CN104000246A - Method for extracting abalone active elements from abalone cooking liquor - Google Patents
Method for extracting abalone active elements from abalone cooking liquor Download PDFInfo
- Publication number
- CN104000246A CN104000246A CN201410261983.4A CN201410261983A CN104000246A CN 104000246 A CN104000246 A CN 104000246A CN 201410261983 A CN201410261983 A CN 201410261983A CN 104000246 A CN104000246 A CN 104000246A
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- abalone
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- 238000010411 cooking Methods 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title claims abstract description 22
- 238000001914 filtration Methods 0.000 claims abstract description 21
- 238000005374 membrane filtration Methods 0.000 claims abstract description 10
- 229910001385 heavy metal Inorganic materials 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims description 15
- 238000004108 freeze drying Methods 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 6
- 241001494479 Pecora Species 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 239000004952 Polyamide Substances 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- 229920002647 polyamide Polymers 0.000 claims description 4
- 238000001728 nano-filtration Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 7
- 150000001413 amino acids Chemical class 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 4
- 150000004676 glycans Chemical class 0.000 abstract description 4
- 229920001184 polypeptide Polymers 0.000 abstract description 4
- 229920001282 polysaccharide Polymers 0.000 abstract description 4
- 239000005017 polysaccharide Substances 0.000 abstract description 4
- 102000004196 processed proteins & peptides Human genes 0.000 abstract description 4
- 108090000765 processed proteins & peptides Proteins 0.000 abstract description 4
- 239000002699 waste material Substances 0.000 abstract description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 3
- 239000011707 mineral Substances 0.000 abstract description 3
- 229930003231 vitamin Natural products 0.000 abstract description 3
- 229940088594 vitamin Drugs 0.000 abstract description 3
- 235000013343 vitamin Nutrition 0.000 abstract description 3
- 239000011782 vitamin Substances 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000010612 desalination reaction Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- FGQYLXHJJYBZGT-UHFFFAOYSA-N Baohuosu Chemical compound COC1=C(O)C(OC)=CC(C=2OC3=C(CC=C(C)C)C(O)=CC(O)=C3C(=O)C=2)=C1 FGQYLXHJJYBZGT-UHFFFAOYSA-N 0.000 description 4
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 235000011194 food seasoning agent Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- JJWSNOOGIUMOEE-UHFFFAOYSA-N Monomethylmercury Chemical compound [Hg]C JJWSNOOGIUMOEE-UHFFFAOYSA-N 0.000 description 1
- 102000015863 Nuclear Factor 90 Proteins Human genes 0.000 description 1
- 108010010424 Nuclear Factor 90 Proteins Proteins 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 241000607768 Shigella Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 241000607272 Vibrio parahaemolyticus Species 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 229960003080 taurine Drugs 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
- A23L17/50—Molluscs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Marine Sciences & Fisheries (AREA)
- Zoology (AREA)
- Mycology (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The invention discloses a method for extracting abalone active elements from abalone cooking liquor. The abalone cooking liquor mainly serves as the main raw materials of the abalone active elements. The abalone active elements are obtained by removing heavy metal in the abalone cooking liquor, then conducting plate frame filtering, conducting membrane filtration and desalination and finally conducting cooling and drying The raw materials of the abalone active elements are the abalone cooking liquor which is waste produced in the abalone processing process, the raw material source is wide, and the waste produced in the abalone processing process is changed into the raw materials. The abalone active elements have the abundant active ingredients such as soluble polysaccharide, polypeptide, free amino acid, various vitamins and mineral substances. The method is simple in extracting technology and suitable for industrial production.
Description
Technical field
The present invention relates to the extractive technique field of Bao Huosu.More specifically, relate to a kind of Bao plain method alive of extracting from abalone cooking liquor.
Background technology
In recent years, along with the popularization of abalone culture technology and the expansion of the market demand, cultivation scale and the production and processing ability of abalone are largely increased.And abalone is in the process that is processed into abalone can, Bao Gan, instant seasoning Bao, need through digesting technoloy.Abalone cooking liquor is exactly the discarded object producing in abalone process, and 1 ton of abalone products of general every processing, will produce the abalone cooking liquor of 1.5 tons of left and right.Abalone processing factory is generally located at seashore, a large amount of abalone cooking liquors is directly entered marine, causes the serious wasting of resources and environmental pollution.The abundant soluble polysaccharide, polypeptide, free amino acid, various vitamin and the mineral matter isoreactivity composition that in abalone cooking liquor after boiling, contain, for a long time without utilizing or processing, all enter environment, enter the eutrophication that causes water quality behind sea, very serious to the pollution of environment.Therefore development and utilization abalone cooking liquor can make full use of resource, can reduce again the pollution to environment, turns waste into wealth.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of Bao plain method method alive of extracting from abalone cooking liquor, and the method extraction process is simple, and suitability for industrialized is produced.
Abalone cooking liquor of the present invention refers to that abalone is in the process that is processed into abalone can, Bao Gan, instant seasoning Bao, the abalone cooking liquor producing in digesting technoloy; Generally refer to the abalone cooking liquor that boiling 1-60min obtains at 80-100 DEG C, 1 ton of abalone products of common every processing, will produce the abalone cooking liquor of 1.5 tons of left and right.
For solving the problems of the technologies described above, the present invention adopts following technical proposals:
An extracting method of the Bao Huosu extracting in abalone cooking liquor, comprises following extraction step:
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: sheep is dwelt to dish 0.5-3 part through low temperature 30-45 DEG C oven dry, pulverize, sieving obtains 40-100 object Sangassivm fuciforime (Harv) Setch powder, and described Sangassivm fuciforime (Harv) Setch powder is joined to 100 portions of abalone cooking liquors, stir;
(2) plate-frame filtering: diatomite 1-3 part is added in the cooking liquor that step (1) obtains and carried out plate-frame filtering;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the abalone cooking liquor after plate-frame filtering, being concentrated into solid content is 16-25%;
(4) adopt polyamide nanofiltration membrane filtration that the salt content in the Bao cooking liquor after concentrated is removed to 1.6%, obtain product Bao through freeze drying and live plain.
Preferably, the described mixing time of step (1) is 1-3 hour.
Preferably, the described plate-frame filtering pressure reduction of step (2) is 0.02-0.04MPa.
Preferably, the described concentration tank vacuum of step (3) is 0.08MPa; The temperature of concentration tank is 70 DEG C; More preferably, described concentration time is 6h.
Preferably, the operating pressure 1.5-2.5MPa of the described membrane filtration of step (4); Operating temperature is 25-35 DEG C.
Preferably, the described freeze drying of step (4) comprises two stages: first stage freeze temperature is-25--35 DEG C that the time is 6-20h; Second stage baking temperature, adsorption stripping and dry temperature is 35-45 DEG C, resolves time 10-25h.
Beneficial effect of the present invention is as follows:
(1) Bao of the present invention plain raw material alive is the discarded object producing in abalone process--abalone cooking liquor, and raw material sources are wide, and being turns waste into wealth the discarded object in abalone production and processing.
(2) Bao of the present invention element alive contains abundant soluble polysaccharide, polypeptide, free amino acid, various vitamin and mineral matter isoreactivity composition.
(3) method extraction process is simple, and suitability for industrialized is produced.
Detailed description of the invention
In order to be illustrated more clearly in the present invention, below in conjunction with preferred embodiment, the present invention is described further.It will be appreciated by those skilled in the art that specifically described content is illustrative and nonrestrictive below, should not limit the scope of the invention with this.
Embodiment 1
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: (umber of the present invention is weight portion) sheep is dwelt to dish through 30 DEG C of oven dry of low temperature, pulverize, sieving obtains Sangassivm fuciforime (Harv) Setch powder, and 1 part of Sangassivm fuciforime (Harv) Setch powder is joined to 100 portions of abalone cooking liquors, stir 2 hours;
(2) plate-frame filtering: 1 part, diatomite is added in the cooking liquor that step (1) obtains and carries out plate-frame filtering; Plate-frame filtering pressure reduction is 0.02MPa;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the abalone cooking liquor after plate-frame filtering, being concentrated into solid content is 25%; Concentration tank vacuum is 0.08MPa; The temperature of concentration tank is 70 DEG C;
(4) adopt polyamide nanofiltration membrane (described film model NF90, molecular cut off 90, film separating layer material: polyamide, cooking liquor temperature 25-40 DEG C, pressure 1.5-3MPa) filter the salt content in the abalone cooking liquor after concentrated is removed to 1.8% by 6.7%, obtain the product Bao element of living through freeze drying.The operating pressure 1.5MPa of membrane filtration; Operating temperature is 25 DEG C.The described cryodesiccated freeze temperature of step (4) is-35 DEG C; Cryodesiccated second stage baking temperature, adsorption stripping and dry temperature is 45 DEG C, resolves time 15h.Abalone cooking liquor raw material per ton obtains 105 kg Bao and lives plain.
After testing, in the Bao element alive that the embodiment of the present invention 1 obtains, each content of material is:
Soluble polysaccharide: 8.6g/100g, soluble protein and polypeptide: 63g/100g, fat: 2.7g/100g, taurine: 0.6g/100g, free amino acid: 3.3g/100g, vitamin E: 0.4mg/100g, inorganic salts: 8.6g/100g, plumbous (in Pb): 0.14mg/kg, cadmium (in Cd): 0.21mg/kg, chromium (in Cr): 0.07mg/kg, methyl mercury (in Hg): 0.08mg/kg, inorganic arsenic (in As): 0.19mg/kg, pathogenic bacteria (salmonella, staphylococcus aureus, vibrio parahemolyticus, Shigella) without detecting.
Embodiment 2
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: sheep is dwelt to dish through 45 DEG C of oven dry of low temperature, pulverize, sieving obtains Sangassivm fuciforime (Harv) Setch powder, and 5 parts of Sangassivm fuciforime (Harv) Setch powders are joined to 100 portions of abalone cooking liquors, stir 2 hours;
(2) plate-frame filtering: 5 parts, diatomite is added in the cooking liquor that step (1) obtains and carries out plate-frame filtering; Plate-frame filtering pressure reduction is 0.04MPa;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the abalone cooking liquor after plate-frame filtering, being concentrated into solid content is 25%; Concentration tank vacuum is 0.08MPa; The temperature of concentration tank is 70 DEG C;
(4) adopt membrane filtration that the salt content in the abalone cooking liquor after concentrated is removed to 1.8%, obtain product Bao through freeze drying and live plain.The operating pressure 2.5MPa of membrane filtration; Operating temperature is 35 DEG C.First stage freeze temperature is-35 DEG C, and the time is 20h; Second stage baking temperature, adsorption stripping and dry temperature is 45 DEG C, resolves time 25h.
Embodiment 3
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: (umber of the present invention is weight portion) sheep is dwelt to dish through 35 DEG C of oven dry of low temperature, pulverize, sieving obtains Sangassivm fuciforime (Harv) Setch powder, and 3 parts of Sangassivm fuciforime (Harv) Setch powders are joined to 100 portions of abalone cooking liquors, stir 2 hours;
(2) plate-frame filtering: 5 parts, diatomite is added in the cooking liquor that step (1) obtains and carries out plate-frame filtering; Plate-frame filtering pressure reduction is 0.03MPa;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the abalone cooking liquor after plate-frame filtering, being concentrated into solid content is 25%; Concentration tank vacuum is 0.07MPa; The temperature of concentration tank is 60 DEG C;
(4) adopt membrane filtration that the salt content in the abalone cooking liquor after concentrated is removed to 1.6%, obtain product Bao through freeze drying and live plain.Wherein, the operating pressure 1.5MPa of membrane filtration; Operating temperature is 30 DEG C.First stage freeze temperature is-25 DEG C, and the time is 6h; Second stage baking temperature, adsorption stripping and dry temperature is 35 DEG C, resolves time 10h.
Obviously; the above embodiment of the present invention is only for example of the present invention is clearly described; and be not the restriction to embodiments of the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here cannot give all embodiments exhaustively, everyly belong to apparent variation or the still row in protection scope of the present invention of variation that technical scheme of the present invention extends out.
Claims (6)
1. from abalone cooking liquor, extract a Bao plain method alive, it is characterized in that, comprise following extraction step:
(1) Sangassivm fuciforime (Harv) Setch powder removes heavy metal: sheep is dwelt to dish 0.5-3 part through low temperature 30-45 DEG C oven dry, pulverize, sieving obtains 40-100 object Sangassivm fuciforime (Harv) Setch powder, and described Sangassivm fuciforime (Harv) Setch powder is joined to 100 portions of abalone cooking liquors, stir;
(2) plate-frame filtering: diatomite 1-3 part is added in the cooking liquor that step (1) obtains and carried out plate-frame filtering;
(3) reduced pressure concentration: use vacuum decompressioning and concentrating tank to carry out reduced pressure concentration the abalone cooking liquor after plate-frame filtering, being concentrated into solid content is 16-25%;
(4) adopt polyamide nanofiltration membrane filtration that the salt content in the Bao cooking liquor after concentrated is removed to 1.6%, obtain product Bao through freeze drying and live plain.
2. the Bao plain method alive of extracting from abalone cooking liquor according to claim 1, is characterized in that, the described mixing time of step (1) is 1-3 hour.
3. the Bao plain method alive of extracting from abalone cooking liquor according to claim 1, is characterized in that, the described plate-frame filtering pressure reduction of step (2) is 0.02-0.04MPa.
4. the Bao plain method alive of extracting from abalone cooking liquor according to claim 1, is characterized in that, the described concentration tank vacuum of step (3) is 0.08MPa; The temperature of concentration tank is 70 DEG C.
5. the Bao plain method alive of extracting from abalone cooking liquor according to claim 1, is characterized in that the operating pressure 1.5-2.5MPa of the described membrane filtration of step (4); Operating temperature is 25-35 DEG C.
6. the Bao plain method alive of extracting from abalone cooking liquor according to claim 1, is characterized in that, the described freeze drying of step (4) comprises two stages: first stage freeze temperature is-25--35 DEG C that the time is 6-20h; Second stage baking temperature, adsorption stripping and dry temperature is 35-45 DEG C, resolves time 8-25h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410261983.4A CN104000246A (en) | 2014-06-13 | 2014-06-13 | Method for extracting abalone active elements from abalone cooking liquor |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410261983.4A CN104000246A (en) | 2014-06-13 | 2014-06-13 | Method for extracting abalone active elements from abalone cooking liquor |
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| CN104000246A true CN104000246A (en) | 2014-08-27 |
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| CN201410261983.4A Pending CN104000246A (en) | 2014-06-13 | 2014-06-13 | Method for extracting abalone active elements from abalone cooking liquor |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104970342A (en) * | 2015-07-14 | 2015-10-14 | 福建省水产研究所 | Abalone viscus sauce and processing method thereof |
| CN104982887A (en) * | 2015-07-23 | 2015-10-21 | 福建省水产研究所 | Fresh abalone element and preparation method therefor |
| CN105732837A (en) * | 2016-03-29 | 2016-07-06 | 福建农林大学 | Method for preparing abalone harslet polysaccharide powder for removing proteins and heavy metals |
| CN108402415A (en) * | 2017-10-18 | 2018-08-17 | 广东海洋大学 | The peptide that detaches preparation in abalone processed side product is anti-oxidant, antihypertensive function and application |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104970342A (en) * | 2015-07-14 | 2015-10-14 | 福建省水产研究所 | Abalone viscus sauce and processing method thereof |
| CN104970342B (en) * | 2015-07-14 | 2017-04-26 | 福建省水产研究所 | Abalone viscus sauce and processing method thereof |
| CN104982887A (en) * | 2015-07-23 | 2015-10-21 | 福建省水产研究所 | Fresh abalone element and preparation method therefor |
| CN105732837A (en) * | 2016-03-29 | 2016-07-06 | 福建农林大学 | Method for preparing abalone harslet polysaccharide powder for removing proteins and heavy metals |
| CN105732837B (en) * | 2016-03-29 | 2018-02-06 | 福建农林大学 | A kind of isolating protein goes the preparation method of the abalone internal organs polysaccharide powder of heavy metal |
| CN108402415A (en) * | 2017-10-18 | 2018-08-17 | 广东海洋大学 | The peptide that detaches preparation in abalone processed side product is anti-oxidant, antihypertensive function and application |
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Application publication date: 20140827 |
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