CN105820598A - Antibacterial textile plant dye and preparation method thereof - Google Patents
Antibacterial textile plant dye and preparation method thereof Download PDFInfo
- Publication number
- CN105820598A CN105820598A CN201610327633.2A CN201610327633A CN105820598A CN 105820598 A CN105820598 A CN 105820598A CN 201610327633 A CN201610327633 A CN 201610327633A CN 105820598 A CN105820598 A CN 105820598A
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- China
- Prior art keywords
- extract
- parts
- vegetable colour
- antibacterial textile
- antibacterial
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0092—Dyes in solid form
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
Abstract
The invention discloses an antibacterial textile plant dye .The antibacterial textile plant dye is prepared from, by weight, 15-25 parts of a plant dye extract, 5-10 parts of sodium lactate, 10-15 parts of a chitosan derivate, 1-4 parts of sorbitan esters, 5-8 parts of paraffin, 2-5 parts of dyeing acid, 1-4 parts of a softening agent and 80-100 parts of deionized water .The plant dye is high in dye fastness, tender in hue, natural, environmentally friendly and low in raw material obtaining cost .The production process is simple, low in carbon and environmentally friendly, the processed fabric contains no toxic substances, no harm is caused to human bodies and environment, the safety is high, and the antibacterial textile plant dye further has the good mold-proof antibacterial performance and antistatic performance.
Description
Technical field
The present invention relates to field of fabric producing technology, specifically a kind of antibacterial textile vegetable colour and preparation method thereof.
Background technology
Along with the raising of people's living standard, textile industry obtains high speed development in China, and China has become textile production big country the most worthy of the name, and textile industry also result in serious environmental pollution while promoting economic development.At present, the chemical dyestuff that dyeing is conventional contains various harmful substance the most in various degree, jeopardizes people healthy, and processing technique length, equipment are many, energy consumption is high, and produced large amount of sewage intractability greatly, costly, poses a big pressure to ecological environment.
Summary of the invention
Therefore, for solving the problems referred to above, the present invention provides a kind of antibacterial textile vegetable colour, high with textile binding strength, and the color even on yarn fabric also has good fungus-resistant performance and antistatic behaviour.Production process low-carbon (LC), environmental protection, to human body and environmentally friendly, safety is high, suits large area to popularize.
The technical solution used in the present invention is: a kind of antibacterial textile vegetable colour, raw material including following weight portion: vegetable colour extract 15-25 part, sodium lactate 5-10 part, chitosan derivatives 10-15 part, sorbitan ester 1-4 part, paraffin 5-8 part, dyeing acid 2-5 part, softening agent 1-4 part, deionized water 80-100 part.
Described vegetable colour extract is one or more in Madder extract, Lignum Sappan extract, Flos Carthami extract.
Described chitosan derivatives is carboxymethyl chitosan or hydroxypropyl chitosan.
Described softening agent is sodium hexameta phosphate.
The preparation method of above-mentioned antibacterial textile vegetable colour, comprises the following steps: vegetable colour raw material is cleaned by (1), crushed after being dried is standby；(2) plant and ethanol after pulverizing compare with the quality of 1: 15 ~ 30 mixs homogeneously, after in the dual-frequency ultrasonic wave extraction equipment of 20 KHz and 33KHz, process 30min, ethanol extract 2-3 time, it is filtrated to get filtrate, (3) by compressed for filtrate spraying, the vegetable colour extract of powder is obtained；(4) sodium lactate, chitosan derivatives, sorbitan ester, paraffin, softening agent and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；(5) joining in the mixed liquor that step (4) obtains by the vegetable colour extract that step (3) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder antibacterial plant dyestuff.
The invention has the beneficial effects as follows: the dyeing fastness of natural plant dyeing of the present invention is high, and tone is soft, natural environmental-protective, and raw material procurement cost is low.Production process is simple, low-carbon (LC), environmental protection, the fabric being processed into does not contains noxious substance, and to human body and environmentally friendly, safety is high, and chitosan derivatives makes the fabric being processed into also have good fungus-resistant performance and antistatic behaviour.
Detailed description of the invention
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment is only used for explaining the present invention, is not intended that limiting the scope of the present invention.
Embodiment 1
A kind of antibacterial textile vegetable colour, including the raw material of following weight portion: Madder extract 15 parts, sodium lactate 10 parts, carboxymethyl chitosan 15 parts, sorbitan ester 4 parts, 5 parts of paraffin, dyeing acid 5 parts, sodium hexameta phosphate 1 part, deionized water 80 parts.
The preparation method of above-mentioned antibacterial textile vegetable colour, comprises the following steps: Radix Rubiae raw material is cleaned by (1), crushed after being dried is standby；(2) Radix Rubiae and ethanol after pulverizing compare with the quality of 1: 20 mixs homogeneously, after in the dual-frequency ultrasonic wave extraction equipment of 20 KHz and 33KHz, process 30min, ethanol extract 2-3 time, being filtrated to get filtrate, (3), by compressed for filtrate spraying, obtain the Madder extract of powder；(4) proportionally sodium lactate, carboxymethyl chitosan, sorbitan ester, paraffin, sodium hexameta phosphate and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；(5) being proportionally added into in the mixed liquor that step (4) obtains by the Madder extract that step (3) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder antibacterial plant dyestuff.
Embodiment 2
A kind of antibacterial textile vegetable colour, including the raw material of following weight portion: Lignum Sappan extract 20 parts, sodium lactate 5 parts, hydroxypropyl chitosan 10 parts, sorbitan ester 1 part, 6 parts of paraffin, dyeing acid 3 parts, sodium hexameta phosphate 2 parts, deionized water 90 parts.
The preparation method of above-mentioned antibacterial textile vegetable colour, comprises the following steps: Lignum Sappan raw material is cleaned by (1), crushed after being dried is standby；(2) Lignum Sappan and ethanol after pulverizing compare with the quality of 1: 15 mixs homogeneously, after in the dual-frequency ultrasonic wave extraction equipment of 20 KHz and 33KHz, process 30min, ethanol extract 2-3 time, being filtrated to get filtrate, (3), by compressed for filtrate spraying, obtain the Lignum Sappan extract of powder；(4) proportionally sodium lactate, hydroxypropyl chitosan, sorbitan ester, paraffin, sodium hexameta phosphate and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；(5) being proportionally added into in the mixed liquor that step (4) obtains by the Lignum Sappan extract that step (3) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder antibacterial plant dyestuff.
Embodiment 3
A kind of antibacterial textile vegetable colour, including the raw material of following weight portion: Flos Carthami extract 25 parts, sodium lactate 8 parts, carboxymethyl chitosan 12 parts, sorbitan ester 2 parts, 8 parts of paraffin, dyeing acid 2 parts, sodium hexameta phosphate 4 parts, deionized water 100 parts.
The preparation method of above-mentioned antibacterial textile vegetable colour, comprises the following steps: Flos Carthami raw material is cleaned by (1), crushed after being dried is standby；(2) Flos Carthami and ethanol after pulverizing compare with the quality of 1: 25 mixs homogeneously, after in the dual-frequency ultrasonic wave extraction equipment of 20 KHz and 33KHz, process 30min, ethanol extract 2-3 time, being filtrated to get filtrate, (3), by compressed for filtrate spraying, obtain the Flos Carthami extract of powder；(4) proportionally sodium lactate, carboxymethyl chitosan, sorbitan ester, paraffin, sodium hexameta phosphate and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；(5) being proportionally added into in the mixed liquor that step (4) obtains by the Flos Carthami extract that step (3) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder antibacterial plant dyestuff.
Embodiment 4
A kind of antibacterial textile vegetable colour, including the raw material of following weight portion: Radix Rubiae and Lignum Sappan extract 25 parts, sodium lactate 6 parts, hydroxypropyl chitosan 15 parts, sorbitan ester 3 parts, 5 parts of paraffin, dyeing acid 5 parts, sodium hexameta phosphate 1 part, deionized water 100 parts.
The preparation method of above-mentioned antibacterial textile vegetable colour, comprises the following steps: Radix Rubiae and Lignum Sappan raw material are cleaned by (1), crushed after being dried is standby；(2) Radix Rubiae after pulverizing and Lignum Sappan and ethanol compare with the quality of 1:30 mixs homogeneously, after in the dual-frequency ultrasonic wave extraction equipment of 20 KHz and 33KHz, process 30min, ethanol extract 2-3 time, it is filtrated to get filtrate, (3) by compressed for filtrate spraying, Radix Rubiae and the Lignum Sappan extract of powder are obtained；(4) proportionally sodium lactate, hydroxypropyl chitosan, sorbitan ester, paraffin, sodium hexameta phosphate and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；(5) Radix Rubiae step (3) obtained and Lignum Sappan extract are proportionally added in the mixed liquor that step (4) obtains, and stirring stands compressed for filtrate spraying after filtering, obtains powder antibacterial plant dyestuff.
Claims (5)
1. an antibacterial textile vegetable colour, it is characterised in that include the raw material of following weight portion:
Vegetable colour extract 15-25 part,
Sodium lactate 5-10 part,
Chitosan derivatives 10-15 part,
Sorbitan ester 1-4 part,
Paraffin 5-8 part,
Dyeing acid 2-5 part,
Softening agent 1-4 part,
Deionized water 80-100 part.
A kind of antibacterial textile vegetable colour the most according to claim 1, it is characterised in that described vegetable colour extract is one or more in Madder extract, Lignum Sappan extract, Flos Carthami extract.
A kind of antibacterial textile vegetable colour the most according to claim 1, it is characterised in that described chitosan derivatives is carboxymethyl chitosan or hydroxypropyl chitosan.
A kind of antibacterial textile vegetable colour the most according to claim 1, it is characterised in that described softening agent is sodium hexameta phosphate.
The preparation method of a kind of antibacterial textile vegetable colour the most according to claim 1, it is characterised in that: comprise the following steps: vegetable colour raw material is cleaned by (1), crushed after being dried is standby；(2) plant after pulverizing is mixed homogeneously with the quality ratio of 1:15 ~ 30 with ethanol, after process 30min, ethanol extract 2-3 time in the dual-frequency ultrasonic wave extraction equipment of 20 KHz and 33KHz, is filtrated to get filtrate；(3) by compressed for filtrate spraying, the vegetable colour extract of powder is obtained；(4) sodium lactate, chitosan derivatives, sorbitan ester, paraffin, softening agent and dyeing acid are added in deionized water, be sufficiently mixed at normal temperatures, form mixed liquor；(5) joining in the mixed liquor that step (4) obtains by the vegetable colour extract that step (3) obtains, stirring stands compressed for filtrate spraying after filtering, obtains powder antibacterial plant dyestuff.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610327633.2A CN105820598A (en) | 2016-05-18 | 2016-05-18 | Antibacterial textile plant dye and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610327633.2A CN105820598A (en) | 2016-05-18 | 2016-05-18 | Antibacterial textile plant dye and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN105820598A true CN105820598A (en) | 2016-08-03 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610327633.2A Pending CN105820598A (en) | 2016-05-18 | 2016-05-18 | Antibacterial textile plant dye and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106436358A (en) * | 2016-08-23 | 2017-02-22 | 苏州市恒信针织印染有限责任公司 | Natural dyeing composition for polyester fabrics and application of natural dyeing composition |
| CN106835745A (en) * | 2017-02-07 | 2017-06-13 | 苏州经贸职业技术学院 | A kind of method of textile finishing |
| CN107022908A (en) * | 2017-03-24 | 2017-08-08 | 合肥云都棉花有限公司 | A kind of colouring method of cotton cloth |
| CN108129876A (en) * | 2018-01-11 | 2018-06-08 | 山东冬瑞高新技术开发有限公司 | A kind of environmental protection composite dye and preparation method thereof |
| CN108178936A (en) * | 2018-02-10 | 2018-06-19 | 陈建峰 | A kind of preparation method of high color fastness vegetable colour |
| CN111206439A (en) * | 2020-01-21 | 2020-05-29 | 河南科技学院 | Textile antibacterial vegetable dye and preparation method thereof |
| CN112160170A (en) * | 2020-09-09 | 2021-01-01 | 苏州森创纺织科技有限公司 | Antibacterial plant dye and extraction method thereof |
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| CN105086505A (en) * | 2015-09-23 | 2015-11-25 | 界首市波菲特服饰有限公司 | Preparation method of natural plant dye |
| CN105111780A (en) * | 2015-09-23 | 2015-12-02 | 界首市波菲特服饰有限公司 | Fabric dye |
| CN105256605A (en) * | 2015-10-20 | 2016-01-20 | 湖州博仁纺织品有限公司 | Novel nanoscale natural dye for digital printing and preparation method of natural dye |
| CN105542509A (en) * | 2016-01-25 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Natural dye for spinning and preparation method thereof |
-
2016
- 2016-05-18 CN CN201610327633.2A patent/CN105820598A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105086505A (en) * | 2015-09-23 | 2015-11-25 | 界首市波菲特服饰有限公司 | Preparation method of natural plant dye |
| CN105111780A (en) * | 2015-09-23 | 2015-12-02 | 界首市波菲特服饰有限公司 | Fabric dye |
| CN105256605A (en) * | 2015-10-20 | 2016-01-20 | 湖州博仁纺织品有限公司 | Novel nanoscale natural dye for digital printing and preparation method of natural dye |
| CN105542509A (en) * | 2016-01-25 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Natural dye for spinning and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106436358A (en) * | 2016-08-23 | 2017-02-22 | 苏州市恒信针织印染有限责任公司 | Natural dyeing composition for polyester fabrics and application of natural dyeing composition |
| CN106835745A (en) * | 2017-02-07 | 2017-06-13 | 苏州经贸职业技术学院 | A kind of method of textile finishing |
| CN107022908A (en) * | 2017-03-24 | 2017-08-08 | 合肥云都棉花有限公司 | A kind of colouring method of cotton cloth |
| CN108129876A (en) * | 2018-01-11 | 2018-06-08 | 山东冬瑞高新技术开发有限公司 | A kind of environmental protection composite dye and preparation method thereof |
| CN108178936A (en) * | 2018-02-10 | 2018-06-19 | 陈建峰 | A kind of preparation method of high color fastness vegetable colour |
| CN111206439A (en) * | 2020-01-21 | 2020-05-29 | 河南科技学院 | Textile antibacterial vegetable dye and preparation method thereof |
| CN112160170A (en) * | 2020-09-09 | 2021-01-01 | 苏州森创纺织科技有限公司 | Antibacterial plant dye and extraction method thereof |
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Application publication date: 20160803 |
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