CN104139434A - Sterilizing and color fixing soak solution for salix integra woven material and using method thereof - Google Patents
Sterilizing and color fixing soak solution for salix integra woven material and using method thereof Download PDFInfo
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- CN104139434A CN104139434A CN201410278757.7A CN201410278757A CN104139434A CN 104139434 A CN104139434 A CN 104139434A CN 201410278757 A CN201410278757 A CN 201410278757A CN 104139434 A CN104139434 A CN 104139434A
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Abstract
The invention relates to the field of modified treatment on materials for weaving artworks and particularly relates to a sterilizing and color fixing soak solution for a salix integra woven material and a using method of the sterilizing and color fixing soak solution. The sterilizing and color fixing soak solution is prepared from raw materials in parts by weight: 2-4 parts of D-sodium erythorbate, 6-8 parts of glycerin, 2-3 parts of madder, 0.5-1 part of safflower, 7-8 parts of sodium hypophosphite, 15-18 parts of polyethylenimine, a proper amount of sodium hydroxide, 250-280 parts of water and 4-5 parts of adjuvant. The raw materials of the soak solution provided by the invention are all environmental-friendly components, do not contain volatile toxic organic matter, components such as sodium hypophosphite, polyethyleneimine, glycerin, can be used for improving the mechanical property of salix integra, enhancing the toughness and strength, improving the dimensional stability and improving the color fastness of pigment and simultaneously has corrosion prevention and sterilization effects; due to the adoption of the natural pigment extracted from the madder and the safflower, the material has a noble and elegant color; and the preparation and using methods of the soak solution, which are disclosed by the invention, are simple, the waste liquid is simple in recycling and treatment; the modified salix integra woven product is not easily mildewed and damaged by insects and is unique and lasting in color and luster, durable in use and high in ornamental value.
Description
Technical field
The present invention relates to baskets craft material modification process field, be specifically related to sterilization fixation soak and using method thereof for a kind of purple willow braided material.
Background technology
The handicraft that the natural establishment material such as rattan, wicker, bamboo cane, all kinds of stalks is made has high viewing and admiring and practical value, and product is found a good sale in both at home and abroad, and the utmost point is liked by consumer, and market potential is huge.Due to their biological speciality, there is inflammable, the shortcoming such as rotten of easily splitting, easily damage by worms, need in actual use to carry out a series of modification, to improve its mechanical property and physicochemical property, make it more easily process and transport storage, improve ornamental value and Practical Performance, conventional processing means are to adopt modification liquid to material immersion treatment, therefore, the preparation of modification liquid is particularly important, and desirable modification liquid need to possess that environment-protecting asepsis, modified effect are lasting, the feature such as do not affect the appearance.
Summary of the invention
The object of the invention is to provide sterilization fixation soak and using method thereof for a kind of purple willow braided material, to improve the processing characteristics of purple willow, promotes and views and admires and practical value, and to achieve these goals, the technical solution used in the present invention is as follows:
Sterilization fixation soak and using method thereof for a kind of purple willow braided material, it is characterized in that, this soak is made by the raw material of following weight portion: D-araboascorbic acid sodium 2-4, glycerine 6-8, madder 2-3, safflower 0.5-1, inferior sodium phosphate 7-8, polymine 15-18, NaOH are appropriate, water 250-280, auxiliary agent 4-5;
Auxiliary agent is made by the raw material of following weight portion: sodium hypophosphite 10-12, Sodium Hyaluronate 2-3, metasilicic acid 4-5, D-sorbite 5-6, yellow rice wine 12-15, tea tree ethereal oil 1-2, Tween 80 1-2, its preparation method is: first Tween 80 is mixed with yellow rice wine, being stirred to it dissolves completely, add again tea tree ethereal oil, after dispersed with stirring 20-30min, add transparent sodium phytate, D-sorbite, continue to stir 15-20min, finally add other leftover materials, stir 30-40min, make paste, obtain auxiliary agent.
Described sterilization fixation soak and using method thereof for a kind of purple willow braided material, its preparation method is:
(1) after madder, safflower clean dry, pulverize, mix with 50 parts of water, and add the NaOH of 0.05 weight portion, stir after 10-15min, material ball milling 1-2h, ball milling finishes to filter after rear standing immersion 5-6h, gets filtrate for later use;
(2) excess water is heated to 50-60 ℃, add D-araboascorbic acid sodium, inferior sodium phosphate, polymine, after being stirred to material and dissolving completely, add again step (1) gained filtrate and other leftover materials except NaOH, keep 50-60 ℃ of temperature, continue to be uniformly mixed 30-40min, finally add appropriate NaOH, regulator solution pH value is 7.5-8.0, obtains soak.
Described sterilization fixation soak and using method thereof for a kind of purple willow braided material, its using method is: purple willow braided material is submerged in above-mentioned soak completely, be incubated airtight immersion 18-20h, take out the clean nature of clear water and dry or dry.
Soak advantage of the present invention is: first, its raw material adopting is environmental protection composition,, containing volatility toxic organic compound composition, does not pollute environment for use; Secondly, the active ingredients such as the inferior sodium phosphate in raw material, polymine, glycerine can be improved the mechanical property of purple willow, promote toughness and intensity, improve dimensional stability, improve the firm coloration degree of pigment, have antisepsis and sterilization effect concurrently; Madder and safflower grind and obtain natural red dyestuff in alkaline solution, give the color and luster of material elegant, avoid the use of organic dyestuff.Soak preparation method of the present invention and using method are simple, solution chemistry stable performance, and waste liquid recycling is simple, the easier machine-shaping of purple willow braided material after processing, process is time saving and energy saving, and product is difficult for mould corruption, color and luster is unique lasting, places for a long time indeformablely, and ornamental value is high.
The specific embodiment
Embodiment
The soak of the present embodiment by following weight portion (kilogram) raw material make: D-araboascorbic acid sodium 3, glycerine 8, madder 3, safflower 0.5, inferior sodium phosphate 8, polymine 18, NaOH are appropriate, water 280, auxiliary agent 5; Auxiliary agent is made by the raw material of following weight portion: sodium hypophosphite 12, Sodium Hyaluronate 3, metasilicic acid 5, D-sorbite 5, yellow rice wine 15, tea tree ethereal oil 1, Tween 80 2, its preparation method is: first Tween 80 is mixed with yellow rice wine, be stirred to it and dissolve completely, then add tea tree ethereal oil, after dispersed with stirring 30min, add transparent sodium phytate, D-sorbite, continue to stir 20min, finally add other leftover materials, stir 40min, make paste, obtain auxiliary agent.
The soak preparation method of the present embodiment is:
(1) after madder, safflower clean dry, pulverize, mix with 50 parts of water, and add the NaOH of 0.05 weight portion, stir after 15min, material ball milling 1.5h, ball milling finishes to filter after rear standing immersion 6h, gets filtrate for later use;
(2) excess water is heated to 50-60 ℃, add D-araboascorbic acid sodium, inferior sodium phosphate, polymine, after being stirred to material and dissolving completely, add again step (1) gained filtrate and other leftover materials except NaOH, keep 50-60 ℃ of temperature, continue to be uniformly mixed 40min, finally add appropriate NaOH, regulator solution pH value is 7.8, obtains soak.
Pretreated purple willow braided material is submerged in above-mentioned soak completely, be incubated airtight immersion 20h, take out the clean nature of clear water and dry or dry, then carry out subsequent handling.Purple willow impact strength after soak of the present invention is processed increases by 19.5% compared with the material of conventional process, bending strength improves 24.6%, easier during braiding, time saving and energy saving, product average production time reduces by 12.3%, and product is placed more than 1 year without problems such as variable color, rotten moth, crackles.
Claims (3)
1. sterilization fixation soak and using method thereof for a purple willow braided material, it is characterized in that, this soak is made by the raw material of following weight portion: D-araboascorbic acid sodium 2-4, glycerine 6-8, madder 2-3, safflower 0.5-1, inferior sodium phosphate 7-8, polymine 15-18, NaOH are appropriate, water 250-280, auxiliary agent 4-5;
Auxiliary agent is made by the raw material of following weight portion: sodium hypophosphite 10-12, Sodium Hyaluronate 2-3, metasilicic acid 4-5, D-sorbite 5-6, yellow rice wine 12-15, tea tree ethereal oil 1-2, Tween 80 1-2, its preparation method is: first Tween 80 is mixed with yellow rice wine, being stirred to it dissolves completely, add again tea tree ethereal oil, after dispersed with stirring 20-30min, add transparent sodium phytate, D-sorbite, continue to stir 15-20min, finally add other leftover materials, stir 30-40min, make paste, obtain auxiliary agent.
2. sterilization fixation soak and using method thereof for a kind of purple willow braided material as claimed in claim 1, its preparation method is:
(1) after madder, safflower clean dry, pulverize, mix with 50 parts of water, and add the NaOH of 0.05 weight portion, stir after 10-15min, material ball milling 1-2h, ball milling finishes to filter after rear standing immersion 5-6h, gets filtrate for later use;
(2) excess water is heated to 50-60 ℃, add D-araboascorbic acid sodium, inferior sodium phosphate, polymine, after being stirred to material and dissolving completely, add again step (1) gained filtrate and other leftover materials except NaOH, keep 50-60 ℃ of temperature, continue to be uniformly mixed 30-40min, finally add appropriate NaOH, regulator solution pH value is 7.5-8.0, obtains soak.
3. sterilization fixation soak and using method thereof for a kind of purple willow braided material as claimed in claim 1, its using method is: purple willow braided material is submerged in above-mentioned soak completely, be incubated airtight immersion 18-20h, take out the clean nature of clear water and dry or dry.
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| CN201410278757.7A CN104139434A (en) | 2014-06-21 | 2014-06-21 | Sterilizing and color fixing soak solution for salix integra woven material and using method thereof |
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| CN201410278757.7A CN104139434A (en) | 2014-06-21 | 2014-06-21 | Sterilizing and color fixing soak solution for salix integra woven material and using method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104924400A (en) * | 2015-06-01 | 2015-09-23 | 阜南县腾博工艺品有限公司 | Corn leaf color fixation treatment method |
| CN104942952A (en) * | 2015-06-01 | 2015-09-30 | 阜南县腾博工艺品有限公司 | Corn leaf color fixing treatment agent |
| CN105291221A (en) * | 2015-10-30 | 2016-02-03 | 阜南县永兴工艺品有限公司 | Bactericidal mildew-proof wicker treatment agent and preparation method thereof |
| CN105365012A (en) * | 2015-11-04 | 2016-03-02 | 阜南县铭钰柳木工艺品有限公司 | Toughening and strengthening pretreating agent for wicker for wickerwork and preparation method of toughening and strengthening pretreating agent |
| CN105368235A (en) * | 2015-10-30 | 2016-03-02 | 阜南县大自然工艺品有限公司 | High gloss anti-aging wicker treating agent and preparation method thereof |
| CN105368240A (en) * | 2015-10-30 | 2016-03-02 | 阜南县大自然工艺品有限公司 | Insect-proofing and moth-proofing wicker treating agent and preparation method thereof |
| CN105400355A (en) * | 2015-10-30 | 2016-03-16 | 阜南县大自然工艺品有限公司 | Air purification wicker treating agent and preparation method thereof |
| CN106182287A (en) * | 2016-07-28 | 2016-12-07 | 安徽信达家居有限公司 | A kind of wicker plaiting article the high-performance coloring agent of purple willow and using method thereof |
| CN106217564A (en) * | 2016-08-31 | 2016-12-14 | 安徽阜南县万家和工艺品有限公司 | A kind of inorganic agent being easy to the dyeing of wicker knitting |
| CN107571367A (en) * | 2017-09-25 | 2018-01-12 | 阜南县大自然工艺品有限公司 | A kind of cogongrass pretreatment soak for the braiding of straw plaited basket |
| CN108015870A (en) * | 2017-12-15 | 2018-05-11 | 霍山县宇顺竹制品有限公司 | A kind of processing method before mao bamboon processing |
| CN108741340A (en) * | 2018-06-26 | 2018-11-06 | 阜南县星光工艺品有限公司 | A kind of preparation method for not removing the peel withy dried flower |
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| JP2001158008A (en) * | 1999-12-02 | 2001-06-12 | Takeda Chem Ind Ltd | Wood preservative |
| JP2005349625A (en) * | 2004-06-09 | 2005-12-22 | Nippon Shokubai Co Ltd | Water soluble wood preservative improved in permeability |
| CN102092068A (en) * | 2010-11-23 | 2011-06-15 | 孟祥荣 | Willow weaving raw material wicker and oak bark dip treating agent and using method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104924400A (en) * | 2015-06-01 | 2015-09-23 | 阜南县腾博工艺品有限公司 | Corn leaf color fixation treatment method |
| CN104942952A (en) * | 2015-06-01 | 2015-09-30 | 阜南县腾博工艺品有限公司 | Corn leaf color fixing treatment agent |
| CN105291221A (en) * | 2015-10-30 | 2016-02-03 | 阜南县永兴工艺品有限公司 | Bactericidal mildew-proof wicker treatment agent and preparation method thereof |
| CN105368235A (en) * | 2015-10-30 | 2016-03-02 | 阜南县大自然工艺品有限公司 | High gloss anti-aging wicker treating agent and preparation method thereof |
| CN105368240A (en) * | 2015-10-30 | 2016-03-02 | 阜南县大自然工艺品有限公司 | Insect-proofing and moth-proofing wicker treating agent and preparation method thereof |
| CN105400355A (en) * | 2015-10-30 | 2016-03-16 | 阜南县大自然工艺品有限公司 | Air purification wicker treating agent and preparation method thereof |
| CN105365012A (en) * | 2015-11-04 | 2016-03-02 | 阜南县铭钰柳木工艺品有限公司 | Toughening and strengthening pretreating agent for wicker for wickerwork and preparation method of toughening and strengthening pretreating agent |
| CN106182287A (en) * | 2016-07-28 | 2016-12-07 | 安徽信达家居有限公司 | A kind of wicker plaiting article the high-performance coloring agent of purple willow and using method thereof |
| CN106217564A (en) * | 2016-08-31 | 2016-12-14 | 安徽阜南县万家和工艺品有限公司 | A kind of inorganic agent being easy to the dyeing of wicker knitting |
| CN107571367A (en) * | 2017-09-25 | 2018-01-12 | 阜南县大自然工艺品有限公司 | A kind of cogongrass pretreatment soak for the braiding of straw plaited basket |
| CN108015870A (en) * | 2017-12-15 | 2018-05-11 | 霍山县宇顺竹制品有限公司 | A kind of processing method before mao bamboon processing |
| CN108741340A (en) * | 2018-06-26 | 2018-11-06 | 阜南县星光工艺品有限公司 | A kind of preparation method for not removing the peel withy dried flower |
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Application publication date: 20141112 |