CN104027829B - A kind of solid freshener containing lemon tea tree derived essential oil and preparation method thereof - Google Patents
A kind of solid freshener containing lemon tea tree derived essential oil and preparation method thereof Download PDFInfo
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- CN104027829B CN104027829B CN201410252619.1A CN201410252619A CN104027829B CN 104027829 B CN104027829 B CN 104027829B CN 201410252619 A CN201410252619 A CN 201410252619A CN 104027829 B CN104027829 B CN 104027829B
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Abstract
The present invention relates to a kind of solid freshener containing lemon tea tree derived essential oil.Its main component and mass fraction are：Composite glue powder 0.5 3%, gel auxiliary agent 0.1 1%, lemon tea tree ethereal oil 1 10%, solubilizer 2 15%, sterilization antiseptic 0.1 0.5%, other components 0.01 0.1%, surplus is deionized water.The invention also discloses a kind of preparation method of the solid freshener containing lemon tea tree derived essential oil, comprise the following steps：1) composite glue powder is first stirred well to clear solution in 90 95 DEG C of hot water, adds gel auxiliary agent, stirring is abundant, is then cooled to 60 65 DEG C, insulated and stirred obtains A liquid；2) lemon tea tree ethereal oil, solubilizer are mixed, stirred.Obtain B liquid；3) B liquid is added in A liquid and mixed, stirred.Then sterilization antiseptic, other components are added, is stirred.Filtering and discharging is canned, and inspection is qualified can packed products.The present invention is using tea tree ethereal oil as fragrant functional component, and not only smell is fresh and clean, refreshes the mind, and with antibacterial, disinfection efficacy.
Description
Technical field
The present invention relates to a kind of air freshener, belong to daily chemical product technical field, and in particular to one kind contains lemon
Solid freshener of lemon tea tree ethereal oil composition and preparation method thereof.
Background technology
In recent years, with the continuous improvement of China's lives of the people level, people are also more next to healthy and domestic environment
More pay attention to.Air quality has become the another focus of attention after food security.Keep the clean of air and environment with
It is pure and fresh, it is everyone hope.Possess pure and fresh air, the fatigue of one day can be eliminated, the nervous body and mind of relaxation is beneficial to
Human body is physically and mentally healthy.But with the abundantization in life with physical product in work and variation, the environment and air of surrounding
It has been contaminated.It is more next the need for air freshener has become life in order to improve air quality and exclude air peculiar smell
More consumers begin to use air freshener to improve air quality.
To play the effect of preparation to greatest extent and improving the use feeling of consumer, make in air freshener manufacture
With every technology such as emulsification, solubilized, gelation, slow release.The technology applied in air freshener is primarily to assign
Perfume, smelly eliminating, suppression stench occur and antibacterial.The air freshener of current commercial type mainly have from form liquid-type,
Three kinds of aerosol-type and gel-type.Wherein most common and practical is gel-type, can slowly discharge the smell of fragrance, user
Just.At present in Chinese market, many consumers worry dangerous using air freshener, and worry is used using air freshener
Essence be chemical synthesis allotment, using human body can be damaged, influence health, can cause sky using air freshener
" secondary pollution " of gas, thus refusal uses air freshener.This also will hinder air freshener market further to develop
Reason.Accordingly, it would be desirable to which the air freshener for developing natural series meets different consumer demands.
Chinese patent CN1524585A discloses a kind of all natural air freshener, and it uses litsea citrate oil, attar of rose to make
For fragrance ingredient, compared with conventional air freshener, the volatile oil of natural origin is employed, more naturally, safely, but shape
State is liquid dosage form, in-convenience in use, and the ginseng of a variety of essential oils matches somebody with somebody, it is likely that the feature fragrance for original essential oil that can scatter and disappear.China
Patent CN1799635A discloses a kind of long effective air freshener, and being prepared which employs hydroexpansivity resin and long-acting gel can
To obtain gel type air freshener, spices is able to slowly discharge.But still using spices as fragrance ingredient, while adding tool
The auxiliary agents such as virose ethylene glycol, its security needs to be investigated.
With the living standard more and more higher of people, requirement to product also more and more higher.Therefore, how to develop a
Excellent air freshener not only possesses purification air, pleasant mental and body, but also it is safe and free of toxic and side effects, store and use
It is convenient, with certain antibacterial, deodorization the effects such as, be the technical barrier that one of ordinary skill in the art face.
The content of the invention
In order to overcome the above-mentioned deficiency of existing air freshener, contain lemon tea tree it is an object of the invention to provide one kind
The solid freshener of derived essential oil, using lemon tea tree ethereal oil as fragrant functional component, not only smell is fresh and clean, refreshes the mind,
And with antibacterial, disinfection efficacy, compared with conventional air freshener, product in use also more environmentally-friendly, green,
Health, safety.
The present invention is achieved by the following technical solutions.
It is proposed by the present invention a kind of containing lemon tea tree derived essential oil solid freshener, include each of following percentage by weight
Raw material components：Composite glue powder 0.5-3%；Gel auxiliary agent 0.1-1%；Lemon tea tree ethereal oil 1-10%；Solubilizer 1-15%；Sterilization
Preservative 0.1-0.5%；Other component 0.01-0.1%；Surplus is deionized water.
Furthermore, it is proposed by the present invention a kind of containing lemon tea tree derived essential oil solid freshener, comprising following heavy
Measure each raw material components of percentage：Composite glue powder 0.6~2.0%；Gel auxiliary agent 0.3~0.8%；Lemon tea tree ethereal oil 2.0~
6.0%；Solubilizer 2.0~8.0%；Sterilization antiseptic 0.1~0.3%；Other components 0.05~0.1%；Surplus is deionization
Water.
Composite glue powder of the present invention is gellan gum, carragheen, locust bean gum, agar, konjac glucomannan, wherein being more highly preferred to knot
The mixing of one or both of cold glue card and drawing glue in any proportion.Gellan gum is a kind of novel microbial exocellular polysaccharide, is
D-Glucose, D-Glucose aldehydic acid, D-Glucose, L- rhamnoses are followed successively by by four glycan molecules to be formed by connecting by glycosidic bond
Macromolecule saccharide compound, with superior gelling performance.Carragheen is a kind of hydrophilic gel, by galactolipin and dehydration gala
Calcium, potassium, sodium, the ammonium salt for the polysaccharide sulfuric ester that sugar is constituted.Gellan gum and carragheen are all the natural hydrophilic gels in source,
It is widely used in grocery trade.
Gel auxiliary agent of the present invention be any one of calcium chloride, calcium lactate, sodium chloride, sodium citrate or two kinds with
Upper mixture, wherein being more highly preferred to calcium lactate.
Lemon tea tree ethereal oil of the present invention is natural fragrant essence, and it had both possessed as lemon pleasant, shaken
The pure and fresh fragrance put forth energy, is described as " the happy oil " in Australia state, and the sterilizing power more stronger than traditional tea oil is possessed again, can be efficiently
The symptoms such as virus infection, hair purulence, the redness of skin are resisted, while consoling skin, reduction is stimulated, and is natural bactericide, anti-corrosion
Agent and antiphlogistic.Its component comprising geranial (22-30%), neral (23-27%), geraniol, citronellal (9-28%) and
Citronellol.
Solubilizer of the present invention have rilanit special, AEO -9, AEO -7,
Mixture more than one or both of this kind -60, Tween-80, wherein being more highly preferred to rilanit special.
Sterilization antiseptic of the present invention have one kind in sodium benzoate, methylisothiazolinone, phenoxetol or
Two or more mixture, wherein being more highly preferred to methylisothiazolinone.
In addition, the invention also provides a kind of preparation side of the above-mentioned type solid pleasant smell agent containing lemon tea tree derived essential oil
Method, comprises the following steps：
1) composite glue powder is first stirred well to clear solution in 90-95 DEG C of hot water, adds gel auxiliary agent, stirring is filled
Point, 60-65 DEG C is then cooled to, insulated and stirred obtains A liquid；
2) lemon tea tree ethereal oil, solubilizer are mixed, stirs, obtain B liquid；
3) B liquid is added in A liquid and mixed, stirred.Then sterilization antiseptic, other components are added, is stirred；
Filtering and discharging is canned, and inspection is qualified can packed products.
Solid freshener of the present invention has the following advantages and beneficial effect compared to prior art：
Using the lemon tea tree ethereal oil of natural origin as fragrant functional component, not only smell is fresh and clean, refreshes the mind, and
With antibacterial, disinfection efficacy.Compared with traditional liquid type air freshener, product open wide place just sustainable fragrant 25 days with
On, it is easy to use.Product is also more environmentally-friendly in use, health, safety.Meet consumer it is green to air, pure and fresh, from
Right requirement.
Embodiment
Below by way of solid containing lemon tea tree ethereal oil of the specific preferred embodiment combination comparative test example to the present invention
Freshener is described in further detail, but the present invention is not limited in following embodiment.
The solid freshener performance test methods containing lemon tea tree ethereal oil of the present invention are as follows：
1st, fragrance preference degree evaluation method.
Evaluation method：The sample of preparation is placed in confined space (about 3m3) in place 2 hours, select tested volunteer man
Female totally 10 (- 55 years old 22 years old age), sensory evaluation is carried out to sample, is scored to evaluate fragrance happiness by following 4 degree
Good degree：10 points, enjoy a lot；8 points, prefer；6 points, typically；0 point, do not like；
2nd, use time evaluation method
The sample (about 70g) parallel (2 groups) of preparation is positioned in half ventilated environment and volatilized naturally, origination date is recorded.
Observe and weigh daily, until sample exhausted or weight constant weight completely, is judged as that record date, calculating uses day using finishing
Number.
Embodiment 1~3
According to the formulation content of table 1, the solid freshener containing lemon tea tree ethereal oil of embodiment 1~3 is prepared respectively, its
Preparation method is：The composite glue powder for first constituting carragheen, konjac glucomannan is stirred well to clear solution in 90-95 DEG C of hot water,
Calcium chloride is added, stirring is abundant, is then cooled to 60-65 DEG C, insulated and stirred obtains A liquid；By lemon tea tree ethereal oil, antioxidant,
Rilanit special is mixed, and is stirred.Obtain B liquid；B liquid is added in A liquid and mixed, is stirred.Then the different thiophene of methyl is added
Oxazoline ketone, pigment, stir.Filtering and discharging is canned.Extract sample and tested by quality standard, inspection is qualified to wrap
Dress up product.
The formula composition of the lemon tea tree ethereal oil solid freshener of the embodiment 1~3 of table 1
Embodiment 4~6
According to the formulation content of table 2, the lemon tea tree ethereal oil solid freshener of embodiment 4~6, its preparation method are prepared respectively
It is：The composite glue powder for first constituting carragheen, locust bean gum is stirred well to clear solution in 90-95 DEG C of hot water, adds breast
Sour calcium, stirring is abundant, is then cooled to 60-65 DEG C, insulated and stirred obtains A liquid；By lemon tea tree ethereal oil, antioxidant, hydrogenation castor
Sesame oil and AEO9 mixing, stir.Obtain B liquid；B liquid is added in A liquid and mixed, is stirred.Then the different thiophene of methyl is added
Oxazoline ketone, pigment, stir.Filtering and discharging is canned.Extract sample and tested by quality standard, inspection is qualified to wrap
Dress up product.
The formula composition of the lemon tea tree ethereal oil solid freshener of the embodiment 4~6 of table 2
Embodiment 7~9
According to the formulation content of table 3, the lemon tea tree ethereal oil solid freshener of embodiment 7~9, its preparation method are prepared respectively
It is：The composite glue powder for first constituting konjac glucomannan, gellan gum is stirred well to clear solution in 90-95 DEG C of hot water, adds chlorination
Potassium, stirring is abundant, is then cooled to 60-65 DEG C, insulated and stirred obtains A liquid；By lemon tea tree ethereal oil, antioxidant, hydrogenated castor
Oil mixing, stirs.Obtain B liquid；B liquid is added in A liquid and mixed, is stirred.Then methylisothiazolinone, color are added
Element, stirs.Filtering and discharging is canned.Extract sample and tested by quality standard, inspection is qualified can be packaged into product.
The formula composition of the lemon tea tree ethereal oil solid freshener of the embodiment 7~9 of table 3
Embodiment 10~12
According to the formulation content of table 4, the lemon tea tree ethereal oil solid freshener of embodiment 10~12, its preparation method are prepared respectively
It is：The composite glue powder for first constituting carragheen, gellan gum is stirred well to clear solution in 90-95 DEG C of hot water, adds chlorination
Calcium, stirring is abundant, is then cooled to 60-65 DEG C, insulated and stirred obtains A liquid；By lemon tea tree ethereal oil, antioxidant, hydrogenated castor
Oil mixing, stirs.Obtain B liquid；B liquid is added in A liquid and mixed, is stirred.Then methylisothiazolinone, color are added
Element, stirs.Filtering and discharging is canned.Extract sample and tested by quality standard, inspection is qualified can be packaged into product.
The formula composition of the lemon tea tree ethereal oil solid freshener of the embodiment 10~12 of table 4
By above-described embodiment, commercial air freshener is contrasted, fragrance preference degree has been carried out and has assessed and use time test,
Experimental result is shown in Table 5, table 6.
The fragrance preference degree of table 5 and use time result
The fragrance preference degree of table 6 and use time result
The test data of 6~table of consolidated statement 7 can be seen that using the consumer likeability of each embodiment product and when using
Between be above commercially available prod.
The characteristics of solid freshener containing lemon tea tree derived essential oil of the present invention, is：
The present invention is fragrant functional component using the lemon tea tree ethereal oil of natural origin, and not only smell is fresh and clean, refreshes oneself
Restoring consciouness.And with antibacterial, disinfection efficacy.Compared with traditional liquid type air freshener, product, which is opened wide, places just sustainable virtue
It is fragrant more than 25 days, it is easy to use.Also more environmentally-friendly, health, the safety of product in use.Meet consumer green to air
Color, pure and fresh, natural requirement.
The above described is only a preferred embodiment of the present invention, any formal limitation not is made to the present invention, therefore
Every any letter made without departing from technical solution of the present invention content, the technical spirit according to the present invention to embodiment described above
Single modification, equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (4)
1. a kind of solid freshener containing lemon tea tree derived essential oil, it is characterised in that be each original by following percentage by weight
Expect component composition：
Above-mentioned solid freshener is prepared by following processing step：
1) composite glue powder is first stirred well to clear solution in 90-95 DEG C of hot water, adds gel auxiliary agent, stirring is abundant, so
After be cooled to 60-65 DEG C, insulated and stirred obtains A liquid；
2) lemon tea tree ethereal oil, solubilizer are mixed, stir to obtain B liquid；
3) B liquid is added in A liquid and mixed, stirred；Then sterilization antiseptic, other components are added, is stirred；Filtering
Discharging is canned, and inspection is qualified can packed products.
2. the solid freshener according to claim 1 containing lemon tea tree derived essential oil, it is characterised in that containing following
Each raw material components of percentage by weight：
Above-mentioned solid freshener is prepared by following processing step：
1) composite glue powder is first stirred well to clear solution in 90-95 DEG C of hot water, adds gel auxiliary agent, stirring is abundant, so
After be cooled to 60-65 DEG C, insulated and stirred obtains A liquid；
2) lemon tea tree ethereal oil, solubilizer are mixed, stir to obtain B liquid；
3) B liquid is added in A liquid and mixed, stirred；Then sterilization antiseptic, other components are added, is stirred；Filtering
Discharging is canned, and inspection is qualified can packed products.
3. the solid freshener according to claim 1 containing lemon tea tree derived essential oil, it is characterised in that：The sterilization
Preservative is mixture more than one or both of sodium benzoate, methylisothiazolinone, phenoxetol.
4. the solid freshener according to claim 1 containing lemon tea tree derived essential oil, it is characterised in that：It is described other
Component is light stabilizer, antioxidant, pigment, and these components are universaling component, and kind does not do specific limitation.
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| CN201410252619.1A CN104027829B (en) | 2014-06-09 | 2014-06-09 | A kind of solid freshener containing lemon tea tree derived essential oil and preparation method thereof |
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| CN104027829B true CN104027829B (en) | 2017-08-11 |
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| CN107469119B (en) * | 2017-08-31 | 2021-05-11 | 广东爱车小屋电子商务科技有限公司 | Incense and preparation method thereof |
| US20210007969A1 (en) * | 2018-01-09 | 2021-01-14 | Lauren Servin | Fast-absorbing cosmetic oil through acacia or other tree gum diffusion process |
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| CN110029022A (en) * | 2019-04-24 | 2019-07-19 | 浙江大学台州研究院 | Solid plant essential oil of sustained release and preparation method thereof |
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