CN103961301A - Gynura procumbens use-activated multiactive natural compound mask and preparation method thereof - Google Patents
Gynura procumbens use-activated multiactive natural compound mask and preparation method thereof Download PDFInfo
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- CN103961301A CN103961301A CN201410234943.0A CN201410234943A CN103961301A CN 103961301 A CN103961301 A CN 103961301A CN 201410234943 A CN201410234943 A CN 201410234943A CN 103961301 A CN103961301 A CN 103961301A
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Abstract
The invention belongs to the field of cosmetics and in particular relates to a gynura procumbens use-activated multiactive natural compound mask and a preparation method thereof. The gynura procumbens use-activated multiactive natural compound mask is characterized by being prepared from the following raw materials in percentage by weight: 93-96% of gynura procumbens extract, 0.5-1.5% of camellia oil, 2.5-5% of abehnoschl manihot honey and 0.3-1% of rosemary. The gynura procumbens extract is taken as a main component, and a small amount of functional plant essence auxiliary material is added. The gynura procumbens use-activated multiactive natural compound mask can realize the moisturizing, whitening, antiwrinkling, antisepsis and anti-inflammation, lifting and tightening, spot solution and anti-acne effects on human skin, no artificial additive is added, and a preparation method is simple.
Description
Technical field
The invention belongs to cosmetic field, relate in particular to a kind of Gynura procumbens (Lour.) Merr. and imitate natural compound recipe facial film of polynary maintenance and preparation method thereof.
Background technology
Traditional making face mask method is: 1, extraction process: western developed country mostly adopts water extraction in conjunction with dynamic warm macerating technique and is aided with advanced equipment, and domestic conventional organic solvents or the decocting high temperature extraction technique of adopting, and equipment is fallen behind mostly. moreExist complex process, solvent consume shortcoming, particularly many compositions large, that extraction efficiency is low, energy consumption is high, pollution is heavy to be subject to pyrolytic and to destroy.2, from material composition: adding numerous additives by various plants extract again and mix, is to be main flow kind on market at present.But because extract kind is more, molecular structure is large, different intermolecular interactions, easily produce oxidation, and poor stability, be easily subject to many factors, as air, temperature, matrix components, formula etc., easily phase mutual interference and character changes between factor, destroy extract characteristic, thereby reduce facial film, use effect; Also make facial film function singleness simultaneously.3, from additive: due to production and sales excessive cycle, need to add the chemical substances such as other chemical preservative, pigment, activating agent, the facial film of existing market is oils and fats, surfactant, anticorrosion and bactericidal agent, antioxidant, pigment, spice etc. substantially.Specifically functional cosmetics also must add wetting agent, viscosifier, astringent, antioxidation auxiliary agent, bleach, UV absorbent etc., and these raw materials are mostly chemical substances, be that human body is produced to acute and chronic harm, greatly reduce purity, safety and the mildness of product.4, artificial odor additive: artificial flavors is cheap, stable in properties; Natural spice is expensive and output is limited.So in order to save cost and to keep the concordance of product odor type conventionally can select artificial essence to add in skin care item, artificial essence easily causes skin allergy inflammation, infringement nervous system and hemopoietic system.Superior cosmetics, the compositions such as contained spice are more complicated, and sensitization chance is just more.5,, from the adaptability of ethnic group skin quality between east and west: Hesperian cosmetics are to do experiment white people, be applicable to white people's skin with it.And Asians is different from westerner's skin quality, thinner more careful, by contrast, Asians's skin is easy to allergy to their cosmetics, so, imported goods is directly brought to use, untoward reaction meeting increases; 6, from service time: the common facial film application time is longer, is generally 20-30 minute.Make a general survey of American-European cosmetics, the overwhelming majority contains chemical analysis additive and consists of many kinds of substance, and the incompatibility exclusiveness of material makes its cosmetics zest large, and the interpolation of antiseptic allows the user of sensitive skin, and future trouble is poor without rising especially.
In recent years, along with raising and the rhythm of life of people's living standard are accelerated, take active components of plants as main pure natural and short facial film skin care item of nursing time, the parent who is more and more subject to consumer looks at.Natural, green, to have no side effect and have the plant skin care item of multiple physiological, Nutrition be now required.
Summary of the invention
In order to solve above technical problem, the invention provides a kind of green, health, natural pure plant mask and the preparation method with multiple efficacies, to human body skin can play moisturizing, brighten wrinkle resistant, anti-inflammation, lift compact, light speckle acne removing, and do not add any man-made additive.
A kind of Gynura procumbens (Lour.) Merr. solving in the present invention of above technical problem imitates natural compound recipe facial film of polynary maintenance and preparation method thereof, it is characterized in that: Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 93-96%, Camellia oil 0.5-1.5%, wild Hibisci Mutabilis Mel 2.3-5%, Herba Rosmarini Officinalis 0.3-1%.Take Gynura procumbens (Lour.) Merr. extract as the main plant essence liquid adjuvant that adds a small amount of function.
Also can by following percentage by weight raw material, be formed by Gynura procumbens (Lour.) Merr. facial film: Gynura procumbens (Lour.) Merr. extract 94-95.5%, Camellia oil 0.8-1.5%, wild Hibisci Mutabilis Mel 3-4%, Herba Rosmarini Officinalis 0.4-0.7%.。
Prioritization scheme can be Gynura procumbens (Lour.) Merr. facial film and is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 95%, Camellia oil 1%, wild Hibisci Mutabilis Mel 3.5%, Herba Rosmarini Officinalis 0.5%.
The manufacture method of the Gynura procumbens (Lour.) Merr. facial film in the present invention is: comprise the following steps:
(1) prepare raw material and weigh: choosing fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby;
(2) extract Gynura procumbens (Lour.) Merr. extract: the Gynura procumbens (Lour.) Merr. in step (1) is ground into after constant temperature 40-55 ℃ of dry 15-25min to 16-20 order granule sieving for standby; Pulverize too carefully, obstruction filtering holes easily hardens; Too thick, solvent is difficult for it fully reaction, can not reach optimum extraction state.
(3) in step (2) container, add ethanol, the Gynura procumbens (Lour.) Merr. granule of concentration 70% again, with the feed liquid ratio of 1:15-30, with ultrasonic instrument, extract 24-40min, power 200w, extracts 2 times continuously, filters, and obtains Gynura procumbens (Lour.) Merr. extract; In the present invention, reasonably liquid example is higher than making extract obtain the effective component extraction rates such as chlorogenic acid, flavone.
(4) in the Gynura procumbens (Lour.) Merr. extract of step (2), add Camellia oil, wild Hibisci Mutabilis Mel, Herba Rosmarini Officinalis, with high-speed emulsifying homogeneous machine uniform stirring 25-40min;
(5) sterilization, sterilizing room fill, the shady and cool place of room temperature lucifuge preserves.
After dry in step (2) described in prioritization scheme in the present invention, Gynura procumbens (Lour.) Merr. water content remains on initial weight 50%-70%.While keeping certain moisture to extract, play lubricated effect, can make its nutritional cost can not destroy because of excessive dehydration simultaneously.Also have, in described step (3), solid-liquid ratio is 1:20.
Described step (3) extraction time is 40min.
In the present invention, in Gynura procumbens (Lour.) Merr. extraction, efficiency is high, impels plant cell tissue's breaking cellular wall or distortion, makes extracts active ingredients more abundant, and extraction ratio significantly improves and reaches 200-250% than traditional handicraft; Extraction time is short: at 24-40 minute, can obtain optimum extraction rate, extraction time shortens more than 2/3 greatly compared with traditional method, and raw material disposal amount is large; Extraction temperature is low: supersound extraction optimum temperature, at 40-55 ℃, has protective effect to the effective ingredient of case of thermal instability, facile hydrolysis or oxidation, simultaneously greatly energy-conservation energy consumption; In Gynura procumbens (Lour.) Merr. extract, impurity is few, and effective ingredient is easy to separation, purification.
Gynura procumbens (Lour.) Merr. imitates the single plant extract of the natural compound recipe facial film of polynary maintenance, integrate numerous effective ingredient and can, as chlorogenic acid and neochlorogenic acid, vitamin C, B1, B2, Squalene, tea polyphenols, several amino acids, plant collagen, preserved the superpower activity of plant extraction liquid.
Facial film in the present invention becomes to belong to the fresh-keeping composition of natural disinfection, contains chlorogenic acid, Squalene, tea polyphenols etc., has anti-inflammation and sterilization effect, facial film does not add antiseptic and fresh-keeping composition, and do not add any chemical substance, the pure gentleness of matter, has reduced allergy or malaise symptoms.
In Gynura procumbens (Lour.) Merr. extract: be rich in the significant surfaces such as plant collagen, chlorogenic acid, natural plants flavonoid and divide.
In Camellia oil: plant squalene: antioxidation, remove in body by base, promote skin histology metabolism, improve xerosis cutis coarse, alleviate psoriasis and this class dermatopathy of dermatitis, there is the effect such as build up resistance of defying age, repair cell
.tea saponin has inhibitory action to the dermopathic Mycophyta of multiple initiation and escherichia coli.Tea poly phenol detoxicating and radiation resistance, antioxidation, removes the greasy of face, convergence pore, check melanin forms.The trace element such as rich in vitamin E and calcium, ferrum, zinc.
Wild Hibisci Mutabilis Mel: can remove interior free yl, add it and contain the trace element such as abundant vitamin A, C, E and selenium, zinc, copper, magnesium, be natural antioxidant, can fundamentally remove the too much free radical of cylinder accumulation.Can effectively suppress lipofuscin, dispel freckle.Also contain a large amount of biological flavones, antimicrobial component is more, and antibacterial is also had to inhibition widely.
Herba Rosmarini Officinalis: rosemary ethereal oil has very strong contraction, tightens lax skin, also can alleviate the situation of hyperemia, swelling.
This facial film is pure plant component, and nutritional labeling and purity are high, and application time shorten is about 5-10 minute, adapts to very much the allegro life style of modern.And utilize the characteristic of the fresh-keeping moisturizing of the composition sterilizing of pure plant mask own, solve the high efficiency of the stable composition of facial film itself and the concertedness of surfactant and sterilization.
The present invention has kept whole nutritional labelings of natural plants nutrient material, so the nutritional labeling in facial film is more complete, effect is more polynary, has that good permeance property, seepage velocity are fast, a good absorbing, instant effect, result of use outstanding feature.
The specific embodiment
Embodiment 1
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 93.5%, Camellia oil 1.5%, wild Hibisci Mutabilis Mel 4%, Herba Rosmarini Officinalis 1%.Take Gynura procumbens (Lour.) Merr. extract as the main plant essence liquid adjuvant that adds a small amount of function.
Prepare raw material and weigh: choosing fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby; Above-mentioned Gynura procumbens (Lour.) Merr. is ground into after 40 ℃ of dry 20min of constant temperature to 18 order granule sieving for standby; The ethanol, the Gynura procumbens (Lour.) Merr. granule that in container, add concentration 70%, with the feed liquid ratio of 1:20, extract 40min with ultrasonic instrument again, and power 200w extracts 2 times continuously, filters, and obtains Gynura procumbens (Lour.) Merr. extract.During pulverizing, Gynura procumbens (Lour.) Merr. granule order is too thin, easily stops up filtering holes during filtration, too large, and during extraction, separating out of limited composition is not best, makes Gynura procumbens (Lour.) Merr. effective ingredient obtain best precipitation state; In Gynura procumbens (Lour.) Merr. extract, add Camellia oil, wild Hibisci Mutabilis Mel, Herba Rosmarini Officinalis, with high-speed emulsifying homogeneous machine uniform stirring 30min; Sterilization, sterilizing room fill, the shady and cool place of room temperature lucifuge preserves.
Embodiment 2
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: 96%, and Camellia oil 0.5%, wild Hibisci Mutabilis Mel 3.2%, Herba Rosmarini Officinalis 0.3%.Take Gynura procumbens (Lour.) Merr. extract as the main plant essence liquid adjuvant that adds a small amount of function.Choose fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby; Above-mentioned Gynura procumbens (Lour.) Merr. is ground into after 55 ℃ of dry 15min of constant temperature to 16 order granule sieving for standby; The ethanol, the Gynura procumbens (Lour.) Merr. granule that in container, add concentration 70%, with the feed liquid ratio of 1:15, extract 24min with ultrasonic instrument again, and power 200w extracts 2 times continuously, filters, and obtains Gynura procumbens (Lour.) Merr. extract.In Gynura procumbens (Lour.) Merr. extract, add Camellia oil, wild Hibisci Mutabilis Mel, Herba Rosmarini Officinalis, with high-speed emulsifying homogeneous machine uniform stirring 25min; Sterilization, sterilizing room fill, the shady and cool place of room temperature lucifuge preserves.
Embodiment 3
Also can by following percentage by weight raw material, be formed by Gynura procumbens (Lour.) Merr. facial film: Gynura procumbens (Lour.) Merr. extract 94%, Camellia oil 1.3%, wild Hibisci Mutabilis Mel 4%, Herba Rosmarini Officinalis 0.7%.
Choose fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby; Above-mentioned Gynura procumbens (Lour.) Merr. is ground into after 50 ℃ of dry 25min of constant temperature to 20 order granule sieving for standby; The ethanol, the Gynura procumbens (Lour.) Merr. granule that in container, add concentration 70%, with the feed liquid ratio of 1:20, extract 30min with ultrasonic instrument again, and power 200w extracts 2 times continuously, filters, and obtains Gynura procumbens (Lour.) Merr. extract.In Gynura procumbens (Lour.) Merr. extract, add Camellia oil, wild Hibisci Mutabilis Mel, Herba Rosmarini Officinalis, with high-speed emulsifying homogeneous machine uniform stirring 20min; Sterilization, sterilizing room fill, the shady and cool place of room temperature lucifuge preserves.
Embodiment 4
Also can by following percentage by weight raw material, be formed by Gynura procumbens (Lour.) Merr. facial film: Gynura procumbens (Lour.) Merr. extract 95.5%, Camellia oil 0.8%, wild Hibisci Mutabilis Mel 3.3%, Herba Rosmarini Officinalis 0.4%.
Choose fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby; Above-mentioned Gynura procumbens (Lour.) Merr. is ground into after 50 ℃ of dry 18min of constant temperature to 18 order granule sieving for standby, dry 50 ℃, 18 orders are to pulverize optimum baking temperature and pulverize order number; The ethanol, the Gynura procumbens (Lour.) Merr. granule that in container, add concentration 70%, with the feed liquid ratio of 1:25, extract 35min with ultrasonic instrument again, and power 200w extracts 2 times continuously, filters, and obtains Gynura procumbens (Lour.) Merr. extract.In Gynura procumbens (Lour.) Merr. extract, add Camellia oil, wild Hibisci Mutabilis Mel, Herba Rosmarini Officinalis, with high-speed emulsifying homogeneous machine uniform stirring 25min; Sterilization, sterilizing room fill, the shady and cool place of room temperature lucifuge preserves.
Embodiment 5
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 95%, Camellia oil 1%, wild Hibisci Mutabilis Mel 3.5%, Herba Rosmarini Officinalis 0.5%.
Preparation method is for implementing in 1.
Embodiment 6
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 94.8%, Camellia oil 1.1%, wild Hibisci Mutabilis Mel 3.4%, Herba Rosmarini Officinalis 0.7%.
Preparation method is for implementing in 1.
Embodiment 7
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 95.3%, Camellia oil 0.9%, wild Hibisci Mutabilis Mel 3.2%, Herba Rosmarini Officinalis 0.6%.
Preparation method is for implementing in 1.
Embodiment 8
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 93%, Camellia oil 1.5%, wild Hibisci Mutabilis Mel 4.6%, Herba Rosmarini Officinalis 0.9%.
Preparation method is for implementing in 1.Gynura procumbens (Lour.) Merr. extract 93-96%, Camellia oil 0.5-1.5%, wild Hibisci Mutabilis Mel 2.3-5%, Herba Rosmarini Officinalis 0.3-1%.Take Gynura procumbens (Lour.) Merr. extract as the main plant essence liquid adjuvant that adds a small amount of function.
Also can by following percentage by weight raw material, be formed by Gynura procumbens (Lour.) Merr. facial film: Gynura procumbens (Lour.) Merr. extract 94-95.5%, Camellia oil 0.8-1.5%, wild Hibisci Mutabilis Mel 3-4%, Herba Rosmarini Officinalis 0.4-0.7%.。
Embodiment 9
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 96%, Camellia oil 0.6%, wild Hibisci Mutabilis Mel 3%, Herba Rosmarini Officinalis 0.4%.
Preparation method is for implementing in 1.
Embodiment 10
Prepare the Gynura procumbens (Lour.) Merr. facial film of 10 jin
Formula is: 9.4 jin of Gynura procumbens (Lour.) Merr. extracts, 0.15 jin of Camellia oil, 0.35 jin of wild Hibisci Mutabilis Mel, 0.1 jin of rosemary ethereal oil.
Preparation method is: 1, choose fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby; 2, extract Gynura procumbens (Lour.) Merr. extract: the Gynura procumbens (Lour.) Merr. in step 1 is ground into after constant temperature 40-55 ℃ of dry 15-25min to 16-20 order granule sieving for standby; 3,94 jin of fresh Gynura procumbens (Lour.) Merr. are adopted to ultrasonic extraction, extraction process condition is: take solid-liquid ratio as 1:20, ultrasonic power is 200w, extraction time 20min, extract 2 times continuously, after filtration, take 9.4 jin of Gynura procumbens (Lour.) Merr. extracts, the extraction ratio of its extract main component chlorogenic acid, plant flavonoids can reach 90%.4, each raw material is weighed by proportioning, pour extract into 20L rustless steel container, separately by 0.15 jin of Camellia oil, 0.35 jin of wild Hibisci Mutabilis Mel, 0.1 jin of rosemary ethereal oil are poured in this rustless steel container, with high-speed emulsifying homogeneous machine, stir, under room temperature, carry out fill, obtain finished product.
Embodiment 11
Prepare the Gynura procumbens (Lour.) Merr. facial film of 10 jin
Formula is: 93 jin of Gynura procumbens (Lour.) Merr. extracts, 0.12 jin of Camellia oil, 0.5 jin of wild Hibisci Mutabilis Mel, 0.08 jin of rosemary ethereal oil.
Preparation method is: other method is with embodiment 10, accurately take 9.3 jin of Gynura procumbens (Lour.) Merr. extracts, each raw material is weighed by proportioning, pour extract into 20L rustless steel container, separately, by 0.12 jin of Camellia oil, 0.5 jin of wild Hibisci Mutabilis Mel, 0.08 jin of rosemary ethereal oil are poured in this rustless steel container, with high-speed emulsifying homogeneous machine, stir, under room temperature, carry out fill, obtain finished product.
Embodiment 12
Prepare the Gynura procumbens (Lour.) Merr. facial film of 10 jin
Formula is: 96 jin of Gynura procumbens (Lour.) Merr. extracts, 0.1 jin of Camellia oil, 0.23 jin of wild Hibisci Mutabilis Mel, 0.07 jin of rosemary ethereal oil.
Preparation method is: preparation method is: other method is with embodiment 10, accurately take 9.6 jin of Gynura procumbens (Lour.) Merr. extracts, each raw material is weighed by proportioning, pour extract into 20L rustless steel container, separately, by 0.1 jin of Camellia oil, 0.23 jin of wild Hibisci Mutabilis Mel, 0.07 jin of rosemary ethereal oil are poured in this rustless steel container, with high-speed emulsifying homogeneous machine, stir, under room temperature, carry out fill, obtain finished product.
Facial film performance indications in table 1 the present invention
Gynura procumbens (Lour.) Merr. imitates the single plant extract of the natural compound recipe facial film of polynary maintenance, integrate numerous effective ingredient and can, as chlorogenic acid and neochlorogenic acid, vitamin C, B1, B2, Squalene, tea polyphenols, several amino acids, plant collagen, preserved the superpower activity of plant extraction liquid.The whole nutritional labelings that kept natural plants nutrient material, so the nutritional labeling in facial film is more complete, effect is more polynary, has that good permeance property, seepage velocity are fast, a good absorbing, instant effect, result of use outstanding feature.
Embodiment 13
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 100%, preparation method is as embodiment 1.
Embodiment 14
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 95%, Camellia oil 5%.Preparation method is as embodiment 1.
Embodiment 15
Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 95%, Camellia oil 1%, wild Hibisci Mutabilis Mel 4%.Preparation method is as embodiment 1.
Table 2 embodiment 13-15 and embodiment 5 Contrast on effect tables:
Experimental design 1:
Choose men and women totally 35 people try out, skin type comprises mixed type skin, oiliness skin, dryness skin, according to the classification of its skin problem, is divided into 5 groups, every group of 7 people, smear once every day, each 10 minutes.Trial effect is just as following table 3:
The effect of table 3 trial edition invention facial film
Gynura procumbens (Lour.) Merr. facial film successively, through the thousands of inferior subsides skin tests repeatedly of 70 people, proves Gynura procumbens (Lour.) Merr. facial film
Belong to hyposensitivity draft medicine adornment product.By drawing, can show that Gynura procumbens (Lour.) Merr. facial film of the present invention is by utilizing effective medicinal ingredient in Gynura procumbens (Lour.) Merr., be applicable to any skin quality, from at the bottom of flesh, for skin, carry nutritional labeling, nourish lastingly, go deep into maintenance, solve that skin is tight, decortication, lack gloss problem.
Gynura procumbens (Lour.) Merr. facial film in the present invention, contained chlorogenic acid, aminoacid, flavonoid, water soluble dietary fiber, Calcium in Plants with ferrum, zinc and vitamin C, B1, etc.The useful material of so multipair human body is integrated in one, and symbiotic co-existence supports mutually.Wherein effective active component, can play the effect of anti-inflammation, removing oils and fats and dirt.And it is well releived and therapeutic effect in addition, be particularly suitable for the skin that corse sweat pore, the colour of skin are dark and gloomy, have bean scar, can blood circulation promoting, accelerate metabolism, thus play treatment skin, restorative effect.This facial film is all gentle especially, is applicable to comprising any skin of responsive skin, non-stimulated.
Experimental design 2: Gynura procumbens (Lour.) Merr. Content of Chlorogenic Acid antibacterial experiment
Test raw material
Gynura procumbens (Lour.) Merr. leaf is dried grinding and sieving 40 orders, and packing Gynura procumbens (Lour.) Merr. chlorogenic acid purity after standby purification is 87.47%.
Bacteriostatic experiment method
(1) configuration of culture medium
Antibacterial culture medium: Carnis Bovis seu Bubali cream albumen knee joint agar culture medium: Carnis Bovis seu Bubali cream 5g, albuminous glands lOg, sodium chloride 5g, agar 20g, pH modulation 7.2, water lOOOmL.Yeast culture medium: bean sprout culture medium: Semen Glycines Germinatus lOOg, glucose 50g, agar 20g, water lOOOmL.Aspergillus niger culture medium: Rhizoma Solani tuber osi culture medium: Rhizoma Solani tuber osi 200g, glucose 20g, agar 20g, water lOOOmL.
(2) preparation of bacteria suspension
With inoculating loop picking one, encircle thalline after actication of culture or spore is put in 50mL sterilized water, add bead shake well 2min, make bacteria containing amount be about 109-10i<: bacteria suspension or the spore suspension of fWmL are standby.
(3) configuration of feed flow test solution
By gained extract and purity, be that 87.47% chlorogenic acid is respectively got 0.32g, with 4mL acetone solution, obtain respectively the medicinal liquid of 80mg/mL, the acetone of take again carries out respectively two-fold dilution three times to every kind of solution of above-mentioned 80mg/mL as solvent, every kind of extract obtain 80mg/mL, 40mg/mL, tri-Concentraton gradient of 20mg/mL for reagent liquid acetone in contrast.
The preparation of plating medium
By the culture medium high pressure steam sterilization preparing, (rc, adopts sterile working to pour in sterilizing culture dish, every culture dish dress 15-20 mL to be cooled to 50-6.Cryopreservation is standby afterwards.
Extracorporeal bacteria inhibitor test
Consider that confession reagent liquid is limited, this test adopts filter paper method.Selecting high-quality filter paper diameter is 12mm circular paper, 121 ° of C autoclaving 30min, then (rC is dried, and is placed in exsiccator standby through 8.Get the scraps of paper that prepare and put into respectively the test liquid of variable concentrations, after immersion 2h, take out.Every kind of each confession examination bacterium of concentration is established 3 repetitions.Then be placed in 37 ° of C constant incubators and cultivate 18 h, antibacterial circle diameter, averages more separately.
In Vitro Bacteriostasis with filter paper method research Gynura procumbens (Lour.) Merr. composition-chlorogenic acid variable concentrations (being to be respectively 80mg/mL, 40mg/mL, 20mg/mL by its concentration of acetone solution) to staphylococcus aureus, Salmonella, escherichia coli, yeast, aspergillus niger, observation inhibition zone size, inhibition zone shows that more greatly fungistatic effect is better.
Result and discussion
Gynura procumbens (Lour.) Merr. Content of Chlorogenic Acid bacteriostatic activity is as following table 4:
The bacteriostatic activity figure of table 4 Gynura procumbens (Lour.) Merr. Content of Chlorogenic Acid
By table 4, can show that chlorogenic acid has very strong inhibitory action to antibacterial, particularly to the inhibitory action of staphylococcus aureus its inhibition zone when concentration is 80mg/mL, can reach 24.9cm; Gram negative bacteria escherichia coli and Salmonella liquid are had to obvious inhibition.Mycete and saccharomycetic bacteriostasis are not obvious.
Experimental design 3: flavone antibacterial experiment in Gynura procumbens (Lour.) Merr.
Adopt and be extracted with ethyl acetate flavone in Gynura procumbens (Lour.) Merr., to 5 kinds, for examination bacterium, all show bacteriostatic activity in various degree, some bacterium is better than to Gynura procumbens (Lour.) Merr. Content of Chlorogenic Acid as the inhibition of saccharomyces cerevisiae, produce this result, may be to pour a libation class material owing to mainly existing the flavonoid that polarity is large in acetic acid ethyl ester layer more, in water layer, mainly contain the material that saccharide and chlorogenic acid polarity are very large and exist, there is antibacterial action.
The bacteriostatic activity figure of flavone in table 5 Gynura procumbens (Lour.) Merr.
By this, test us and can know that in Gynura procumbens (Lour.) Merr. and Gynura procumbens (Lour.) Merr., chlorogenic acid extracting has good antibacterial action.Gynura procumbens (Lour.) Merr. Content of Chlorogenic Acid has stronger inhibitory action to antibacterial.
The extracorporeal bacteria inhibitor test of Gynura procumbens (Lour.) Merr. extract shows: in invention Gynura procumbens (Lour.) Merr. this staphylococcus aureus and Resistant strain, dysentery bacterium, Bacillus typhi, Salmonella paratyphi, escherichia coli, pseudomonas aeruginosa etc. are all had to inhibitory action in various degree.
The present invention adopts pure plant extract and surfactant and the combination of other optimizing components, green, and health, natural, safe and non-stimulating, there is the effect of beauty and skin care bactericidal antiphlogistic, result of use is obvious, instant effect.The present invention is with low cost, convenient to use, and cost performance is high.The present invention is of many uses, not only can make facial film, can also be used as the general body cares such as hand, foot.
Claims (7)
1. a Gynura procumbens (Lour.) Merr. imitates natural compound recipe facial film of polynary maintenance and preparation method thereof, it is characterized in that: Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 93-96%, Camellia oil 0.5-1.5%, wild Hibisci Mutabilis Mel 2.3-5%, Herba Rosmarini Officinalis 0.3-1%.
2. a kind of Gynura procumbens (Lour.) Merr. according to claim 1 imitates natural compound recipe facial film of polynary maintenance and preparation method thereof, it is characterized in that: Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 94-95.5%, Camellia oil 0.8-1.5%, wild Hibisci Mutabilis Mel 3-4%, Herba Rosmarini Officinalis 0.4-0.7%.
3. a kind of Gynura procumbens (Lour.) Merr. according to claim 1 imitates natural compound recipe facial film of polynary maintenance and preparation method thereof, it is characterized in that: Gynura procumbens (Lour.) Merr. facial film is comprised of following percentage by weight raw material: Gynura procumbens (Lour.) Merr. extract 95%, Camellia oil 1%, wild Hibisci Mutabilis Mel 3.5%, Herba Rosmarini Officinalis 0.5%.
4. a kind of Gynura procumbens (Lour.) Merr. according to claim 1 imitates the preparation method of the natural compound recipe facial film of polynary maintenance, it is characterized in that: comprise the following steps:
(1) prepare raw material and weigh: choosing fresh, clean Gynura procumbens (Lour.) Merr. base of leaf and whole strain plant, put into washing machine and containing 0.8-1.2mg/L Ozone Water, carry out cleaning and sterilizing with every liter; Prepare Camellia oil, wild Hibisci Mutabilis Mel and Herba Rosmarini Officinalis raw material for standby;
(2) extract Gynura procumbens (Lour.) Merr. extract: the Gynura procumbens (Lour.) Merr. in step (1) is ground into after constant temperature 40-55 ℃ of dry 15-25min to 16-20 order granule sieving for standby;
(3) in step (2) container, add ethanol, the Gynura procumbens (Lour.) Merr. granule of concentration 70% again, with the feed liquid ratio of 1:15-30, with ultrasonic instrument, extract 24-40min, power 200w, extracts 2 times continuously, filters, and obtains Gynura procumbens (Lour.) Merr. extract;
(4) in the Gynura procumbens (Lour.) Merr. extract of step (3), add Camellia oil, wild Hibisci Mutabilis Mel, Herba Rosmarini Officinalis, with high-speed emulsifying homogeneous machine uniform stirring 25-40min;
(5) sterilization, sterilizing room fill, the shady and cool place of room temperature lucifuge preserves.
5. a kind of Gynura procumbens (Lour.) Merr. according to claim 4 imitates the preparation method of the natural compound recipe facial film of polynary maintenance, it is characterized in that: after dry in step (2), Gynura procumbens (Lour.) Merr. water content remains on initial weight 50%-70%.
6. a kind of Gynura procumbens (Lour.) Merr. according to claim 4 imitates the preparation method of the natural compound recipe facial film of polynary maintenance, it is characterized in that: in step (3), solid-liquid ratio is 1:20.
7. a kind of Gynura procumbens (Lour.) Merr. according to claim 4 imitates the preparation method of the natural compound recipe facial film of polynary maintenance, it is characterized in that: step (3) extraction time is 40min.
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