CN101704633A - Colored glazed glass and production method thereof - Google Patents
Colored glazed glass and production method thereof Download PDFInfo
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- CN101704633A CN101704633A CN200910224711A CN200910224711A CN101704633A CN 101704633 A CN101704633 A CN 101704633A CN 200910224711 A CN200910224711 A CN 200910224711A CN 200910224711 A CN200910224711 A CN 200910224711A CN 101704633 A CN101704633 A CN 101704633A
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Abstract
The invention belongs to the technical field of deep processing of glass, in particular to colored glazed glass and a production method thereof. The colored glazed glass is prepared by the following method: cleaning a glass substrate, then drying, roll-coating a layer of high-temperature inorganic glass glaze or screen-printing the glass glaze on the surface of the glass, and they drying; and further heating the glass to a softening point, and then slowly reducing the temperature for annealing, thereby preparing a finished product. The color glazed glass produced by the method does not contain volatile harmful substances and can be any color and translucent or opaque; and the secondary processing can be carried out, and the glass has no deformation or color change, thereby being an environment-friendly high-grade glass decorative product which can meet the needs of customers to the maximum extent; in addition, the glass substrate can be any dimension, and the maximum dimension of the glass which can be produced is 1.83 multiplied by 2.44M.
Description
(1) technical field
The invention belongs to glass deep process technology field, particularly a kind of colored glazed glass and production method thereof.
(2) background technology
Current social development is rapid, people's living standard significantly promotes, the indoor and outdoor finishing material is more and more stricter to the requirement of quality and environmental protection aspect, but finishing material major part in the market all exists different defectives, as: common colored paint glass back of the body lacquer easily comes off, and is easy to change, fade, because of use in the production process to be that the organic printing ink of low temperature is volatile go out objectionable impuritiess such as benzene, toluene, the infringement HUMAN HEALTH, and can not carry out hot-work such as tempering, hot bending once more.Finishing material such as marble, grouan, major part all have certain radioactivity, are no lack of the example that the finishing descendant's who causes thus healthy state is endangered both at home and abroad.Finishing materials such as timber floor have formaldehyde and produce because used organic tackiness agent.The tempering colored glazed glass be by with the glass glaze by silk screen printing on glass surface, after drying, tempering are handled, permanent a kind of antiacid alkali that is sintered in glass surface and obtains of glaze and safe novel decorative glasswork, wherein harmful organic substances and radioactive element content do not have substantially; In the market can be customized to its size, still, there is secondary processing such as can not punching, cut in this kind glass, and the shortcoming that shape can not change makes the autonomy of decoration be subjected to very big restriction.
(3) summary of the invention
The object of the present invention is to provide a kind of colored glazed glass and production method thereof, so that a kind of harmful organic substance, radioelement of not containing to be provided, and the ambetti of secondary processing such as can punch, cut arbitrarily.
The technical solution used in the present invention is as follows:
A kind of colored glazed glass is made by laxative remedy: with the clean after drying of glass substrate, and in glass surface roller coat one deck high temperature unorganic glass glaze or silk screen printing upper glass glaze, oven dry then; Again with glass heats behind the softening temperature slowly cooling annealing make finished product.
Described slow cooling annealing is carried out according to following steps: the glass surface temperature is progressively reduced to 570-590 ℃, 540-560 ℃, 460-480 ℃, 290-310 ℃ successively, be cooled to normal temperature then naturally.
Described oven dry is carried out at 130-180 ℃, preferred 150 ℃.Can take long drying time when lesser temps carries out, otherwise then dry the short period.
Described high temperature unorganic glass glaze at the glass back roller coat can be deployed into shades of colour, roller coat becomes all thickness;
Glass substrate can be any width, and the maximum space of a whole page can be 1.83*2.44m.
Glass heats, and the temperature of glass surface will reach the fusing point of unorganic glass glaze and the softening temperature of glass, and glass and glass glaze are perfectly merged at glass surface.
Slowly the cooling annealing process also can carry out according to general method, and purpose is to reduce the unrelieved stress and the surface stress of glass inside, as long as can realize this purpose.And in the technology that the present invention adopts, the surface temperature that progressively reduces glass can realize by number of ways, as utilize the temperature head etc. of hot air circulation countercurrent flow, control annealing furnace top and the bottom, after the glass surface temperature is low, can also force the multiple mode of cooling to be cooled to normal temperature by naturally cooling, hot air circulation cooling, cold wind.
The colored glazed glass that the present invention produces, itself does not contain volatile injurant matter, can be any color, can make translucent and opaque; And through secondary slow annealing process, the unrelieved stress of glass inside and surface stress reach the stress requirement of common float glass basically, and substantially less than 3MPa, and glass and glass glaze have merged as its surface stress; Therefore can be according to client's self needs, carry out secondary processing, for example tempering, hot bending, punching, edging, cut etc., in secondary processing, indeformable, the nondiscoloration of glass itself, be a kind of environmental protection, satisfy the high-grade glass decorative product of client's needs to greatest extent. its glass substrate can be any size in addition, and maximum can be produced the glass of 1.83*2.44M.
(4) embodiment:
Below with specific embodiment technical scheme of the present invention is described, but protection scope of the present invention is not limited thereto:
Embodiment 1
Colored glazed glass, concrete preparation process is as follows:
1) at first transparent sheet glass is cleaned up, in 100 ℃ of oven dry;
2) with clean cleaning glass later, through roller coating machine, the inorganic aqueous glass ink of high temperature of roll marks last layer white, the line number of used roller is 55 lines, every square metre 160 gram of ink usage;
3), under 150 ℃ condition, carry out heating, drying and handle the glass that has white inorganic ink;
4) above-mentioned glass is sent to process furnace and heats, temperature is 680 ℃;
5) glass more than the softening point temperature is carried out anneal, the annealing furnace design temperature of fs is 381 ℃ on top, and temperature of lower is 406 ℃, makes the glass surface temperature reduce to 580 ℃; Subordinate phase top design temperature is 394 ℃, 448 ℃ of bottom design temperatures, and the glass surface temperature is reduced to 550 ℃; Phase III top is 259 ℃, and temperature of lower is 288 ℃, and the glass surface temperature is reduced to 470 ℃; The quadravalence section is 150 ℃, and the glass surface temperature is reduced to 300 ℃ substantially, and five-stage is the naturally cooling cooling, and the 6th stage was that cold wind is cooled to normal temperature, promptly made finished glass.
Embodiment 2
Colored glazed glass, concrete preparation process is as follows:
1) at first transparent sheet glass is cleaned up, in 120 ℃ of oven dry;
2) silk screen of pre-designed pattern is placed on above the clean cleaning glass later, adopts the red inorganic aqueous printing ink of high temperature, print designing on the silk screen of pattern, ink usage is every square metre 50 gram;
3), under 140 ℃ condition, carry out heating, drying and handle the glass that has red inorganic aqueous printing ink;
4) above-mentioned glass is sent to process furnace and heats, temperature is 670 ℃;
5) glass more than the softening point temperature is carried out anneal, the annealing furnace design temperature of fs is 390 ℃ on top, and temperature of lower is 400 ℃; Subordinate phase top design temperature is 395 ℃, 430 ℃ of bottom design temperatures; Phase III top is 249 ℃, and temperature of lower is 260 ℃; The quadravalence section is 100 ℃, and five-stage is the naturally cooling cooling, and the 6th stage was that cold wind is cooled to normal temperature, promptly made the finished product colored glazed glass.
Embodiment 3
Colored glazed glass, concrete preparation process is as follows:
1) at first transparent sheet glass is cleaned up, in 150 ℃ of oven dry;
2) with clean cleaning glass later, through roller coating machine, the inorganic aqueous glass ink of high temperature of roll marks last layer green, the line number of used roller is 55 lines, every square metre 150 gram of ink usage;
3), under 150 ℃ condition, carry out heating, drying and handle the glass that has green inorganic aqueous printing ink;
4) above-mentioned glass is sent to process furnace and heats, temperature is 685 ℃;
5) glass more than the softening point temperature is carried out anneal, the annealing furnace design temperature of fs is 381 ℃ on top, and temperature of lower is 406 ℃; Subordinate phase top design temperature is 394 ℃, 448 ℃ of bottom design temperatures; Phase III top is 259 ℃, and temperature of lower is 288 ℃; The quadravalence section is 150 ℃, and five-stage is the naturally cooling cooling, and the 6th stage was that cold wind is cooled to normal temperature, promptly made the finished product colored glazed glass.
Claims (7)
1. a colored glazed glass is characterized in that, is made by laxative remedy: with the clean after drying of glass substrate, and in glass surface roller coat one deck high temperature unorganic glass glaze or silk screen printing upper glass glaze, oven dry then; Again with glass heats behind the softening temperature slowly cooling annealing make finished product.
2. colored glazed glass as claimed in claim 1, it is characterized in that, described slow cooling annealing is carried out according to following steps: the glass surface temperature is progressively reduced to 570-590 ℃, 540-560 ℃, 460-480 ℃, 290-310 ℃ successively, be cooled to normal temperature then naturally.
3. colored glazed glass as claimed in claim 1 or 2 is characterized in that, oven dry is carried out at 130-180 ℃.
4. the production method of the described colored glazed glass of claim 1 is characterized in that, with the clean after drying of glass substrate, and in glass surface roller coat one deck high temperature unorganic glass glaze or silk screen printing upper glass glaze, oven dry then; With glass heats behind the softening temperature slowly cooling annealing make finished product.
5. the production method of colored glazed glass as claimed in claim 4, it is characterized in that, described slow cooling annealing is carried out according to following steps: the glass surface temperature is progressively reduced to 570-590 ℃, 540-560 ℃, 460-480 ℃, 290-310 ℃ successively, be cooled to normal temperature then naturally.
6. as claim 4 or 5 described colored glazed glass, it is characterized in that oven dry is carried out at 130-180 ℃.
7. the production method of colored glazed glass as claimed in claim 6 is characterized in that, described bake out temperature is 150 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910224711A CN101704633A (en) | 2009-05-14 | 2009-11-10 | Colored glazed glass and production method thereof |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910064895.4 | 2009-05-14 | ||
| CN200910224711A CN101704633A (en) | 2009-05-14 | 2009-11-10 | Colored glazed glass and production method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN101704633A true CN101704633A (en) | 2010-05-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN200910224711A Pending CN101704633A (en) | 2009-05-14 | 2009-11-10 | Colored glazed glass and production method thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102260045A (en) * | 2010-03-18 | 2011-11-30 | 杨德宁 | Environment-friendly, energy-saving and low-melting-point color glaze decoration flat glass with high annealing temperature and strength and preparation method thereof |
| CN102730981A (en) * | 2011-04-15 | 2012-10-17 | 中航三鑫股份有限公司 | Method for processing colored glazing glass with double colors pattern |
| CN103386852A (en) * | 2012-05-11 | 2013-11-13 | 佛山市南海中康亿美佳钢化玻璃有限公司 | Preparation method of decorative glass with three-dimensional pattern |
| CN105804335A (en) * | 2016-03-25 | 2016-07-27 | 沈阳首佳通用玻璃有限公司 | Gate plate type energy-saving switchable glass |
| CN106145637A (en) * | 2016-08-05 | 2016-11-23 | 湖北新华光信息材料有限公司 | A kind of chalcogenide glass surface printing method |
| CN106830697A (en) * | 2017-03-09 | 2017-06-13 | 曾志明 | A kind of method for preparing safety glass |
| CN106977111A (en) * | 2017-05-22 | 2017-07-25 | 陶圣香 | A kind of production method of environment-friendly type colored glazed glass |
| CN106986550A (en) * | 2017-04-27 | 2017-07-28 | 东莞市银泰玻璃有限公司 | A kind of making can secondary operation artistic glass processing technology |
| CN109896755A (en) * | 2019-04-17 | 2019-06-18 | 东方美涂(哈尔滨)科技有限公司 | A kind of multifunctional glass dalle and preparation method thereof |
| CN110835237A (en) * | 2019-05-14 | 2020-02-25 | 信义玻璃工程（东莞）有限公司 | Method for manufacturing firm color glazed glass and firm color glazed glass |
| CN112551913A (en) * | 2020-12-28 | 2021-03-26 | 广州美术学院 | Trepanning plate glass and preparation method and application thereof |
| CN113860755A (en) * | 2021-11-05 | 2021-12-31 | 安徽省华耀玻璃有限公司 | Continuous production process of colored glaze glass capable of automatically spraying colored glaze |
| CN114407571A (en) * | 2022-01-17 | 2022-04-29 | 蚌埠权盛机械制造有限公司 | Manufacturing process of high-temperature sintered glass decorative picture |
-
2009
- 2009-11-10 CN CN200910224711A patent/CN101704633A/en active Pending
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102260045A (en) * | 2010-03-18 | 2011-11-30 | 杨德宁 | Environment-friendly, energy-saving and low-melting-point color glaze decoration flat glass with high annealing temperature and strength and preparation method thereof |
| CN102730981A (en) * | 2011-04-15 | 2012-10-17 | 中航三鑫股份有限公司 | Method for processing colored glazing glass with double colors pattern |
| CN102730981B (en) * | 2011-04-15 | 2015-09-30 | 中航三鑫股份有限公司 | Double-colored pattern colored glazed glass working method |
| CN103386852A (en) * | 2012-05-11 | 2013-11-13 | 佛山市南海中康亿美佳钢化玻璃有限公司 | Preparation method of decorative glass with three-dimensional pattern |
| CN105804335A (en) * | 2016-03-25 | 2016-07-27 | 沈阳首佳通用玻璃有限公司 | Gate plate type energy-saving switchable glass |
| CN106145637A (en) * | 2016-08-05 | 2016-11-23 | 湖北新华光信息材料有限公司 | A kind of chalcogenide glass surface printing method |
| CN106145637B (en) * | 2016-08-05 | 2019-01-01 | 湖北新华光信息材料有限公司 | A kind of chalcogenide glass surface printing method |
| CN106830697A (en) * | 2017-03-09 | 2017-06-13 | 曾志明 | A kind of method for preparing safety glass |
| CN106986550A (en) * | 2017-04-27 | 2017-07-28 | 东莞市银泰玻璃有限公司 | A kind of making can secondary operation artistic glass processing technology |
| CN106977111A (en) * | 2017-05-22 | 2017-07-25 | 陶圣香 | A kind of production method of environment-friendly type colored glazed glass |
| CN109896755A (en) * | 2019-04-17 | 2019-06-18 | 东方美涂(哈尔滨)科技有限公司 | A kind of multifunctional glass dalle and preparation method thereof |
| CN109896755B (en) * | 2019-04-17 | 2022-07-01 | 东方美涂(哈尔滨)科技有限公司 | Multifunctional glass decorative plate and preparation method thereof |
| CN110835237A (en) * | 2019-05-14 | 2020-02-25 | 信义玻璃工程（东莞）有限公司 | Method for manufacturing firm color glazed glass and firm color glazed glass |
| CN112551913A (en) * | 2020-12-28 | 2021-03-26 | 广州美术学院 | Trepanning plate glass and preparation method and application thereof |
| CN113860755A (en) * | 2021-11-05 | 2021-12-31 | 安徽省华耀玻璃有限公司 | Continuous production process of colored glaze glass capable of automatically spraying colored glaze |
| CN114407571A (en) * | 2022-01-17 | 2022-04-29 | 蚌埠权盛机械制造有限公司 | Manufacturing process of high-temperature sintered glass decorative picture |
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Application publication date: 20100512 |