CN104031403A - Method for preparing tender maple leaf natural dyestuff and application thereof - Google Patents
Method for preparing tender maple leaf natural dyestuff and application thereof Download PDFInfo
- Publication number
- CN104031403A CN104031403A CN201410269204.5A CN201410269204A CN104031403A CN 104031403 A CN104031403 A CN 104031403A CN 201410269204 A CN201410269204 A CN 201410269204A CN 104031403 A CN104031403 A CN 104031403A
- Authority
- CN
- China
- Prior art keywords
- dyestuff
- folium evodiae
- evodiae trichotomae
- tender folium
- tender
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Coloring (AREA)
Abstract
The invention relates to a method for preparing a tender maple leaf natural dyestuff and application thereof. The preparation method comprises the following steps: (1) cleaning the collected tender maple leaves by using clear water, drying in the air and mechanically grinding to obtain tender maple leaf powder; (2) adding the tender maple leaf powder into an aqueous solution of ethanol with the pH value of 8-10, stirring with a wooden stick and standing; (3) performing reflux extraction, raising the temperature of the extracting solution to 75-95 DEG C, and filtering; and (4) obtaining the concentrated tender maple leaf natural dyestuff by utilizing a reduced-pressure distillation method. The environmental pollution is avoided in the process of extracting the concentrated tender maple leaf natural dyestuff; the dyed fabric is soft in touch and safe to wear, carcinogenic and teratogenetic response is avoided, and damage of dyes on the fabric to infants is not needed to be worried after the fabric is put on infants, and the tender maple leaves are abundant, can be extracted simply and is stable in quality.
Description
Technical field
The present invention relates to natural dyestuff and applied field thereof, particularly a kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof.
Background technology
Now society no matter be science and technology or social economy all in develop rapidly, people's standard of living is constantly improving, the quality of life is also in the variation that matter occurs, the health that increasing people not only eats hope, that wears also wants healthy.But what in life, wear is nearly all the dyestuff of chemosynthesis, this dyestuff not only in the process of being produced to the Nature, people's health is damaged, after textile dyeing, it is unnatural that the color and luster of fabric seems, it is also very uncomfortable that people wear, particularly infant, what they like taking just toward putting in the mouth, very dangerous.
Summary of the invention
The object of the invention is in order to overcome above deficiency, a kind of preparation method and application thereof of tender Folium Evodiae trichotomae natural dyestuff are provided, the present invention can effectively utilize natural resources, not pollute in preparation process, very economical and practical, and applied fabric color nature, healthy practical, there is anti-microbial property.
Technical scheme provided by the invention is: a kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff, comprises the following steps:
(1) utilize clear water to clean, dry the tender Folium Evodiae trichotomae of collecting, utilize machinery that the tender Folium Evodiae trichotomae drying is pulverized and obtained tender Folium Evodiae trichotomae powder;
(2) tender Folium Evodiae trichotomae powder is joined concentration of volume percent be 40～80% and the aqueous ethanolic solution of pH value 8～10 in, the mass ratio of tender Folium Evodiae trichotomae powder and aqueous ethanolic solution is 1:10～50, leaves standstill 3～5 minutes after utilizing wooden stick to stir;
(3) carry out refluxing extraction, extracting solution is warmed up to 75～95 DEG C, insulation 30～90min, filters also;
(4) utilize the method for underpressure distillation to make the liquid volume after filtration be concentrated to 1/5～1/3 of original volume, the tender Folium Evodiae trichotomae natural dyestuff that obtains concentrating.
Further improve and be, the invention provides a kind of method of aforementioned tender Folium Evodiae trichotomae natural dyestuff to fabric substantive dyeing of utilizing, comprise step:
(1) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:10～60, and dyestuff pH value is adjusted to 7～8;
(2) thing to be dyed of real silk or wool material is put in water and soaked into, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50～60 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:20～60, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff;
(3), after having dyeed, washing, dries.
Further improve and be, the invention provides and a kind ofly utilize aforementioned tender Folium Evodiae trichotomae natural dyestuff application to carry out the method for antimicrobial treatment for fabric, comprise the following steps:
(1) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:20～40, and dyestuff pH value is adjusted to 7.5～8;
(2) thing to be dyed of real silk or wool material is put in water and soaked into, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50～60 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:20～60, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff;
(3), after having dyeed, washing, dries.
The invention has the advantages that: the present invention extracts natural dyestuff from tender Folium Evodiae trichotomae, and real silk, wool fabric are dyeed, colour fastness is high, and dye uptake is high, and color and luster is naturally characteristic, and natural environmental protection; Real silk, wool fabric after the dyeing of tender maple leaf has excellent germ resistance streptococcus aureus, colibacillary bacteriostasis rate reached respectively to 90.95%, 85.72% simultaneously.The leaching process of whole tender Folium Evodiae trichotomae dyestuff can not shine into environmental pollution; Fabric touch after dyeing is soft, wears safety, does not have reaction carcinogenic, teratogenesis, after infant's dress, no longer needs to worry the injury of dyestuff to child on fabric; And tender Folium Evodiae trichotomae abundant raw material, extract simply steady quality.
embodiment:
Embodiment 1:
Tender Folium Evodiae trichotomae is cleaned, dried, mechanical disintegration, take 1 kilogram, powder, be 10 by 50 kilograms of pH values 40% aqueous ethanolic solution, after stirring, at 95 DEG C of temperature, soak into 30min, after filtration, remove solid matter, liquid after filtration carries out underpressure distillation and is concentrated into 5 liters, is tender Folium Evodiae trichotomae natural dyestuff.
Embodiment 2:
Tender Folium Evodiae trichotomae is cleaned, dried, mechanical disintegration, take 1 kilogram, powder, be 8 by 10 kilograms of pH values 80% aqueous ethanolic solution, after stirring, at 75 DEG C of temperature, soak into 90min, after filtration, remove solid matter, liquid after filtration carries out underpressure distillation and is concentrated into 10 liters, is tender Folium Evodiae trichotomae natural dyestuff.
Embodiment 3:
Tender Folium Evodiae trichotomae is cleaned, dried, mechanical disintegration, take 1 kilogram, powder, be 9 by 30 kilograms of pH values 80% aqueous ethanolic solution, after stirring, at 85 DEG C of temperature, soak into 45min, after filtration, remove solid matter, liquid after filtration carries out underpressure distillation and is concentrated into 5 liters, is tender Folium Evodiae trichotomae natural dyestuff.
Embodiment 4:
(1) thing to be dyed of real silk material is put in water and soaked into, taking-up is directly extracted stand-by;
(2) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:60, and dyestuff pH value is adjusted to 7, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:60, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff, after having dyeed, washing, dries.
(3) above-mentioned dyeing sample is oyster.
Embodiment 5:
(1) thing to be dyed of real silk material is put in water and soaked into, taking-up is directly extracted stand-by;
(2) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:40, and dyestuff pH value is adjusted to 7.5, control the temperature of tender Folium Evodiae trichotomae dyestuff at 55 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:40, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff, after having dyeed, washing, dries.
(3) above-mentioned dyeing sample is yellow-green colour.
Embodiment 6:
(1) thing to be dyed of real silk material is put in water and soaked into, taking-up is directly extracted stand-by;
(2) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:10, and dyestuff pH value is adjusted to 8, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:20, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff, after having dyeed, washing, dries.
(3) above-mentioned dyeing sample is dark yellow-green.
Embodiment 7:
(1) thing to be dyed of real silk material is put in water and soaked into, taking-up is directly extracted stand-by;
(2) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:40, and dyestuff pH value is adjusted to 8, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:20, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff, after having dyeed, washing, dries.
(3), with reference to E2149-01 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record DYED FABRICS streptococcus aureus, colibacillary bacteriostasis rate are respectively to 92.10%, 86.35%.
Embodiment 8:
(1) thing to be dyed of real silk material is put in water and soaked into, taking-up is directly extracted stand-by;
(2) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:30, and dyestuff pH value is adjusted to 7.8, control the temperature of tender Folium Evodiae trichotomae dyestuff at 55 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:40, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff, after having dyeed, washing, dries.
(3), with reference to E2149-01 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record DYED FABRICS streptococcus aureus, colibacillary bacteriostasis rate are respectively to 93.05%, 87.65%.
Embodiment 9
(1) thing to be dyed of real silk material is put in water and soaked into, taking-up is directly extracted stand-by;
(2) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:20, and dyestuff pH value is adjusted to 7.5, control the temperature of tender Folium Evodiae trichotomae dyestuff at 60 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:60, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff, after having dyeed, washing, dries.
(3), with reference to E2149-01 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record DYED FABRICS streptococcus aureus, colibacillary bacteriostasis rate are respectively to 91.25%, 86.85%.
Claims (3)
1. a preparation method for tender Folium Evodiae trichotomae natural dyestuff, comprises the following steps:
(1) utilize clear water to clean, dry the tender Folium Evodiae trichotomae of collecting, utilize machinery that the tender Folium Evodiae trichotomae drying is pulverized and obtained tender Folium Evodiae trichotomae powder;
(2) tender Folium Evodiae trichotomae powder is joined concentration of volume percent be 40～80% and the aqueous ethanolic solution of pH value 8～10 in, the mass ratio of tender Folium Evodiae trichotomae powder and aqueous ethanolic solution is 1:10～50, leaves standstill 3～5 minutes after utilizing wooden stick to stir;
(3) carry out refluxing extraction, extracting solution is warmed up to 75～95 DEG C, insulation 30～90min, filters also;
(4) utilize the method for underpressure distillation to make the liquid volume after filtration be concentrated to 1/5～1/3 of original volume, the tender Folium Evodiae trichotomae natural dyestuff that obtains concentrating.
2. utilize the method for tender Folium Evodiae trichotomae natural dyestuff to fabric substantive dyeing described in claim 1, comprise step:
(1) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:10～60, and dyestuff pH value is adjusted to 7～8;
(2) thing to be dyed of real silk or wool material is put in water and soaked into, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50～60 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:20～60, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff;
(3), after having dyeed, washing, dries.
3. utilize tender Folium Evodiae trichotomae natural dyestuff application described in claim 1 to carry out the method for antimicrobial treatment for fabric, comprise the following steps:
(1) concentrated tender Folium Evodiae trichotomae natural dyestuff and the quality of water are hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:20～40, and dyestuff pH value is adjusted to 7.5～8;
(2) thing to be dyed of real silk or wool material is put in water and soaked into, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50～60 DEG C, taking-up puts it in the tender Folium Evodiae trichotomae dyestuff having mixed up after directly extracting, make the volume of thing to be dyed and the volume of tender Folium Evodiae trichotomae dyestuff be controlled at 1:20～60, thing whole to be dyed need to be placed 90min at tender Folium Evodiae trichotomae dyestuff;
(3), after having dyeed, washing, dries.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410269204.5A CN104031403B (en) | 2014-06-17 | 2014-06-17 | A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410269204.5A CN104031403B (en) | 2014-06-17 | 2014-06-17 | A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104031403A true CN104031403A (en) | 2014-09-10 |
| CN104031403B CN104031403B (en) | 2016-03-16 |
Family
ID=51462410
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410269204.5A Active CN104031403B (en) | 2014-06-17 | 2014-06-17 | A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104031403B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105011114A (en) * | 2015-06-29 | 2015-11-04 | 梁海林 | Preparation method of maple leaf concentrated solution |
| CN105088832A (en) * | 2015-09-22 | 2015-11-25 | 贵州省工程复合材料中心 | Low-temperature wool staining method |
| CN106235326A (en) * | 2016-07-21 | 2016-12-21 | 天峨县全盛蜂业科技有限公司 | The extracting method of a kind of Folium Alangii juice and application |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102454119A (en) * | 2010-10-18 | 2012-05-16 | 南通曙光染织有限公司 | Extraction of tea-leaf natural dye and dyeing method for silk broadcloth |
-
2014
- 2014-06-17 CN CN201410269204.5A patent/CN104031403B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102454119A (en) * | 2010-10-18 | 2012-05-16 | 南通曙光染织有限公司 | Extraction of tea-leaf natural dye and dyeing method for silk broadcloth |
Non-Patent Citations (6)
| Title |
|---|
| 姜平川: "枫叶黑色素理化性质研究", 《食品工业科技》 * |
| 李效文等: "枫香秋叶色素变化及与环境因子的关系", 《浙江农业科学》 * |
| 杨科家等: "元宝枫叶片花色素苷的提取及其稳定性研究", 《中国农学通报》 * |
| 胡敬志等: "枫香叶片色素含量变化及其与叶色变化的关系", 《西北农林科技大学学报(自然科学版)》 * |
| 蒋新龙: "枫香树叶红色素提取工艺研究", 《中国酿造》 * |
| 陈乃富: "红枫红色素的提取及其稳定性研究", 《天然产物研究与开发》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105011114A (en) * | 2015-06-29 | 2015-11-04 | 梁海林 | Preparation method of maple leaf concentrated solution |
| CN105088832A (en) * | 2015-09-22 | 2015-11-25 | 贵州省工程复合材料中心 | Low-temperature wool staining method |
| CN106235326A (en) * | 2016-07-21 | 2016-12-21 | 天峨县全盛蜂业科技有限公司 | The extracting method of a kind of Folium Alangii juice and application |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104031403B (en) | 2016-03-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106590018A (en) | Tobacco natural plant dye, preparation method, and application thereof | |
| CN103614933B (en) | It is a kind of to utilize the colouring method that cellulose fibre is contaminated on green peel of walnut natural dye | |
| CN1952020A (en) | Chestnut shell natural dye preparation and its uses | |
| CN104031403B (en) | A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof | |
| CN109750533B (en) | Plant-based light fastness improver and preparation method and application thereof | |
| CN103725032A (en) | Preparation method and application of natural lotus receptacle pigment | |
| CN104059382A (en) | Natural textile dye and preparation method thereof | |
| CN102061104A (en) | Method for extracting pigment used for real silk dyeing from purple potato | |
| CN105778556B (en) | A kind of violet dyes extracting method and tint applications | |
| CN104479397A (en) | Vaccinium bracteatum Thunb. plant dye extraction method | |
| CN102911517A (en) | Preparation method and usage of special tea dye for silk | |
| CN102604419B (en) | Method for preparing taro stem leaf vegetable dye and dyeing natural silk or wool by using taro stem leaf vegetable dye | |
| CN108948781A (en) | The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method | |
| CN104059380A (en) | Preparation and application of waxberry fruit natural dye | |
| CN105255213A (en) | Method for preparing natural dye through walnut green husk waste | |
| CN112252056A (en) | Wax printing color fixing method for vegetable natural dye | |
| CN106118128A (en) | Plant dye and the weaving material of this plant dye dyeing is prepared with Hebei Folium et Caulis Indigoferae Tinctoriae | |
| CN103966862A (en) | Method for dyeing short fiber yarn | |
| CN106118129A (en) | A kind of bronze-colored stain of knitting | |
| CN105544239A (en) | Bamboo fiber dyeing method based on natural mangosteen dye | |
| CN105754370A (en) | Natural textile dye and sound wave dyeing application thereof | |
| CN103526575A (en) | Process for dyeing fabric by using red sorghum pigment | |
| CN101532245B (en) | Method for extracting, from myrobalan, finishing agent having a function of removing formaldehyde, and applications thereof | |
| JPH01124691A (en) | Dyeing method by coloring matter in food | |
| CN102335112A (en) | Purely natural plant hair-dyeing cream |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |