CN104131294A - 一种具有抗菌效果的铝及铝合金混合抛光液及其制备方法 - Google Patents
一种具有抗菌效果的铝及铝合金混合抛光液及其制备方法 Download PDFInfo
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- 238000005498 polishing Methods 0.000 title claims abstract description 23
- 229910000838 Al alloy Inorganic materials 0.000 title claims abstract description 15
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 239000004411 aluminium Substances 0.000 title claims abstract description 13
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 13
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- REZZEXDLIUJMMS-UHFFFAOYSA-M dimethyldioctadecylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC REZZEXDLIUJMMS-UHFFFAOYSA-M 0.000 claims abstract description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 7
- ZMZNLKYXLARXFY-UHFFFAOYSA-H cerium(3+);oxalate Chemical compound [Ce+3].[Ce+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O ZMZNLKYXLARXFY-UHFFFAOYSA-H 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 4
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 4
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004202 carbamide Substances 0.000 claims abstract description 4
- OSPSWZSRKYCQPF-UHFFFAOYSA-N dibutoxy(oxo)phosphanium Chemical compound CCCCO[P+](=O)OCCCC OSPSWZSRKYCQPF-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229940041616 menthol Drugs 0.000 claims abstract description 4
- RCIVOBGSMSSVTR-UHFFFAOYSA-L stannous sulfate Chemical compound [SnH2+2].[O-]S([O-])(=O)=O RCIVOBGSMSSVTR-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910000375 tin(II) sulfate Inorganic materials 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 10
- 239000004664 distearyldimethylammonium chloride (DHTDMAC) Substances 0.000 claims description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 6
- 229920002785 Croscarmellose sodium Polymers 0.000 claims description 6
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 6
- 229960001681 croscarmellose sodium Drugs 0.000 claims description 6
- 235000010947 crosslinked sodium carboxy methyl cellulose Nutrition 0.000 claims description 6
- 239000003995 emulsifying agent Substances 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 4
- CBBPCTUZWQXJDG-UHFFFAOYSA-N 2-(2-hydroxyethyl)tetradecanoic acid Chemical compound CCCCCCCCCCCCC(C(O)=O)CCO CBBPCTUZWQXJDG-UHFFFAOYSA-N 0.000 claims description 3
- -1 Lauryl Alcohol ester Chemical class 0.000 claims description 3
- 229960000583 acetic acid Drugs 0.000 claims description 3
- 239000012362 glacial acetic acid Substances 0.000 claims description 3
- 235000019353 potassium silicate Nutrition 0.000 claims description 3
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 238000005260 corrosion Methods 0.000 abstract description 3
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- 229910052751 metal Inorganic materials 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- NRADEFPIEBTIED-UHFFFAOYSA-N 1-(2-tridecyl-4,5-dihydroimidazol-1-yl)ethanol Chemical compound CCCCCCCCCCCCCC1=NCCN1C(C)O NRADEFPIEBTIED-UHFFFAOYSA-N 0.000 abstract 1
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 abstract 1
- 241000894006 Bacteria Species 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
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- 229960001759 cerium oxalate Drugs 0.000 abstract 1
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- 239000000176 sodium gluconate Substances 0.000 abstract 1
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Abstract
本发明公开了一种具有抗菌效果的铝及铝合金混合抛光液，其特征在于，由下列重量份的原料制成：草酸铈9-11、双十八烷基二甲基氯化铵3-5、羟乙基肉豆蔻酸咪唑啉4-6、亚磷酸二正丁酯1.5-2、薄荷醇2-3、硫酸亚锡0.7-1.5、葡萄糖酸钠2-3、冰醋酸4-6、尿素3-5、助剂5-7、去离子水300；本发明添加双十八烷基二甲基氯化铵，既有抗菌功效又可以在铝合金加工表面形成易吸附的表层，以及助剂的添加，在可以在金属表面形成一层保护膜，可以阻止空气腐蚀金属表面；本发明混合抛光液抗菌防腐蚀，抛光性能优良，表面光亮，而且抛光液为水基材质，能大幅降低抛光时摩擦产生的温度，起到冷却的效果。
Description
技术领域
本发明涉及表面处理技术领域，特别是一种具有抗菌效果的铝及铝合金混合抛光液及其制备方法。
背景技术
铝及铝合金化学抛光的方法应用比较广泛，但是存在的最大的缺点是由于抛光液温度高，反应快，在自动线上生产时，一个工位到下一个工位所需时间长，造成工件从化学抛光槽出来后，携带大量残留化学抛光药水而停留在空中，在残液下流、低落的过程中同时由于空气的存在对表面产生过腐蚀、氧化在表面形成异色等，而且由于抛光液含有混合油状物，容易产生腐败变质形象，从而影响了产品品质。
发明内容
本发明的目的是提供一种具有抗菌效果的铝及铝合金混合抛光液及其制备方法。
为了实现本发明的目的，本发明通过以下方案实施：
一种具有抗菌效果的铝及铝合金混合抛光液，由下列重量份的原料制成：草酸铈9-11、双十八烷基二甲基氯化铵3-5、羟乙基肉豆蔻酸咪唑啉4-6、亚磷酸二正丁酯1.5-2、薄荷醇2-3、硫酸亚锡0.7-1.5、葡萄糖酸钠2-3、冰醋酸4-6、尿素3-5、助剂5-7、去离子水300；
所述助剂由以下重量份的原料制成：三氧化二铝4-6、纳米二氧化钛5-7、硅酸钠1-2、丙二醇甲醚醋酸酯3-4、十二碳醇酯2-3、丙烯酸甲酯2-4、交联羧甲基纤维素钠2-3、乳化剂BP4-5、水50-54；制备方法是首先将三氧化二铝、纳米二氧化钛、交联羧甲基纤维素钠、乳化剂BP加入一半量的水中，研磨1-2小时，然后缓慢加入其余剩余成分，缓慢加热至70℃-80℃，在300-500转/分条件下搅拌反应30-50分钟，冷却至室温即得。
本发明所述一种具有抗菌效果的铝及铝合金混合抛光液，由以下具体步骤制成：
(1)将草酸铈、双十八烷基二甲基氯化铵混合均匀，加入适量的去离子水，加热至30℃-35℃，研磨25-35分钟，得到混合A料；
（2）将除助剂之外的其余剩余成分加入到反应釜中，搅拌混合均匀，缓慢加热至35℃-45℃，保温1-1.5小时，得到混合B料；
（3）将保温的混合B料边搅拌边缓慢加入到混合A料中，充分搅拌后加入助剂，继续搅拌25-35分钟，冷却至室温即得。
本发明的优异效果是：本发明添加双十八烷基二甲基氯化铵，既有抗菌功效又可以在铝合金加工表面形成易吸附的表层，以及助剂的添加，在可以在金属表面形成一层保护膜，可以阻止空气腐蚀金属表面；本发明混合抛光液抗菌防腐蚀，抛光性能优良，表面光亮，而且抛光液为水基材质，能大幅降低抛光时摩擦产生的温度，起到冷却的效果。
具体实施方式
下面通过具体实例对本发明进行详细说明。
一种具有抗菌效果的铝及铝合金混合抛光液，由下列重量份（公斤）的原料制成：草酸铈9、双十八烷基二甲基氯化铵3、羟乙基肉豆蔻酸咪唑啉4、亚磷酸二正丁酯1.5、薄荷醇2、硫酸亚锡0.7、葡萄糖酸钠2、冰醋酸4、尿素3、助剂5、去离子水300；
所述助剂由以下重量份（公斤）的原料制成：三氧化二铝4、纳米二氧化钛5、硅酸钠1、丙二醇甲醚醋酸酯3、十二碳醇酯2、丙烯酸甲酯2、交联羧甲基纤维素钠2、乳化剂BP4、水50；制备方法是首先将三氧化二铝、纳米二氧化钛、交联羧甲基纤维素钠、乳化剂BP加入一半量的水中，研磨1-2小时，然后缓慢加入其余剩余成分，缓慢加热至70℃-80℃，在300-500转/分条件下搅拌反应30-50分钟，冷却至室温即得。
本发明所述一种具有抗菌效果的铝及铝合金混合抛光液，由以下具体步骤制成：
(1)将草酸铈、双十八烷基二甲基氯化铵混合均匀，加入适量的去离子水，加热至30℃-35℃，研磨25-35分钟，得到混合A料；
（2）将除助剂之外的其余剩余成分加入到反应釜中，搅拌混合均匀，缓慢加热至35℃-45℃，保温1-1.5小时，得到混合B料；
（3）将保温的混合B料边搅拌边缓慢加入到混合A料中，充分搅拌后加入助剂，继续搅拌25-35分钟，冷却至室温即得。
实验检测结果：肉眼观察各铝合金工件的表面，工件表面外观均匀、无异色或有轻微色差、且无雪花；采用微型光泽仪A-4430（德国BYK公司）测试各抛光铝合金工件表面的光泽度，光泽度为50Gu。
Claims (2)
1.一种具有抗菌效果的铝及铝合金混合抛光液，其特征在于，由下列重量份的原料制成：草酸铈9-11、双十八烷基二甲基氯化铵3-5、羟乙基肉豆蔻酸咪唑啉4-6、亚磷酸二正丁酯1.5-2、薄荷醇2-3、硫酸亚锡0.7-1.5、葡萄糖酸钠2-3、冰醋酸4-6、尿素3-5、助剂5-7、去离子水300；
所述助剂由以下重量份的原料制成：三氧化二铝4-6、纳米二氧化钛5-7、硅酸钠1-2、丙二醇甲醚醋酸酯3-4、十二碳醇酯2-3、丙烯酸甲酯2-4、交联羧甲基纤维素钠2-3、乳化剂BP4-5、水50-54；制备方法是首先将三氧化二铝、纳米二氧化钛、交联羧甲基纤维素钠、乳化剂BP加入一半量的水中，研磨1-2小时，然后缓慢加入其余剩余成分，缓慢加热至70℃-80℃，在300-500转/分条件下搅拌反应30-50分钟，冷却至室温即得。
2.根据权利要求1所述一种具有抗菌效果的铝及铝合金混合抛光液，其特征在于，由以下具体步骤制成：
(1)将草酸铈、双十八烷基二甲基氯化铵混合均匀，加入适量的去离子水，加热至30℃-35℃，研磨25-35分钟，得到混合A料；
（2）将除助剂之外的其余剩余成分加入到反应釜中，搅拌混合均匀，缓慢加热至35℃-45℃，保温1-1.5小时，得到混合B料；
（3）将保温的混合B料边搅拌边缓慢加入到混合A料中，充分搅拌后加入助剂，继续搅拌25-35分钟，冷却至室温即得。
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3464870A (en) * | 1965-06-25 | 1969-09-02 | North American Aluminum Corp | Aluminum polishing process |
| JPS55113883A (en) * | 1979-02-26 | 1980-09-02 | Yoshimitsu Takahashi | Al same alloy chemical polishing composition of alkaline bath |
| CN1031574A (zh) * | 1987-06-19 | 1989-03-08 | 北京航空学院 | 铝及铝合金碱性化学抛光溶液 |
| US20060130936A1 (en) * | 2002-09-09 | 2006-06-22 | Magnesum Technolgy Limited | Surface treatment of magnesium and its alloys |
| CN101368272A (zh) * | 2007-08-15 | 2009-02-18 | 江苏海迅实业集团股份有限公司 | 铝及铝合金材料抛光液 |
| CN102925900A (zh) * | 2012-10-19 | 2013-02-13 | 贵州航天林泉电机有限公司 | 一种碱性化学抛光液及碱性化学抛光方法 |
| CN103334107A (zh) * | 2013-05-21 | 2013-10-02 | 内蒙古包钢钢联股份有限公司 | 镁铝合金抛光液、制备方法及其抛光方法 |
-
2014
- 2014-07-01 CN CN201410308663.XA patent/CN104131294B/zh active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3464870A (en) * | 1965-06-25 | 1969-09-02 | North American Aluminum Corp | Aluminum polishing process |
| JPS55113883A (en) * | 1979-02-26 | 1980-09-02 | Yoshimitsu Takahashi | Al same alloy chemical polishing composition of alkaline bath |
| CN1031574A (zh) * | 1987-06-19 | 1989-03-08 | 北京航空学院 | 铝及铝合金碱性化学抛光溶液 |
| US20060130936A1 (en) * | 2002-09-09 | 2006-06-22 | Magnesum Technolgy Limited | Surface treatment of magnesium and its alloys |
| CN101368272A (zh) * | 2007-08-15 | 2009-02-18 | 江苏海迅实业集团股份有限公司 | 铝及铝合金材料抛光液 |
| CN102925900A (zh) * | 2012-10-19 | 2013-02-13 | 贵州航天林泉电机有限公司 | 一种碱性化学抛光液及碱性化学抛光方法 |
| CN103334107A (zh) * | 2013-05-21 | 2013-10-02 | 内蒙古包钢钢联股份有限公司 | 镁铝合金抛光液、制备方法及其抛光方法 |
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