic fertilizer by rapidly treating straw with probiotics
CN105777216A (en) * 2016-03-17 2016-07-20 哈尔滨市企效生物科技有限公司 Technique of utilizing probiotic combination to quickly treat manure to produce feed and fertilizer
CN107540476A (en) * 2017-09-28 2018-01-05 三门峡龙飞生物工程有限公司 A kind of full water-soluble bio-organic fertilizer and preparation method thereof
CN109336687A (en) * 2018-11-19 2019-02-15 黑龙江八农垦大学 Hydrolyzed yeast zinc foliar fertilizer, production method and application
CN113860963B (en) * 2021-09-14 2023-05-12 湖北国硒科技发展有限公司 Organic selenium-rich nutrient solution and preparation method and application thereof

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CN103896646A (en) * 2014-04-21 2014-07-02 厦门禾嘉吉升生物技术有限公司 Preparation method of microorganism organic fertilizer

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Publication number Priority date Publication date Assignee Title
CN101717303A (en) * 2009-12-11 2010-06-02 杨宝森 Biological organic water-soluble fertilizer and preparation method thereof
CN202269379U (en) * 2011-01-21 2012-06-13 西昌学院 Circulating type potato residue anaerobic fermentation tower filled with CO2
CN103214299A (en) * 2012-01-19 2013-07-24 刘旭辉 Organic water-soluble fertilizer containing amino acid microbes, and preparation method thereof
CN102936166A (en) * 2012-11-29 2013-02-20 南宁市英德肥业有限责任公司 Water-soluble organic/inorganic compound fertilizer prepared by molasses fermentation liquor and preparation method of fertilizer
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