CN103947817A - Method for preparing semen cannabis protein powder from degreased semen cannabis residue - Google Patents
Method for preparing semen cannabis protein powder from degreased semen cannabis residue Download PDFInfo
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- CN103947817A CN103947817A CN201410174134.5A CN201410174134A CN103947817A CN 103947817 A CN103947817 A CN 103947817A CN 201410174134 A CN201410174134 A CN 201410174134A CN 103947817 A CN103947817 A CN 103947817A
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Abstract
The invention discloses a method for preparing semen cannabis protein powder from degreased semen cannabis residue, relating to the technical field of development and application of semen cannabis. The method comprises the steps of with degreased semen cannabis residue as a raw material, carrying out hot water protein extraction, filtrating, concentrating filtrate, and drying under the assistance of a drying aid to obtain the semen cannabis protein powder. According to the method, hot water is used as an extractant to improve the extraction efficiency of semen cannabis protein; as impurities such as an organic solvent and a acid-base reagent are not added, the extracted semen cannabis protein is not required to be purified, and the remaining semen cannabis residue is not polluted and can be used for preparing byproducts such as feeds or fertilizers, and therefore, the comprehensive utilization value of the semen cannabis is improved.
Description
Technical field
The present invention relates to development technique and the applied technical field thereof of fire fiber crops, specifically a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue.
Background technology
Fructus cannabis is commonly called as fiery pockmarks, hempseed, Ma Ren, is one of medicinal material medical in China and healthy food material.< < Chinese pharmacopoeia > > version in 2010 is recorded: fructus cannabis is moraceae plants hemp
cannabis sativa L.dry mature fruit.Health ministry is defended method prison and is sent out [2002] No. 51 file < < Ministry of Public Health about the notice > > of further standard healthy food material management, fructus cannabis is listed in to " the article list that is food and medicine ".Research shows, fiery fiber crops contain rich in protein, mainly contain edestin and numb benevolence albumin, is to hold digestible complete protein, can strengthen body fatigue resistance and immunologic function, is wherein rich in necessary each seed amino acid of human body.This seminar early-stage Study result shows, the different places of production, Guangxi fructus cannabis matter content is between 20.73%～24.29%, and average content 22.38%, can consider it as a kind of plant protein resource, to develop.
The existing market ramie product of getting angry mainly contains fiery numb kernel, fiery sesame oil, fiery numb soup, and kind is comparatively single, and mostly is rough-wrought product.Therefore, the comprehensive development and utilization to fructus cannabis profound level, high value, has great importance.First fructus cannabis is carried out to cold pressing degreasing and can obtain fructus cannabis oil, the residue after extraction is purifying protein further, and its comprehensive utilization benefit and prospect are by considerable.
Fructus cannabis has multiple extracting method, as sodium chloride solution extraction method, organic solvent extractionprocess, caustic extraction method, enzyme process etc.Chinese patent 201310068420.9(application number) a kind of FRUCTUS CANNABIS extraction process is disclosed, this process using sodium chloride solution extracts FRUCTUS CANNABIS, the fructus cannabis grouts that deoil through squeezing are dissolved in the sodium chloride solution of 20 times of amounts, sodium chloride concentration is 4%-6%, be heated to after 55-65 ℃, stir 60 minutes, in the environment of insulation, carry out liquid-solid separating treatment, by isolated extract, be cooled to 0-4 ℃, and albumen mud is obtained in sedimentation in the temperature of 0-4 ℃, utilize pure water to desalt, after absolute ethyl alcohol anhydrates, the albumen mud anhydrating desalting is dried, obtain highly purified FRUCTUS CANNABIS.Chinese patent 200410022197.5(application number) a kind of fructus cannabis powder and its preparation method and application is disclosed, this patent adopts organic solvent extractionprocess to extract fructus cannabis, the numb seed of fire is process screening and removing impurities, selected classification, through Fast Heating, cooling fast, the green stone roller shelling of machinery, the separated grease of normal temperature machinery cold press, make shelling cold press fiber crops benevolence albumose sheet, albumose sheet is dropped in extractor, adopt the grease in propane or butane extraction embryo sheet and isolate protein, after 4-6 extract and separate, obtain the numb benevolence protein wet dregs after separated grease, through decompression gasification, vacuumize precipitation and pressure recovery solvent, obtain the degreasing fiber crops benevolence albumen dregs of rice, through further powder process with after screening out impurity, be required fructus cannabis powder.Chinese literature " the heavy legal system of the molten acid of alkali is for fructus cannabis technical study " (> > brewages in < < China) discloses a kind of method that alkali lye extracts fructus cannabis, the method be take fructus cannabis as raw material, it is carried out after ungrease treatment, utilize the heavy legal system of the molten acid of alkali for fructus cannabis protein isolate and determine its optimum process condition, test shows, extract 50 ℃ of temperature, alkali is carried time 0.5h, pH1.0, solid-liquid ratio 1:20, the heavy pH5.0 of acid is optimum process condition, the recovery rate of protein is 29.54% with this understanding.Chinese literature " fructus cannabis aqueous enzymatic method Study on Preparation " (> > brewages in < < China) discloses a kind of technique with Enzymatic Extraction fructus cannabis, and this technological process is that fructus cannabis → cleaning and screening → pulverizing → extraction carry that oil → oven dry → degreasing fructus cannabis powder → enzymolysis → enzyme → filtration, washing → protein liquid go out.
In the numb protein extracting method of several fire, sodium chloride extracts extract in FRUCTUS CANNABIS method need to cool to 0-4 ℃, consumes energy more above, and purification process also needs to desalt to anhydrate, and operates more loaded down with trivial details; Organic solvent extractionprocess need to add organic solvent, and the later stage is difficult to remove, and affects protein quality; Alkali liquor extraction method requires stricter to technological parameter, need more experimental facilities; The enzyme preparation price comparison that Enzymatic Extraction is used is expensive, and production cost is high.This several method all can only extract the fructus cannabis of part, also remains a part of protein and other nutritional labelings in fructus cannabis residue, but owing to having introduced the impurity such as acid, alkali, salt in leaching process, the residue extracting after albumen is unsuitable for other purposes.
The numb albumen of fire is dissolved in pure water, water extracts fiery numb albumen can avoid introducing impurity, the fire fiber crops albumen and the remaining fructus cannabis residue that extract do not need to purify, be beneficial to further processing, but under normal temperature, the solubility of fiery numb albumen in water is less, extraction efficiency is very low, does not reach industrial requirement.Therefore, the technique of the numb albumen of Aqua pure extract fire need to be improved, and increases the solubility of fiery numb albumen in water, improves the extraction efficiency of fiery numb albumen.
Summary of the invention
In order to solve the deficiency of existing fructus cannabis extractive technique, the invention provides a kind of method of producing fiery numb albumen from degreasing fructus cannabis residue, the numb albumen of fire solubility in hot water is larger, use the numb albumen of hot water extracting fire, improve fiery numb protein extraction efficiency, do not introduce the impurity such as organic solvent, acid-base reagent simultaneously, the fire fiber crops albumen extracting does not need purifying, remaining fructus cannabis residue is not contaminated, can be for byproducts such as Fodder making or fertilizer, the comprehensive utilization value that has improved fructus cannabis, the method comprises the steps:
(1) protein extraction: add hot water in degreasing fructus cannabis residue, soak, filter, get filtrate, collect filter residue;
(2) filtrate is concentrated: filtrate is concentrated, obtain concentrate;
(3) confection preparation: add drying aid in concentrate, become admixing medical solutions;
(4) albumen powder process: admixing medical solutions is dried, and powder process, obtains fructus cannabis powder;
Described hot water is the hot water of 50-90 ℃; Described hot water is the hot water of 4-8 times of degreasing fructus cannabis residue weight.
As further restriction of the present invention, in step (1), described immersion is for soaking 1-3 hour.
As further restriction of the present invention, in step (1), described protein extraction repeats 1-3 time, and filtrate is merged.Protein extraction process repeats 1-3 the complete stripping of albumen guaranteeing in fructus cannabis residue, improves protein extracting ratio.
As further restriction of the present invention, in step (2), described simmer down to 55-65 ℃ reduced pressure concentration.
As further restriction of the present invention, in step (2), when described concentrate is 55-65 ℃, relative density reaches the concentrate of 1.10-1.15.
As further restriction of the present invention, in step (3), described drying aid is one or more in dextrin, maltodextrin, lactose, Icing Sugar.
As further restriction of the present invention, described drying aid is the drying aid of the weight of 0.6-0.8 part concentrate soluble solid.In order to make the present invention openly more abundant, in step (3), the computational methods of the weight of concentrate soluble solid are: accurate weighing concentrate gross weight, take a small amount of concentrate, put in the clean evaporating dish that is dried to constant weight, water bath method, move into oven drying, take out, put and in drier, be cooled to constant weight, the soluble solid of a small amount of concentrate in accurate weighing evaporating dish, the weight of all soluble solids in concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight.
As further restriction of the present invention, in step (4), described be dried into drying under reduced pressure or spraying dry.
As further restriction of the present invention, described drying under reduced pressure is temperature 55-65 ℃, the drying under reduced pressure of vacuum-0.08MPa～-0.1Mpa.
As further restriction of the present invention, described spraying is dried as keeping fluid temperature 55-65 ℃, EAT 170-190 ℃, and feed liquor speed 450-550ml/min, sprays dry.
Compared with prior art, the present invention has the following advantages:
(1) fiery numb albumen solubility in hot water is larger than solubility in normal-temperature water, uses the numb albumen of hot water extracting fire, the 10-12% when 1.5-2% of fiery numb protein extracting ratio during from normal temperature brings up to hot water.
(2) with the numb albumen of hot water extracting fire, do not introduce the impurity such as organic solvent, acid-base reagent, the fire fiber crops albumen of extraction does not need purifying, has simplified technological process.
(3) extract remaining fructus cannabis residue after fiery numb albumen and do not pollute, can, for byproducts such as Fodder making or fertilizer, improve the comprehensive utilization value of fructus cannabis.
(4) concentrate adds drying aid to be dried powder process, has improved albumen powder rate of drying, has reduced energy consumption.
(5) concentrate maintains lower temperature at drying under reduced pressure or spraying in dry, can keep fructus cannabis sex change not to occur in dry run, and two kinds of drying means efficiency is high, improved the processing speed of product.
(6) albumen powder moderate heat fiber crops protein content reaches 75-80%, is of high nutritive value, and market prospects are good.
(7) the method hot water and drying aid used is cheap, and instrument and equipment is simple, and production cost is lower.
Accompanying drawing explanation
Fig. 1 is process chart of the present invention.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described.
embodiment 1
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 50 ℃ of hot water that add 4 times of weight in extractor as extractant, after stirring at 50 ℃ extracting at constant temperature 1 hour, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 1 time, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.10(55 ℃ for 55 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 12.81g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.5933 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=3.84g.
(5) in step (3) gained concentrate, add maltodextrin as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.6:1, and 2.30g, stirs.
(6) step (5) gained confection is placed in to baking oven, 55 ℃ ,-0.08MPa drying under reduced pressure is made powder, obtains fructus cannabis powder 3.56g.
Fructus cannabis recovery rate is 9.7%, and in albumen powder, protein content is 75.4%.
embodiment 2
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 70 ℃ of hot water that add 6 times of weight in extractor as extractant, after stirring at 70 ℃ extracting at constant temperature 2 hours, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 2 times, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.10(60 ℃ for 60 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 13.67g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6850 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.68g.
(5) in step (3) gained concentrate, add dextrin as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.7:1, and 3.28g, stirs.
(6) step (5) gained confection is kept to 60 ℃ of fluid temperature, spray dry, EAT is 170 ℃, and feed liquor speed 450ml/min obtains fructus cannabis powder 4.20g.
Fructus cannabis recovery rate is 11.8%, and in albumen powder, protein content is 77.8%.
embodiment 3
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 90 ℃ of hot water that add 8 times of weight in extractor as extractant, after stirring at 90 ℃ extracting at constant temperature 3 hours, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 1 time, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.12(65 ℃ for 65 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 13.16g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6641 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.37g.
(5) in step (3) gained concentrate, add lactose as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.8:1, and 3.50g, stirs.
(6) step (5) gained confection is placed in to baking oven, 65 ℃ ,-0.09MPa drying under reduced pressure is made powder, obtains fructus cannabis powder 4.05g.
Fructus cannabis recovery rate is 11.2%, and in albumen powder, protein content is 76.5%.
embodiment 4
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 70 ℃ of hot water that add 4 times of weight in extractor as extractant, after stirring at 70 ℃ extracting at constant temperature 3 hours, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 3 times, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.12(65 ℃ for 65 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 14.47g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6073 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.39g.
(5) in step (3) gained concentrate, add Icing Sugar as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.7:1, and 3.07g, stirs.
(6) step (5) gained confection is kept to 65 ℃ of fluid temperature, spray dry, EAT is 180 ℃, and feed liquor speed 500ml/min obtains fructus cannabis powder 4.30g.
Fructus cannabis recovery rate is 12.3%, and in albumen powder, protein content is 79.2%.
embodiment 5
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 90 ℃ of hot water that add 6 times of weight in extractor as extractant, after stirring at 90 ℃ extracting at constant temperature 1 hour, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 1 time, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.13(55 ℃ for 55 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 14.74g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6103 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.50g.
(5) in step (3) gained concentrate, add dextrin, lactose as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.6:1, and dextrin, lactose respectively add 1.35g, stir.
(6) step (5) gained confection is kept to 55 ℃ of fluid temperature, spray dry, EAT is 190 ℃, and feed liquor speed 550ml/min obtains fructus cannabis powder 3.87g.
Fructus cannabis recovery rate is 10.8%, and in albumen powder, protein content is 77.2%.
embodiment 6
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 50 ℃ of hot water that add 8 times of weight in extractor as extractant, after stirring at 50 ℃ extracting at constant temperature 2 hours, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 2 times, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.13(60 ℃ for 60 ℃ of the filtrate in step (3) concentration tank) concentrate, accurate weighing concentrate gross weight is 13.45g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6341 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.26g.
(5) in step (3) gained concentrate, add maltodextrin, lactose, Icing Sugar as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.8:1, and maltodextrin, lactose, Icing Sugar respectively add 1.14g, stir.
(6) step (5) gained confection is kept to 60 ℃ of fluid temperature, spray dry, EAT is 180 ℃, and feed liquor speed 500ml/min obtains fructus cannabis powder 3.85g.
Fructus cannabis recovery rate is 10.6%, and in albumen powder, protein content is 76.3%.
embodiment 7
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 90 ℃ of hot water that add 4 times of weight in extractor as extractant, after stirring at 90 ℃ extracting at constant temperature 2 hours, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 3 times, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.14(55 ℃ for 55 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 13.66g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6434 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.39g.
(5) in step (3) gained concentrate, add dextrin, maltodextrin, lactose, Icing Sugar as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.8:1, and dextrin, maltodextrin, lactose, Icing Sugar respectively add 0.88g, stir.
(6) step (5) gained confection is placed in to baking oven, 55 ℃ ,-0.1MPa drying under reduced pressure.Obtain fructus cannabis powder 4.00g.
Fructus cannabis recovery rate is 10.9%, and in albumen powder, protein content is 75.4%.
embodiment 8
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 50 ℃ of hot water that add 6 times of weight in extractor as extractant, after stirring at 50 ℃ extracting at constant temperature 3 hours, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 2 times, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.15(65 ℃ for 65 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 14.12g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6845 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.83g.
(5) in step (3) gained concentrate, add lactose, Icing Sugar as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.7:1, and lactose, Icing Sugar respectively add 1.69g, stir.
(6) step (5) gained confection is placed in to baking oven, 65 ℃ ,-0.08MPa drying under reduced pressure.Obtain fructus cannabis powder 4.07g.
Fructus cannabis recovery rate is 11.3%, and in albumen powder, protein content is 76.9%.
embodiment 9
(1) take fructus cannabis residue 50g, leaching process: residue feeds intake in extractor, toward 70 ℃ of hot water that add 8 times of weight in extractor as extractant, after stirring at 70 ℃ extracting at constant temperature 1 hour, filter, get filtrate and be placed in concentration tank, collect residue.
(2) repeat above-mentioned steps (1) leaching process 1 time, merging filtrate is in concentration tank.
(3) by the measured value when being evaporated to relative density 1.15(60 ℃ for 60 ℃ of the filtrate in step (2) concentration tank) concentrate, accurate weighing concentrate gross weight is 13.85g.
(4) accurate weighing concentrate 2g, put in the clean evaporating dish that is dried to constant weight, water bath method, 105 ℃ of oven dryings 3 hours, take out, in accurate weighing evaporating dish, the soluble solid of a small amount of concentrate is 0.6286 g to constant weight to put in drier cooling 30 minutes, the amount of all soluble solids in step (3) gained concentrate=(soluble solid of a small amount of concentrate/a small amount of concentrate weight) * concentrate gross weight=4.35g.
(5) in step (3) gained concentrate, add maltodextrin, Icing Sugar as drying aid, drying aid and fructus cannabis soluble solid weight ratio are 0.6:1, and maltodextrin, Icing Sugar respectively add 1.36g, stir.
(6) step (5) gained confection is kept to 60 ℃ of fluid temperature, spray dry, EAT is 190 ℃, and feed liquor speed 550ml/min obtains fructus cannabis powder 3.94g.
Fructus cannabis recovery rate is 11.1%, and in albumen powder, protein content is 78.3%.
Claims (10)
1. from degreasing fructus cannabis residue, produce a method for fiery numb albumen powder, it is characterized in that: the method comprises the steps:
(1) protein extraction: add hot water in degreasing fructus cannabis residue, soak, filter, get filtrate;
(2) filtrate is concentrated: filtrate is concentrated, obtain concentrate;
(3) admixing medical solutions preparation: add the drying aid proportional with concentrate soluble solid weight in concentrate, obtain admixing medical solutions;
(4) albumen powder process: admixing medical solutions is dried, and powder process, obtains fructus cannabis powder;
Described hot water is 50-90 ℃ of hot water; Described hot water is the hot water of 4-8 times of degreasing fructus cannabis residue weight.
2. in a kind of degreasing fructus cannabis residue according to claim 1, extract the method for fiery numb albumen powder, it is characterized in that: in step (1), described immersion is for soaking 1-3 hour.
3. a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue according to claim 1 and 2, is characterized in that: in step (1), described protein extraction repeats 1-3 time, and filtrate is merged.
4. a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue according to claim 1, is characterized in that: in step (2), described filtrate simmer down to is reduced pressure concentration at 55-65 ℃ by filtrate.
5. according to a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue described in claim 1 or 4, it is characterized in that: in step (2), when described concentrate is 55-65 ℃, relative density reaches the concentrate of 1.10-1.15.
6. a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue according to claim 1, is characterized in that: in step (3), described drying aid is one or more in dextrin, maltodextrin, lactose, Icing Sugar.
7. according to a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue described in claim 1 or 6, it is characterized in that: described drying aid is the drying aid of the weight of 0.6-0.8 part concentrate soluble solid.
8. a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue according to claim 1, is characterized in that: in step (4), described be dried into drying under reduced pressure or spraying dry.
9. a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue according to claim 8, is characterized in that: described drying under reduced pressure is temperature 55-65 ℃ the drying under reduced pressure of vacuum-0.08MPa～-0.1Mpa.
10. a kind of method of producing fiery numb albumen powder from degreasing fructus cannabis residue according to claim 8, it is characterized in that: described spraying is dried as keeping fluid temperature 55-65 ℃, EAT 170-190 ℃, the spraying of feed liquor speed 450-550ml/min is dry.
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| CN104472641A (en) * | 2014-12-31 | 2015-04-01 | 广西壮族自治区农业科学院农产品加工研究所 | Fructus cannabis protein biscuit and preparation method thereof |
| CN105061554A (en) * | 2015-08-12 | 2015-11-18 | 晋城市汉恩宝生物科技有限公司 | CBD (cannabidiol)-rich fructus cannabis concentrate protein powder and preparation method thereof |
| CN106011207A (en) * | 2016-06-29 | 2016-10-12 | 大连深蓝肽科技研发有限公司 | Method for extracting fructus cannabis oligopeptide from fructus cannabis cake |
| CN105994930A (en) * | 2016-05-16 | 2016-10-12 | 黄山普和康生物科技有限公司 | Process for processing high-purity fructus cannabis protein power |
| CN108013206A (en) * | 2016-10-28 | 2018-05-11 | 汉义生物科技（北京）有限公司 | A kind of numb chewing gum of fire |
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