CN104140758B - A kind of high temperature resistant wall covering and preparation method thereof - Google Patents
A kind of high temperature resistant wall covering and preparation method thereof Download PDFInfo
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- CN104140758B CN104140758B CN201410334454.2A CN201410334454A CN104140758B CN 104140758 B CN104140758 B CN 104140758B CN 201410334454 A CN201410334454 A CN 201410334454A CN 104140758 B CN104140758 B CN 104140758B
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Abstract
A kind of high temperature resistant wall covering and preparation method thereof, this coating comprises the following raw material according to mass fraction meter: 12～20 parts of organic siliconresins, 12～20 parts of fluorubber, 4～9 parts of zinc carbonates, 20～27 parts of alundum (Al2O3)s, 5～12 parts of sepiolites, 15～25 parts of silica flours, 7～15 parts of aluminum pastes, 0.3～1.2 part, NaOH, 3～8 parts of titanate esters, 23～40 parts of boric acid, 2～5 parts of benzoin ethyl ethers, 70～100 parts, water. Coating provided by the invention has excellent shock-resistant, heat-resisting, heat insulation and anti-wear performance, and the high temperature resistant time is long, is especially suitable for the application of high temperature place metope.
Description
Technical field
The invention belongs to technical field of coatings, be specifically related to a kind of high temperature resistant wall covering and preparation method thereof.
Background technology
Wall covering refers to for building wall and rises and decorate and protection, makes building wall beautiful and clean, also can play protection building wall, the effect that extends its service life simultaneously. Wall covering comprises interior wall coating and exterior coating two large divisions by building wall classification. Interior wall coating is focused on decorating and environmental protection; Exterior coating is focused on protection and durable. Wall covering is except itself decoration and protective effect, also to rich and varied, fashion, health environment-friendly trend development. People are brilliant at the decorative effect of wishing coating, magnificent mansion, elegant, romance, warm in, also wish that coating itself is pollution-free, health environment-friendly, individual character and be rich in third dimension.
Under some specific condition, the inside and outside wall of for example fireplace, the inwall of high-temperature workshop, they are usually under the state in high temperature, and common wall covering can not meet requirement far away. Wall covering is in the market high temperature resistant and heat-proof quality is poor, and the high temperature resistant time is short, and it is wear-resisting and flame retardant effect is poor simultaneously, and coating of long duration is easy to cracking and comes off.
Summary of the invention
The technical scheme solving:For shortcomings such as high temperature resistant and poor, high temperature resistant time of heat-proof quality of existing wall covering are short, the invention provides a kind of high temperature resistant wall covering and preparation method thereof.
Technical scheme:A kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 12～20 parts of organic siliconresins, 12～20 parts of fluorubber, 4～9 parts of zinc carbonates, 20～27 parts of alundum (Al2O3)s, 5～12 parts of sepiolites, 15～25 parts of silica flours, 7～15 parts of aluminum pastes, 0.3～1.2 part, NaOH, 3～8 parts of titanate esters, 23～40 parts of boric acid, 2～5 parts of benzoin ethyl ethers, 70～100 parts, water.
One described above is high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 15～18 parts of organic siliconresins, 14～17 parts of fluorubber, 5～7 parts of zinc carbonates, 23～25 parts of alundum (Al2O3)s, 8～10 parts of sepiolites, 18～22 parts of silica flours, 9～12 parts of aluminum pastes, 0.6～1 part, NaOH, 4.5～6.5 parts of titanate esters, 28～35 parts of boric acid, 3.5～4 parts of benzoin ethyl ethers, 80～90 parts, water.
One described above is high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 16.5 parts of organic siliconresins, 16 parts of fluorubber, 6 parts of zinc carbonates, 24 parts of alundum (Al2O3)s, 9 parts of sepiolites, 20 parts of silica flours, 10.5 parts of aluminum pastes, 0.8 part, NaOH, 5.5 parts of titanate esters, 31 parts of boric acid, 3.7 parts of benzoin ethyl ethers, 85 parts, water.
The preparation method of a kind of high temperature resistant wall covering described above, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 30～50min, and being ground to fineness is 50～70 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
In second step described above, milling time is 40min, and being ground to fineness is 60 μ m.
Beneficial effect:The invention provides a kind of high temperature resistant wall covering and preparation method thereof, this coating has been undertaken rational composite by organic siliconresin, fluorubber and other additives, make coating there is excellent shock-resistant, heat-resisting, heat insulation and anti-wear performance, and the high temperature resistant time is long, be especially suitable for the application of high temperature place metope.
Detailed description of the invention
Embodiment 1
The present embodiment provides a kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 12 parts of organic siliconresins, 12 parts of fluorubber, 4 parts of zinc carbonates, 20 parts of alundum (Al2O3)s, 5 parts of sepiolites, 15 parts of silica flours, 7 parts of aluminum pastes, 0.3 part, NaOH, 3 parts of titanate esters, 23 parts of boric acid, 2 parts of benzoin ethyl ethers, 70 parts, water.
A preparation method for high temperature resistant wall covering, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 30min, and being ground to fineness is 50 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Embodiment 2
The present embodiment provides a kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 20 parts of organic siliconresins, 20 parts of fluorubber, 9 parts of zinc carbonates, 27 parts of alundum (Al2O3)s, 12 parts of sepiolites, 25 parts of silica flours, 15 parts of aluminum pastes, 1.2 parts, NaOH, 8 parts of titanate esters, 40 parts of boric acid, 5 parts of benzoin ethyl ethers, 100 parts, water.
A preparation method for high temperature resistant wall covering, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 50min, and being ground to fineness is 70 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Embodiment 3
The present embodiment provides a kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 15 parts of organic siliconresins, 14 parts of fluorubber, 5 parts of zinc carbonates, 23 parts of alundum (Al2O3)s, 8 parts of sepiolites, 18 parts of silica flours, 9 parts of aluminum pastes, 0.6 part, NaOH, 4.5 parts of titanate esters, 28 parts of boric acid, 3.5 parts of benzoin ethyl ethers, 80 parts, water.
A preparation method for high temperature resistant wall covering, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 35min, and being ground to fineness is 55 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Embodiment 4
The present embodiment provides a kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 18 parts of organic siliconresins, 17 parts of fluorubber, 7 parts of zinc carbonates, 25 parts of alundum (Al2O3)s, 10 parts of sepiolites, 22 parts of silica flours, 12 parts of aluminum pastes, 1 part, NaOH, 6.5 parts of titanate esters, 35 parts of boric acid, 4 parts of benzoin ethyl ethers, 90 parts, water.
A preparation method for high temperature resistant wall covering, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 45min, and being ground to fineness is 65 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Embodiment 5
The present embodiment provides a kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 16 parts of organic siliconresins, 15 parts of fluorubber, 5.5 parts of zinc carbonates, 23 parts of alundum (Al2O3)s, 8.5 parts of sepiolites, 19 parts of silica flours, 10 parts of aluminum pastes, 0.7 part, NaOH, 4.8 parts of titanate esters, 29 parts of boric acid, 3.6 parts of benzoin ethyl ethers, 82 parts, water.
A preparation method for high temperature resistant wall covering, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 40min, and being ground to fineness is 60 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Embodiment 6
The present embodiment provides a kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 16.5 parts of organic siliconresins, 16 parts of fluorubber, 6 parts of zinc carbonates, 24 parts of alundum (Al2O3)s, 9 parts of sepiolites, 20 parts of silica flours, 10.5 parts of aluminum pastes, 0.8 part, NaOH, 5.5 parts of titanate esters, 31 parts of boric acid, 3.7 parts of benzoin ethyl ethers, 85 parts, water.
A preparation method for high temperature resistant wall covering, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 40min, and being ground to fineness is 60 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Reference examples 1
Be with the difference of embodiment 1: in the first step, do not add alundum (Al2O3) and sepiolite, in the 3rd step, do not add boric acid, benzoin ethyl ether. Specifically refer to:
A kind of high temperature resistant wall covering, comprises the following raw material according to mass fraction meter: 12 parts of organic siliconresins, 12 parts of fluorubber, 4 parts of zinc carbonates, 15 parts of silica flours, 7 parts of aluminum pastes, 0.3 part, NaOH, 3 parts of titanate esters, 70 parts, water.
The preparation method of this reference examples, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 30min, and being ground to fineness is 50 μ m, obtains mixture B;
The 3rd step: add titanate esters and water in mixture B, add NaOH after mixing, continue to mix and remember finished product.
Performance test
Embodiment 1 to 6, reference examples 1 gained finished product are used for to film, gained coating are carried out to performance test, wherein, result of the test as in the table below:
Result of the test
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Reference examples 1 | |
| Adhesive force/level | 1 | 1 | 1 | 1 | 1 | 1 | 2 |
| Impact strength/kgcm | 57 | 64 | 58 | 55 | 61 | 63 | 50 |
| Heat resistance (1000 DEG C) | 4min film is complete | 5min film is complete | 3min film is complete | 4min film is complete | 5min film is complete | 7min film is complete | 2min film is complete |
| Abrasion resistance | Do not see the bottom for 3720 times | Do not see the bottom for 3712 times | Do not see the bottom for 3811 times | Do not see the bottom for 3823 times | Do not see the bottom for 3855 times | Do not see the bottom for 3867 times | Do not see the bottom for 3500 times |
As can be seen from the table, relatively can find out with reference examples 1 by embodiment 1, by adding alundum (Al2O3), sepiolite, boric acid and benzoin ethyl ether, make this coating there is excellent shock-resistant, heat-resisting, heat insulation and anti-wear performance.
Above the embodiment of the present invention is described in detail, for one of ordinary skill in the art, according to the thought of the embodiment of the present invention, all will change in specific embodiments and applications, in sum, this description should not be construed as limitation of the present invention.
Claims (5)
1. a high temperature resistant wall covering, it is characterized in that, formed by the raw material of following mass fraction meter: 12～20 parts of organic siliconresins, 12～20 parts of fluorubber, 4～9 parts of zinc carbonates, 20～27 parts of alundum (Al2O3)s, 5～12 parts of sepiolites, 15～25 parts of silica flours, 7～15 parts of aluminum pastes, 0.3～1.2 part, NaOH, 3～8 parts of titanate esters, 23～40 parts of boric acid, 2～5 parts of benzoin ethyl ethers, 70～100 parts, water.
2. the high temperature resistant wall covering of one according to claim 1, it is characterized in that, formed by the raw material of following mass fraction meter: 15～18 parts of organic siliconresins, 14～17 parts of fluorubber, 5～7 parts of zinc carbonates, 23～25 parts of alundum (Al2O3)s, 8～10 parts of sepiolites, 18～22 parts of silica flours, 9～12 parts of aluminum pastes, 0.6～1 part, NaOH, 4.5～6.5 parts of titanate esters, 28～35 parts of boric acid, 3.5～4 parts of benzoin ethyl ethers, 80～90 parts, water.
3. the high temperature resistant wall covering of one according to claim 1, it is characterized in that, formed by the raw material of following mass fraction meter: 16.5 parts of organic siliconresins, 16 parts of fluorubber, 6 parts of zinc carbonates, 24 parts of alundum (Al2O3)s, 9 parts of sepiolites, 20 parts of silica flours, 10.5 parts of aluminum pastes, 0.8 part, NaOH, 5.5 parts of titanate esters, 31 parts of boric acid, 3.7 parts of benzoin ethyl ethers, 85 parts, water.
4. a preparation method for high temperature resistant wall covering as claimed in claim 1, is characterized in that, comprises the following steps:
The first step: organic siliconresin, fluorubber, zinc carbonate, alundum (Al2O3), sepiolite, silica flour and aluminum paste are added in mixer, be uniformly mixed and obtain mixture A;
Second step: mixture A is added to grinding machine for grinding 30～50min, and being ground to fineness is 50～70 μ m, obtains mixture B;
The 3rd step: add titanate esters, boric acid, benzoin ethyl ether and water in mixture B, add NaOH after mixing, continue to mix and get product.
5. the preparation method of a kind of high temperature resistant wall covering according to claim 4, is characterized in that: in described second step, milling time is 40min, and being ground to fineness is 60 μ m.
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| CN201410334454.2A CN104140758B (en) | 2014-07-15 | 2014-07-15 | A kind of high temperature resistant wall covering and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101033369A (en) * | 2007-04-19 | 2007-09-12 | 重庆三峡油漆股份有限公司 | Semi-interpenetrating network structure double-component fire resistant paint |
| CN101230224A (en) * | 2008-02-27 | 2008-07-30 | 孟中 | Fluorosilicone rubber nano composite alloy three-proof paint and production method thereof |
| CN102585696A (en) * | 2012-02-13 | 2012-07-18 | 江苏大学 | Methyl phenyl silicone resin base high-temperature-resistant coating and preparation method thereof |
| CN102816519A (en) * | 2012-07-25 | 2012-12-12 | 江苏科技大学 | Inorganic-organic high temperature-resistant coating and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02305875A (en) * | 1989-05-19 | 1990-12-19 | Ube Ind Ltd | Heat-resistant coating material |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101033369A (en) * | 2007-04-19 | 2007-09-12 | 重庆三峡油漆股份有限公司 | Semi-interpenetrating network structure double-component fire resistant paint |
| CN101230224A (en) * | 2008-02-27 | 2008-07-30 | 孟中 | Fluorosilicone rubber nano composite alloy three-proof paint and production method thereof |
| CN102585696A (en) * | 2012-02-13 | 2012-07-18 | 江苏大学 | Methyl phenyl silicone resin base high-temperature-resistant coating and preparation method thereof |
| CN102816519A (en) * | 2012-07-25 | 2012-12-12 | 江苏科技大学 | Inorganic-organic high temperature-resistant coating and preparation method thereof |
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