CN104000243A - Method for extracting oyster powder from oyster cooking liquor - Google Patents
Method for extracting oyster powder from oyster cooking liquor Download PDFInfo
- Publication number
- CN104000243A CN104000243A CN201410261829.7A CN201410261829A CN104000243A CN 104000243 A CN104000243 A CN 104000243A CN 201410261829 A CN201410261829 A CN 201410261829A CN 104000243 A CN104000243 A CN 104000243A
- Authority
- CN
- China
- Prior art keywords
- oyster
- cooking liquor
- extracting
- temperature
- ostreae testa
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000237502 Ostreidae Species 0.000 title claims abstract description 65
- 235000020636 oyster Nutrition 0.000 title claims abstract description 65
- 238000010411 cooking Methods 0.000 title claims abstract description 51
- 238000000034 method Methods 0.000 title claims abstract description 21
- 239000000843 powder Substances 0.000 title claims abstract description 21
- 238000001914 filtration Methods 0.000 claims abstract description 21
- 238000005374 membrane filtration Methods 0.000 claims abstract description 10
- 229910001385 heavy metal Inorganic materials 0.000 claims abstract description 6
- 238000004108 freeze drying Methods 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 6
- 241001494479 Pecora Species 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 239000004952 Polyamide Substances 0.000 claims description 4
- 229920002647 polyamide Polymers 0.000 claims description 4
- 238000001728 nano-filtration Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 abstract description 8
- 239000002994 raw material Substances 0.000 abstract description 7
- 150000001413 amino acids Chemical class 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 4
- 150000004676 glycans Chemical class 0.000 abstract description 4
- 229920001184 polypeptide Polymers 0.000 abstract description 4
- 229920001282 polysaccharide Polymers 0.000 abstract description 4
- 239000005017 polysaccharide Substances 0.000 abstract description 4
- 102000004196 processed proteins & peptides Human genes 0.000 abstract description 4
- 108090000765 processed proteins & peptides Proteins 0.000 abstract description 4
- 229960003080 taurine Drugs 0.000 abstract description 4
- 239000002699 waste material Substances 0.000 abstract description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 3
- 239000011707 mineral Substances 0.000 abstract description 3
- 229930003231 vitamin Natural products 0.000 abstract description 3
- 229940088594 vitamin Drugs 0.000 abstract description 3
- 235000013343 vitamin Nutrition 0.000 abstract description 3
- 239000011782 vitamin Substances 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract 1
- 238000010612 desalination reaction Methods 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 description 4
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 4
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- 102000015863 Nuclear Factor 90 Proteins Human genes 0.000 description 1
- 108010010424 Nuclear Factor 90 Proteins Proteins 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
- A23L17/50—Molluscs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/51—Concentration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/40—Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a method for extracting oyster powder from oyster cooking liquor. The oyster cooking liquor serves as raw materials of the oyster powder. The method comprises the steps that heavy metal in the oyster cooking liquor is removed at first, then vacuum concentration and plate frame filtration are conducted on the oyster cooking liquor, membrane filtration and desalination are conducted on the oyster cooking liquor, the oyster cooking liquor is frozen and dried, and the oyster powder is obtained at last. The raw materials of the oyster powder are the oyster cooking liquor which is waste produced in the oyster processing process, the raw material source is wide, and the waste produced in the oyster processing process is changed into the raw materials. The oyster powder has the abundant active ingredients such as soluble polysaccharide, polypeptide, taurine, free amino acid, various vitamins and mineral substances. The method is simple in extracting technology and suitable for industrial production.
Description
Technical field
The present invention relates to the extraction art field of ostreae testa pulverata.More specifically, relate to a kind of method of extracting ostreae testa pulverata from oyster cooking liquor.
Background technology
In recent years, along with the popularization of oyster culture technology and the expansion of the market demand, cultivation scale and the production and processing ability of oyster are largely increased.And oyster is in the process that is processed into oyster can, dried oyster, need through digesting technoloy.Oyster cooking liquor is exactly the discarded object producing in oyster process, and 1 ton of oyster product of general every processing, will produce the oyster cooking liquor of 1.5 tons of left and right.Oyster processing factory is generally located at seashore, a large amount of oyster cooking liquors is directly entered marine, causes the serious wasting of resources and environmental pollution.The abundant soluble polysaccharide containing in oyster cooking liquor after boiling, polypeptide, taurine, free amino acid, various vitamin and mineral matter isoreactivity composition; for a long time without utilizing or processing; all enter environment; enter the eutrophication that causes water quality behind sea, very serious to the pollution of environment.Therefore development and utilization oyster cooking liquor can make full use of resource, can reduce the pollution to environment again, turns waste into wealth.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of method of extracting ostreae testa pulverata from oyster cooking liquor, and the method extraction process is simple, and suitability for industrialized is produced.
Oyster cooking liquor of the present invention refers to the oyster cooking liquor that oyster produces in being processed into the digesting technoloy of the products such as oyster can, dried oyster; 1 ton of dried oyster of general every processing or 7 tons of oyster canned packs, will produce the oyster cooking liquor of 0.6 ton of left and right.Described oyster cooking liquor refers to the oyster cooking liquor that boiling 10-60min obtains at 100 ℃.
For solving the problems of the technologies described above, the present invention adopts following technical proposals:
From oyster cooking liquor, extract a method for ostreae testa pulverata, comprise following extraction step:
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: sheep is dwelt to dish 1-5 part (umber of the present invention is weight portion) through low temperature 30-45 ℃ oven dry, pulverize, sieving obtains 40-100 object Sangassivm fuciforime (Harv) Setch powder, described Sangassivm fuciforime (Harv) Setch powder is joined in 100 portions of oyster cooking liquors, stir;
(2) plate-frame filtering: diatomite 1-5 part is added in the cooking liquor that step (1) obtains and carried out plate-frame filtering;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the cooking liquor after plate-frame filtering, being concentrated into solid content is 22-27%;
(4) adopt polyamide nanofiltration membrane filtration that the salt content in the oyster cooking liquor after concentrated is removed to 1.6%, through freeze drying, obtain ostreae testa pulverata.
Preferably, the described mixing time of step (1) is 2 hours.
Preferably, the described plate-frame filtering pressure reduction of step (2) is 0.02-0.04MPa.
Preferably, the described concentration tank vacuum of step (3) is 0.07-0.09MPa; The temperature of concentration tank is 65-75 ℃.
Preferably, the operating pressure 1.5-2.5MPa of the described membrane filtration of step (4); Operating temperature is 25-35 ℃.
Preferably, the described freeze drying of step (4) comprises two stages: first stage freeze temperature is-25--35 ℃ that the time is 6-20h; Second stage baking temperature, adsorption stripping and dry temperature is 35-45 ℃, resolves time 8-25h.
Beneficial effect of the present invention is as follows:
(1) ostreae testa pulverata raw material of the present invention is the discarded object producing in oyster process--oyster cooking liquor, and raw material sources are wide, and being turns waste into wealth the discarded object in oyster production and processing.
(2) the abundant soluble polysaccharide that ostreae testa pulverata of the present invention contains, polypeptide, taurine, free amino acid, various vitamin and mineral matter isoreactivity composition.
(3) method extraction process is simple, and suitability for industrialized is produced.
The specific embodiment
In order to be illustrated more clearly in the present invention, below in conjunction with preferred embodiment, the present invention is described further.It will be appreciated by those skilled in the art that specifically described content is illustrative and nonrestrictive below, should not limit the scope of the invention with this.
Embodiment 1
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: 1 part of (umber of the present invention is weight portion) sheep is dwelt to dish through 30 ℃ of oven dry of low temperature, pulverize, sieving obtains Sangassivm fuciforime (Harv) Setch powder, and Sangassivm fuciforime (Harv) Setch powder is joined to 100 portions of oyster cooking liquors, stir 2 hours;
(2) plate-frame filtering: 1 part, diatomite is added in the cooking liquor that step (1) obtains and carries out plate-frame filtering; Plate-frame filtering pressure reduction is 0.02MPa;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the oyster cooking liquor after plate-frame filtering, being concentrated into solid content is 25%; Concentration tank vacuum is 0.08MPa; The temperature of concentration tank is 70 ℃;
(4) adopt polyamide nanofiltration membrane (model NF90, molecular cut off 90, film separating layer material: polyamide, cooking liquor temperature 25-40 ℃, pressure 1.5-3MPa) filter the salt content in the oyster cooking liquor after concentrated is removed to 1.6%, through freeze drying, obtain product ostreae testa pulverata.The operating pressure 1.5MPa of membrane filtration; Operating temperature is 25 ℃.The described cryodesiccated freeze temperature of step (4) is-35 ℃; Cryodesiccated second stage baking temperature, adsorption stripping and dry temperature is 45 ℃, resolves time 15h.
Each content of material of the ostreae testa pulverata that the embodiment of the present invention 1 obtains is as follows: soluble polysaccharide: 6.2g/100g; polypeptide: 65g/100g; fat: 2.3g/100g; taurine: 1.3/100g; free amino acid: 3.7/100g; vitamin E: 0.4mg/100g, inorganic salts: 7g/100g, oyster cooking liquor raw material per ton can obtain 120 kg ostreae testa pulverata.
Embodiment 2
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: 5 parts of (umber of the present invention is weight portion) sheep are dwelt to dish through 45 ℃ of oven dry of low temperature, pulverize, sieving obtains Sangassivm fuciforime (Harv) Setch powder, and Sangassivm fuciforime (Harv) Setch powder is joined to oyster cooking liquor, stir 2 hours;
(2) plate-frame filtering: 5 parts, diatomite is added in the cooking liquor that step (1) obtains and carries out plate-frame filtering; Plate-frame filtering pressure reduction is 0.04MPa;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the oyster cooking liquor after plate-frame filtering, being concentrated into solid content is 25%; Concentration tank vacuum is 0.08MPa; The temperature of concentration tank is 70 ℃;
(4) adopt membrane filtration that the salt content in the oyster cooking liquor after concentrated is removed to 1.6%, through freeze drying, obtain product ostreae testa pulverata.The operating pressure 2.5MPa of membrane filtration; Operating temperature is 35 ℃.The described freeze drying of step (4) comprises two stages: first stage freeze temperature is-35 ℃, and the time is 6h; Second stage baking temperature, adsorption stripping and dry temperature is 45 ℃, resolves time 20h.
Embodiment 3
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: 3 parts of (umber of the present invention is weight portion) sheep are dwelt to dish through 35 ℃ of oven dry of low temperature, pulverize, sieving obtains Sangassivm fuciforime (Harv) Setch powder, and Sangassivm fuciforime (Harv) Setch powder is joined to oyster cooking liquor, stir 2 hours;
(2) plate-frame filtering: 5 parts, diatomite is added in the cooking liquor that step (1) obtains and carries out plate-frame filtering; Plate-frame filtering pressure reduction is 0.03MPa;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the oyster cooking liquor after plate-frame filtering, being concentrated into solid content is 25%; Concentration tank vacuum is 0.07MPa; The temperature of concentration tank is 60 ℃;
(4) adopt membrane filtration that the salt content in the oyster cooking liquor after concentrated is removed to 1.6%, through freeze drying, obtain product ostreae testa pulverata.Wherein, the operating pressure 1.5MPa of membrane filtration; Operating temperature is 30 ℃.The described freeze drying of step (4) comprises two stages: first stage freeze temperature is-25 ℃, and the time is 20h; Second stage baking temperature, adsorption stripping and dry temperature is 35 ℃, resolves time 8h.
Obviously; the above embodiment of the present invention is only for example of the present invention is clearly described; and be not the restriction to embodiments of the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here cannot give all embodiments exhaustive, every still row in protection scope of the present invention of apparent variation that technical scheme of the present invention extends out or change that belong to.
Claims (6)
1. from oyster cooking liquor, extract a method for ostreae testa pulverata, it is characterized in that, the method comprises the following steps:
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: sheep is dwelt to dish 1-5 part through low temperature 30-45 ℃ oven dry, pulverize, sieving obtains 40-100 object Sangassivm fuciforime (Harv) Setch powder, described Sangassivm fuciforime (Harv) Setch powder is joined in 100 portions of oyster cooking liquors, stir;
(2) plate-frame filtering: diatomite 1-5 part is added in the cooking liquor that step (1) obtains and carried out plate-frame filtering;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the cooking liquor after plate-frame filtering, being concentrated into solid content is 22-27%;
(4) adopt polyamide nanofiltration membrane filtration that the salt content in the oyster cooking liquor after concentrated is removed to 1.6%, through freeze drying, obtain ostreae testa pulverata.
2. the method for extracting ostreae testa pulverata from oyster cooking liquor according to claim 1, is characterized in that, the described mixing time of step (1) is 1-3 hour.
3. the method for extracting ostreae testa pulverata from oyster cooking liquor according to claim 1, is characterized in that, the described plate-frame filtering pressure reduction of step (2) is 0.02-0.04MPa.
4. the method for extracting ostreae testa pulverata from oyster cooking liquor according to claim 1, is characterized in that, the described concentration tank vacuum of step (3) is 0.08MPa; The temperature of concentration tank is 70 ℃.
5. the method for extracting ostreae testa pulverata from oyster cooking liquor according to claim 1, is characterized in that, the operating pressure 1.5-2.5MPa of the described membrane filtration of step (4); Operating temperature is 25-35 ℃.
6. the method for extracting ostreae testa pulverata from oyster cooking liquor according to claim 1, is characterized in that, the described freeze drying of step (4) comprises two stages: first stage freeze temperature is-25--35 ℃ that the time is 6-20h; Second stage baking temperature, adsorption stripping and dry temperature is 35-45 ℃, resolves time 8-25h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410261829.7A CN104000243B (en) | 2014-06-13 | 2014-06-13 | A kind of method extracting Concha Ostreae powder from Concha Ostreae cooking liquor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410261829.7A CN104000243B (en) | 2014-06-13 | 2014-06-13 | A kind of method extracting Concha Ostreae powder from Concha Ostreae cooking liquor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104000243A true CN104000243A (en) | 2014-08-27 |
| CN104000243B CN104000243B (en) | 2016-07-06 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201410261829.7A Active CN104000243B (en) | 2014-06-13 | 2014-06-13 | A kind of method extracting Concha Ostreae powder from Concha Ostreae cooking liquor |
Country Status (1)
| Country | Link |
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| CN (1) | CN104000243B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104478765A (en) * | 2014-11-27 | 2015-04-01 | 山东好当家海洋发展股份有限公司 | Method for extracting taurine from poached oyster liquid |
| CN104544077A (en) * | 2015-01-09 | 2015-04-29 | 沈阳皇冠蓝莓生物科技有限公司 | Blueberry probiotic chewable tablet and preparation method thereof |
| CN105433337A (en) * | 2015-11-13 | 2016-03-30 | 集美大学 | Method for preparing seafood seasoning powder by using oyster and short necked clam cooking liquor |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104478765A (en) * | 2014-11-27 | 2015-04-01 | 山东好当家海洋发展股份有限公司 | Method for extracting taurine from poached oyster liquid |
| CN104478765B (en) * | 2014-11-27 | 2016-06-15 | 山东好当家海洋发展股份有限公司 | A kind of oyster water cooking liquid extracts the method for taurine |
| CN104544077A (en) * | 2015-01-09 | 2015-04-29 | 沈阳皇冠蓝莓生物科技有限公司 | Blueberry probiotic chewable tablet and preparation method thereof |
| CN104544077B (en) * | 2015-01-09 | 2017-02-01 | 沈阳皇冠蓝莓生物科技有限公司 | Blueberry probiotic chewable tablet and preparation method thereof |
| CN105433337A (en) * | 2015-11-13 | 2016-03-30 | 集美大学 | Method for preparing seafood seasoning powder by using oyster and short necked clam cooking liquor |
| CN105433337B (en) * | 2015-11-13 | 2018-07-27 | 集美大学 | A method of preparing seafood toppings using oyster and mottle clam cooking liquor |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104000243B (en) | 2016-07-06 |
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