CN106118129A - A kind of bronze-colored stain of knitting - Google Patents
A kind of bronze-colored stain of knitting Download PDFInfo
- Publication number
- CN106118129A CN106118129A CN201610549275.XA CN201610549275A CN106118129A CN 106118129 A CN106118129 A CN 106118129A CN 201610549275 A CN201610549275 A CN 201610549275A CN 106118129 A CN106118129 A CN 106118129A
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- CN
- China
- Prior art keywords
- knitting
- bronze
- ultrasonic
- flower
- colored
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0034—Mixtures of two or more pigments or dyes of the same type
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
Abstract
The invention discloses the bronze-colored stain of a kind of knitting, be made up of following raw material: Cortex Pini, chestnut shell, rapeseed meal, dry Folium paulowniae, Periostracum Serpentis shell, Folium Camelliae sinensis leftover bits and pieces, flower of poplar, leumus coccinea L. Var. Iutea corner, yellow Flos Lilii viriduli, Cassia surattensis flower, Flos kerriae japonicae, Fructus Mangifera Indicae, ginkgo nut.The bronze-colored stain of the knitting that the present invention provides, preparation is simple, extracts through pure natural plant raw material, cheap, and cost-effective 16.3%；According to brown and the characteristic of yellow plant, extract brown and yellow respectively, and carry out color and luster collocation according to three primary colors collocation principle, the most quickly, obtain natural bronze-colored；Only ultrasonic in the aqueous solution of stain need to soak in short-term during dyeing, improve work efficiency, even dyeing, pure color; colour-fast, anti-mould and anti-moth, it is simple to storage, extend using period; without any toxic reagent, safety and environmental protection, there is health care and plant flavour, protect health.
Description
Technical field
The invention mainly relates to dyestuff manufacture field, particularly relate to the bronze-colored stain of a kind of knitting.
Background technology
Bronze-colored, the dark brown of similar bronze color, it is used to refer to skin color more, is pursued by numerous people, healthy, property
The skin color of sense, so being also a kind of color comparing fashion.In existing knitting, the most dye five face with dyestuff
Six colors, bronze-colored is exactly a kind of popular color and luster, but current knitting is bronze-colored for chemical dye, and dye is bronze-colored impure
Just, easily fading, pollute environment, some dyes even can produce toxic gas during dye system, threatens the health of human body.
Thus, in knitting field preparation one, knitting is dyed copper-colored pure natural plant dyestuff, uniform color,
Color is pure, bright and new beautiful, is difficult to fade, and environmental protection, giving out plant fragrance for a long time, the body and mind of useful people is good for
Health, simultaneously it can be avoided that the harm produced human body in dyeing course.
Summary of the invention
In order to make up the defect of prior art, it is an object of the invention to provide the bronze-colored stain of a kind of knitting.
The bronze-colored stain of a kind of knitting, is made up of the raw material of following weight portion: Cortex Pini 55 ~ 57, chestnut shell 42 ~
44, rapeseed meal 40 ~ 42, dry Folium paulowniae 36 ~ 38, Periostracum Serpentis shell 28 ~ 30, Folium Camelliae sinensis leftover bits and pieces 28 ~ 30, flower of poplar 13 ~ 15, HUANGLONG ship
Spend 25 ~ 27, yellow Flos Lilii viriduli 25 ~ 27, Cassia surattensis spend 23 ~ 25, Flos kerriae japonicae 23 ~ 25, Fructus Mangifera Indicae 21 ~ 23, ginkgo nut 21 ~ 23.
A kind of preparation method of the bronze-colored stain of knitting, concrete steps include:
(1) Cortex Pini, chestnut shell, rapeseed meal, dry Folium paulowniae, Periostracum Serpentis shell, Folium Camelliae sinensis leftover bits and pieces and flower of poplar are pulverized, excessively 60 ~
80 mesh sieves, obtain vegetable material A, add the distilled water of pH8.5 ~ 9.5 of vegetable material A weight 6 ~ 7 times amount, in 60 ~ 65 DEG C, 35 ~ 37kHz
Ultrasonic 45 ~ 50 minutes, filter, obtain extracting solution and filtering residue, add the distilled water of pH8.5 ~ 9.5 of filtering residue weight 4 ~ 5 times amount, in 65
~ 70 DEG C, ultrasonic 35 ~ 40 minutes of 28 ~ 30kHz, filter, and merges all extracting solution, crosses the microporous filter membrane of 0.22 μm, 70 ~ 72 DEG C of bakings
Doing to water content is 0 ~ 4%, obtains brown pigment；
(2) leumus coccinea L. Var. Iutea corner, yellow Flos Lilii viriduli, Cassia surattensis flower, Flos kerriae japonicae, Fructus Mangifera Indicae and ginkgo nut are pulverized, cross 60 ~ 80 mesh sieves, obtain plant
Material C, add vegetable material C weight 8 ~ 9 times amount the ethanol solution that volume fraction is 78 ~ 80%, in 45 ~ 50 DEG C, 31 ~ 33kHz ultrasonic
40 ~ 45 minutes, filtering, cross the microporous filter membrane of 0.22 μm, 40 ~ 42 DEG C of rotary evaporation in vacuo to water content are 30 ~ 32%, in 64 ~ 66
DEG C drying is 0 ~ 4% to water content, obtains xanthein；
(3) in brown pigment and xanthein, add the distilled water of each pigment weight 2 times amount respectively, be configured to brown color respectively
Cellulose solution and xanthein solution；
(4) xanthein solution is added in brown pigment solution, stir, in 32 ~ 34 DEG C, 38 ~ 40kHz ultrasonic 20 ~ 25
Minute, obtain the bronze-colored stain of knitting；
(5) packaging, obtains finished product.
The using method of the bronze-colored stain of described knitting, during use, the color and luster depth on demand adds distilled water and carries out
Dilution, is configured to dyeing liquor, it would be desirable to the knitting of dyeing is dipped in dyeing liquor, the ultrasonic immersion of 60 ~ 62kHz 20 ~ 25 minutes, soon
Speed dyeing, takes out, be placed in temperature be 14 ~ 16 DEG C, humidity be 36 ~ 38% environment in natural drying.
The invention have the advantage that the bronze-colored stain of a kind of knitting that the present invention provides, preparation is simple, through pure natural
Plant material extracts, cheap, and cost-effective 16.3%；According to brown and the characteristic of yellow plant, extract brown and Huang respectively
Color, and carry out color and luster collocation according to three primary colors collocation principle, the most quickly, obtain natural bronze-colored；Only need to be in dyeing during dyeing
Ultrasonic in the aqueous solution of agent soak in short-term, improve work efficiency, even dyeing, pure color, colour-fast, anti-mould and anti-moth,
Being easy to storage, extend using period, without any toxic reagent, safety and environmental protection, have health care and plant flavour, protection human body is good for
Health.
Detailed description of the invention
With specific embodiment, the present invention is described below.
Embodiment 1
The bronze-colored stain of a kind of knitting, is made up of the raw material of following weight portion: Cortex Pini 55, chestnut shell 42, rapeseed meal
40, dry Folium paulowniae 36, Periostracum Serpentis shell 28, Folium Camelliae sinensis leftover bits and pieces 28, flower of poplar 13, leumus coccinea L. Var. Iutea corner 25, yellow Flos Lilii viriduli 25, Cassia surattensis flower
23, Flos kerriae japonicae 23, Fructus Mangifera Indicae 21, ginkgo nut 21.
A kind of preparation method of the bronze-colored stain of knitting, concrete steps include:
(1) Cortex Pini, chestnut shell, rapeseed meal, dry Folium paulowniae, Periostracum Serpentis shell, Folium Camelliae sinensis leftover bits and pieces and flower of poplar are pulverized, cross 80 mesh
Sieve, obtains vegetable material A, adds the distilled water of the pH9 of vegetable material A weight 7 times amount, in 65 DEG C, ultrasonic 45 ~ 50 minutes of 37kHz, mistake
Filter, obtains extracting solution and filtering residue, adds the distilled water of the pH9 of filtering residue weight 5 times amount, in 70 DEG C, ultrasonic 40 minutes of 30kHz, filters,
Merging all extracting solution, cross the microporous filter membrane of 0.22 μm, 70 DEG C dry to water content is 0 ~ 4%, obtains brown pigment；
(2) leumus coccinea L. Var. Iutea corner, yellow Flos Lilii viriduli, Cassia surattensis flower, Flos kerriae japonicae, Fructus Mangifera Indicae and ginkgo nut are pulverized, cross 80 mesh sieves, obtain vegetable material C,
Add the ethanol solution that volume fraction is 78% of vegetable material C weight 8 times amount, in 45 DEG C, ultrasonic 40 minutes of 31kHz, filter, mistake
The microporous filter membrane of 0.22 μm, 40 DEG C of rotary evaporation in vacuo to water content are 32%, and drying to water content in 65 DEG C is 0 ~ 4%, obtains yellow
Color pigment；
(3) in brown pigment and xanthein, add the distilled water of each pigment weight 2 times amount respectively, be configured to brown color respectively
Cellulose solution and xanthein solution；
(4) xanthein solution is added in brown pigment solution, stir, in 32 DEG C, ultrasonic 25 minutes of 38kHz, obtain volume
The bronze-colored stain of fabric；
(5) packaging, obtains finished product.
The using method of the bronze-colored stain of described knitting, during use, the color and luster depth on demand adds distilled water and carries out
Dilution, is configured to dyeing liquor, it would be desirable to the knitting of dyeing is dipped in dyeing liquor, and the ultrasonic immersion of 60kHz 25 minutes quickly contaminates
Color, takes out, be placed in temperature be 16 DEG C, humidity be 36% environment in natural drying.
Embodiment 2
The bronze-colored stain of a kind of knitting, is made up of the raw material of following weight portion: Cortex Pini 56, chestnut shell 43, rapeseed meal
41, dry Folium paulowniae 37, Periostracum Serpentis shell 29, Folium Camelliae sinensis leftover bits and pieces 29, flower of poplar 14, leumus coccinea L. Var. Iutea corner 26, yellow Flos Lilii viriduli 26, Cassia surattensis flower
24, Flos kerriae japonicae 24, Fructus Mangifera Indicae 22, ginkgo nut 22.
Preparation and application, with embodiment 1.
Embodiment 3
The bronze-colored stain of a kind of knitting, is made up of the raw material of following weight portion: Cortex Pini 57, chestnut shell 44, rapeseed meal
42, dry Folium paulowniae 38, Periostracum Serpentis shell 30, Folium Camelliae sinensis leftover bits and pieces 30, flower of poplar 15, leumus coccinea L. Var. Iutea corner 27, yellow Flos Lilii viriduli 27, Cassia surattensis flower
25, Flos kerriae japonicae 25, Fructus Mangifera Indicae 23, ginkgo nut 23.
Preparation and application, with embodiment 1.
Comparative example
The bronze-colored stain of existing knitting.
Embodiment and the index evaluation of comparative example stain:
With the stain of comparative example, identical knitting being carried out dyeing process by embodiment respectively, all knitting are not carried out
Anti-mould and anti-moth process, detect after being disposed, being placed in temperature is 35 DEG C, humidity be 85% environment in carry out anti-mould and anti-moth
Effect detection, the index evaluation of embodiment and comparative example stain is shown in Table 1.
Table 1: embodiment and the index evaluation of comparative example stain
| Project | Embodiment | Comparative example |
| Cost-effective/(%) | 16.3 | — |
| Color and luster | Uniformly, pure | Uneven, impure |
| Abnormal flavour | Nothing, has fragrance | Have |
| Occur mouldy damaging by worms/(my god) | 24~26 | 3~4 |
| Toxicity | Nothing | Have |
Note: " " indicate without.
The result of table 1 shows, the bronze-colored stain of embodiment knitting, with low cost, compared with comparative example, saves into
Basis 16.3%, knitting even dyeing, pure color, there is natural plant flavour, the knitting after dyeing, place 24 ~ 26 days
Rear just have under a small amount of Signs of Mould, home can keep 6 months the most mouldy damaging by worms, the Gu of the knitting that the present invention provides is described
Copper coloration agent has preferable Color.
Claims (3)
1. the bronze-colored stain of a knitting, it is characterised in that be made up of the raw material of following weight portion: Cortex Pini 55 ~ 57,
Chestnut shell 42 ~ 44, rapeseed meal 40 ~ 42, dry Folium paulowniae 36 ~ 38, Periostracum Serpentis shell 28 ~ 30, Folium Camelliae sinensis leftover bits and pieces 28 ~ 30, flower of poplar 13 ~
15, leumus coccinea L. Var. Iutea corner 25 ~ 27, yellow Flos Lilii viriduli 25 ~ 27, Cassia surattensis spend 23 ~ 25, Flos kerriae japonicae 23 ~ 25, Fructus Mangifera Indicae 21 ~ 23, ginkgo nut 21 ~ 23.
The preparation method of the bronze-colored stain of knitting the most according to claim 1, it is characterised in that concrete steps bag
Include:
(1) Cortex Pini, chestnut shell, rapeseed meal, dry Folium paulowniae, Periostracum Serpentis shell, Folium Camelliae sinensis leftover bits and pieces and flower of poplar are pulverized, excessively 60 ~
80 mesh sieves, obtain vegetable material A, add the distilled water of pH8.5 ~ 9.5 of vegetable material A weight 6 ~ 7 times amount, in 60 ~ 65 DEG C, 35 ~ 37kHz
Ultrasonic 45 ~ 50 minutes, filter, obtain extracting solution and filtering residue, add the distilled water of pH8.5 ~ 9.5 of filtering residue weight 4 ~ 5 times amount, in 65
~ 70 DEG C, ultrasonic 35 ~ 40 minutes of 28 ~ 30kHz, filter, and merges all extracting solution, crosses the microporous filter membrane of 0.22 μm, 70 ~ 72 DEG C of bakings
Doing to water content is 0 ~ 4%, obtains brown pigment；
(2) leumus coccinea L. Var. Iutea corner, yellow Flos Lilii viriduli, Cassia surattensis flower, Flos kerriae japonicae, Fructus Mangifera Indicae and ginkgo nut are pulverized, cross 60 ~ 80 mesh sieves, obtain plant
Material C, add vegetable material C weight 8 ~ 9 times amount the ethanol solution that volume fraction is 78 ~ 80%, in 45 ~ 50 DEG C, 31 ~ 33kHz ultrasonic
40 ~ 45 minutes, filtering, cross the microporous filter membrane of 0.22 μm, 40 ~ 42 DEG C of rotary evaporation in vacuo to water content are 30 ~ 32%, in 64 ~ 66
DEG C drying is 0 ~ 4% to water content, obtains xanthein；
(3) in brown pigment and xanthein, add the distilled water of each pigment weight 2 times amount respectively, be configured to brown color respectively
Cellulose solution and xanthein solution；
(4) xanthein solution is added in brown pigment solution, stir, in 32 ~ 34 DEG C, 38 ~ 40kHz ultrasonic 20 ~ 25
Minute, obtain the bronze-colored stain of knitting；
(5) packaging, obtains finished product.
3. according to the using method of the bronze-colored stain of knitting described in claim 1 ~ 2, it is characterised in that on-demand during use
The color and luster depth wanted adds distilled water and is diluted, and is configured to dyeing liquor, it would be desirable to the knitting of dyeing is dipped in dyeing liquor, 60 ~
The ultrasonic immersion of 62kHz 20 ~ 25 minutes, takes out, be placed in temperature be 14 ~ 16 DEG C, humidity be 36 ~ 38% environment in natural drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610549275.XA CN106118129A (en) | 2016-07-13 | 2016-07-13 | A kind of bronze-colored stain of knitting |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610549275.XA CN106118129A (en) | 2016-07-13 | 2016-07-13 | A kind of bronze-colored stain of knitting |
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| Publication Number | Publication Date |
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| CN106118129A true CN106118129A (en) | 2016-11-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610549275.XA Pending CN106118129A (en) | 2016-07-13 | 2016-07-13 | A kind of bronze-colored stain of knitting |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107234694A (en) * | 2017-05-25 | 2017-10-10 | 李超 | A kind of manufacture craft of bamboo knitting |
| CN107254192A (en) * | 2017-07-25 | 2017-10-17 | 王吉云 | A kind of bamboo wood mould coloring agent, preparation method and its production application |
| CN109233329A (en) * | 2018-10-24 | 2019-01-18 | 云南农业大学 | A kind of salacca edulis salak method for extracting pigment |
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| CN102876070A (en) * | 2012-06-19 | 2013-01-16 | 湖北紫鑫生物科技有限公司 | Method for extracting brown pigment of chestnut shells by using ultrasonic waves |
| CN103044956A (en) * | 2012-12-14 | 2013-04-17 | 北京林业大学 | Method for extracting natural haematochrome from larch bark |
| CN103319912A (en) * | 2013-07-18 | 2013-09-25 | 黑龙江生态工程职业学院 | Hickory nut shell brown pigment and its preparation method |
| CN103725032A (en) * | 2013-12-13 | 2014-04-16 | 常州大学 | Preparation method and application of natural lotus receptacle pigment |
| CN103804949A (en) * | 2014-03-01 | 2014-05-21 | 哈尔滨市工艺美术有限责任公司 | Dye for preparing bronze wheat straws and production method thereof |
| CN104419217A (en) * | 2013-09-08 | 2015-03-18 | 青岛鹏远康华天然产物有限公司 | Preparation method of high-efficiency combination pigment |
| CN105713418A (en) * | 2016-01-21 | 2016-06-29 | 苏州印丝特纺织数码科技有限公司 | Natural mango dye based on mango yellow pigment and preparation method of natural mango dye |
-
2016
- 2016-07-13 CN CN201610549275.XA patent/CN106118129A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102876070A (en) * | 2012-06-19 | 2013-01-16 | 湖北紫鑫生物科技有限公司 | Method for extracting brown pigment of chestnut shells by using ultrasonic waves |
| CN103044956A (en) * | 2012-12-14 | 2013-04-17 | 北京林业大学 | Method for extracting natural haematochrome from larch bark |
| CN103319912A (en) * | 2013-07-18 | 2013-09-25 | 黑龙江生态工程职业学院 | Hickory nut shell brown pigment and its preparation method |
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| CN103804949A (en) * | 2014-03-01 | 2014-05-21 | 哈尔滨市工艺美术有限责任公司 | Dye for preparing bronze wheat straws and production method thereof |
| CN105713418A (en) * | 2016-01-21 | 2016-06-29 | 苏州印丝特纺织数码科技有限公司 | Natural mango dye based on mango yellow pigment and preparation method of natural mango dye |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107234694A (en) * | 2017-05-25 | 2017-10-10 | 李超 | A kind of manufacture craft of bamboo knitting |
| CN107254192A (en) * | 2017-07-25 | 2017-10-17 | 王吉云 | A kind of bamboo wood mould coloring agent, preparation method and its production application |
| CN109233329A (en) * | 2018-10-24 | 2019-01-18 | 云南农业大学 | A kind of salacca edulis salak method for extracting pigment |
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Application publication date: 20161116 |
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