CN103938448A - Production method of antibacterial polysulfonamide fabric - Google Patents
Production method of antibacterial polysulfonamide fabric Download PDFInfo
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- CN103938448A CN103938448A CN201410161646.8A CN201410161646A CN103938448A CN 103938448 A CN103938448 A CN 103938448A CN 201410161646 A CN201410161646 A CN 201410161646A CN 103938448 A CN103938448 A CN 103938448A
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Abstract
The invention relates to the textile field, and in particular relates to a production method of an antibacterial polysulfonamide fabric. The production method comprises the steps of preparing materials, implementing billet yarns, warping, slashing, weaving, washing, dehydrating, and post-finishing. The antibacterial polysulfonamide fabric has a good antibacterial effect, and Shengma fibers are added in the billet yarns to improve the antibacterial property of the fabric; the antibacterial finishing procedure is added in the post-finishing step, the antibacterial effect of the polysulfonamide fabric can be effectively improved and the market competitiveness of the fabric is improved.
Description
Technical field
The present invention relates to the production method of fabric, especially a kind of production method of antimicrobial form virtue sulfone synthetic fibre fabric.
Background technology
Along with scientific and technical progress, the raising of the level of the productive forces, people are also more and more higher for the requirement of wearing fabric.Virtue sulfone synthetic fibre (PPSU terephthalamide fiber) belongs to aromatic polyamide class exotic material, is called for short: its outstanding heat-resisting ability of PSA. can make it in 300 DEG C of hot-airs, heat 100h, and strength loss is less than 5%, and limited oxygen index exceedes 33; Also have good dyeability, electric insulation, resistance to chemical corrosion, radioresistance etc.
Due to the outstanding performance of fragrant sulfone synthetic fibre fabric, it is widely used in: make fire-entry suit, special working suit, high-temperature-resistant filtering material, F.H class B insulation paper, for special dimensions such as safeguard protection, environmental protection, chemical industry, aerospace; But, because its career field is special, just there is new challenge for the anti-microbial property of fabric, if fabric anti-microbial property is bad, very easily the personnel's of wearing health is damaged, the fabric that cannot ensure health performance is to have long-range development prospect.
Therefore, working out a kind of fragrant sulfone synthetic fibre fabric that can be effectively antibacterial is one of current fragrant sulfone synthetic fibre fabric industry major issue that need to solve.
Summary of the invention
Goal of the invention: the object of the invention is in order to solve the deficiencies in the prior art, a kind of production method of fragrant sulfone synthetic fibre fabric that can be effectively antibacterial is provided.
Technical scheme: in order to realize above object, the production method of a kind of antimicrobial form virtue of the present invention sulfone synthetic fibre fabric, comprises step:
(a) prepare material: select percentage by weight to be respectively 90% 15tex polysulphonamide fiber, 9% 10tex Sheng-bast fiber, 1% conductive fiber;
(b) base yarn: successively to above-mentioned fiber carry out blowing, comb and parallel cotton fibers prior to spinning, mixed also, rove, spun yarn processing, form base yarn;
(c) warping: the base yarn in step (b) is put into warping machines warping, and described warping Bigpian yarn is even, and the speed of a motor vehicle is 280-285r/min;
(d) sizing: the slurry of warping base yarn later being put into Sizing machines floods, described slurry comprises following percentage by weight material: modified starch slurry 5-8g/L, solid propenoic acid resin 6-10g/L, wax disk(-sc) 1-2g/L, antistatic additive 1-2g/L, anti-UV auxiliary agent 2-3g/L, smooth agent SPT-90 3-4g/L, slurry temperature 80-85 DEG C, the Sizing machines speed of a motor vehicle is 40-50r/min, the rate of sizing is 9-10%, and regain is 5-6.5%;
(e) weave cotton cloth: base yarn is manufactured to grey cloth through sword loom;
(f) washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, water lotion in liquid stream cylinder is containing degreaser 1-3g/L, chelated dispersants 3-5g/L, softener 3-4g/L, first grey cloth is cleaned to 20-30min in the water lotion of 85 DEG C, clean 10-15min with the water lotion of 50 DEG C again, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 30-40 DEG C again cleans 10-15min;
(g) dehydration;
(h) after, arrange: the grey cloth of drying after dehydration is carried out to antibiotic finish, shaping process, complete arrangement; Wherein sizing need to be immersed grey cloth in sizing solution, and described sizing solution comprises following components by weight percent:
100 parts of epoxy resin
Smooth agent 3-5 part
Catalyst 1-5 part
Softener 25-35 part;
(i) inspection;
(j) packaging.
In order to improve the antibacterial effect of fragrant sulfone synthetic fibre fabric, extend its antibacterial time, antibiotic finish described in step (h) is for adopting nano-silver antibacterial finishing agent to carry out antibiotic finish to grey cloth, for normally used Nano Silver particle diameter in fabric nano-silver antibacterial finishing agent is 2-5nm, colorless and odorless transparency liquid is main antibacterial raw material, the efficient fabric antibacterial finishing agent forming through NEW TYPE OF COMPOSITE mode, is widely used in each kind fabrics such as various textiless, nonwoven fabric, leather.Antibacterial effect is more than 99%.
Antibiotic finishing method comprises the following steps:
1. pad: grey cloth is immersed in antiseptic solution, and described antiseptic solution comprises: nano-silver antibacterial finishing agent 3-5g/L, stabilizing agent 2-3g/L, urea 1-2g/L, solution temperature is 80-90 DEG C, and dip time is 20-40min, and pick-up is 100%;
2. dry: the grey cloth after padding is sent into drying machine drying, and bake out temperature is 80-90 DEG C, and the time is 2-3min;
3. cure: the grey cloth after drying is cured to processing, and stoving temperature is 140-145 DEG C, and the time of curing is 5-10min.
Smooth agent described in step (h) is any in KGS-9068, organic silicone oil, paraffin, the present invention, by adopting above-mentioned smooth agent, can effectively improve the smoothness of fragrant sulfone synthetic fibre fabric, improves fabric feel quality, enhance one's market competitiveness, expand the scope of application of fabric.
Catalyst nano TiO described in step (h)
2, nanometer SiO
2in any.
Use citric acid and maleic anhydride mixing dressing liquid at nanocatalyst SiO
2or TiO
2effect under fragrant sulfone synthetic fibre fabric is carried out to wrinkle proofing, after arranging, the creasy recovery angle of fabric obviously improves, and ultimate strength declines little.
In order to improve the soft effect to antimicrobial form virtue sulfone synthetic fibre fabric, the softener described in step (h) is one or more compositions in ammoniacal liquor modified organic silicon, hydrophilic solubility organosilicon, low molecular polyethylene emulsion.
In order to improve the anti-flammability of antimicrobial form virtue sulfone synthetic fibre fabric, after described step (e), increase flame-proof treatment operation, the technique of described flame-proof treatment comprises the following steps:
Pad: grey cloth is immersed in flame retardant solution, and described solution comprises fire retardant 2-5g/L, buffer 1-2g/L, stabilizing agent 3-6g/L, catalyst 2-3g/L, softener 5-8g/L, sticking agent 4-5g/L;
Dry: above-mentioned grey cloth is put into dryer, and bake out temperature is 80-90 DEG C;
Bake: the grey cloth after drying is cured to processing, and stoving temperature is 160-170 DEG C;
Washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, water lotion in liquid stream cylinder is containing degreaser 1-3g/L, and chelated dispersants 3-5g/L first cleans 20-30min by grey cloth in the water lotion of 85 DEG C, clean 10-15min with the water lotion of 50 DEG C again, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 30-40 DEG C again cleans 10-15min.
Beneficial effect: the production method of antibiotic aromatic spun silk cotton face fabric provided by the invention compared with prior art, has the following advantages:
1. good anti-bacterial effect: the present invention by adding Sheng-bast fiber in base yarn, improve the antimicrobial form of fabric, because the present invention is merely able to increase antibiotic finish operation at postfinishing process, can effectively improve the antibacterial effect of fragrant sulfone synthetic fibre fabric again, improve the market competitiveness of fabric;
2. comfortable feel: the present invention increases softener in rinsing machine finishing process, effectively makes the deliquescing of fabric texture, improves the comfortableness of fabric, expands the scope of application of fabric;
3. good flame resistance: the present invention, by adding polysulphonamide fiber at base yarn, can effectively ensure the heat resistance of fabric, owing to can carrying out flame-proof treatment after step weaving cotton cloth, further improves the anti-flammability of fragrant sulfone synthetic fibre fabric again, improves the security of fabric;
4. antistatic effect is strong: the present invention adds conductive fiber in base yarn, effectively prevents that fabric from producing static in the time wearing, and ensures the comfortableness of fabric dress;
5. technique of the present invention is simple, and simple operation can be promoted the use of.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail; but illustrate that protection scope of the present invention is not limited to the concrete scope of the present embodiment simultaneously; based on the embodiment in the present invention; those of ordinary skill in the art, not making the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1:
A production method for antimicrobial form virtue sulfone synthetic fibre fabric, comprises step:
(a) prepare material: select percentage by weight to be respectively 90% 15tex polysulphonamide fiber, 9% 10tex Sheng-bast fiber, 1% conductive fiber;
(b) base yarn: successively to above-mentioned fiber carry out blowing, comb and parallel cotton fibers prior to spinning, mixed also, rove, spun yarn processing, form base yarn;
(c) warping: the base yarn in step (b) is put into warping machines warping, and described warping Bigpian yarn is even, and the speed of a motor vehicle is 280r/min;
(d) sizing: the slurry of warping base yarn later being put into Sizing machines floods, described slurry comprises following percentage by weight material: modified starch slurry 5g/L, solid propenoic acid resin 6-g/L, wax disk(-sc) 1g/L, antistatic additive 1g/L, anti-UV auxiliary agent 2g/L, smooth agent SPT-90 3g/L, 80 DEG C of slurry temperatures, the Sizing machines speed of a motor vehicle is 40r/min, the rate of sizing is 9%, and regain is 5%;
(e) weave cotton cloth: base yarn is manufactured to grey cloth through sword loom;
(f) washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, the water lotion in liquid stream cylinder is containing degreaser 1g/L, chelated dispersants 3g/L, softener 3g/L, first grey cloth is cleaned to 20min in the water lotion of 85 DEG C, then clean 10min with the water lotion of 50 DEG C, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 30 DEG C again cleans 10min;
(g) dehydration;
(h) after, arrange: the grey cloth of drying after dehydration is carried out to antibiotic finish, shaping process, complete arrangement; Wherein antibiotic finishing method comprises the following steps:
1. pad: grey cloth is immersed in antiseptic solution, and described antiseptic solution comprises: nano-silver antibacterial finishing agent 3.5g/L, stabilizing agent 2.3g/L, urea 1.2g/L, solution temperature is 80 DEG C, and dip time is 22min, and pick-up is 100%;
2. dry: the grey cloth after padding is sent into drying machine drying, and bake out temperature is 80 DEG C, and the time is 2.5min;
3. cure: the grey cloth after drying is cured to processing, and stoving temperature is 140 DEG C, and the time of curing is 5min.
Described sizing need to be immersed grey cloth in sizing solution, and described sizing solution comprises following components by weight percent:
100 parts of epoxy resin
3.5 parts of smooth agent KGS-9068
Citric acid, maleic anhydride, nanocatalyst SiO
2mix 2.5 parts of dressing liquids
28 parts of ammoniacal liquor modified organic silicons;
(i) inspection;
(j) packaging.
Embodiment 2
A production method for antimicrobial form virtue sulfone synthetic fibre fabric, comprises step:
(a) prepare material: select percentage by weight to be respectively 90% 15tex polysulphonamide fiber, 9% 10tex Sheng-bast fiber, 1% conductive fiber;
(b) base yarn: successively to above-mentioned fiber carry out blowing, comb and parallel cotton fibers prior to spinning, mixed also, rove, spun yarn processing, form base yarn;
(c) warping: the base yarn in step (b) is put into warping machines warping, and described warping Bigpian yarn is even, and the speed of a motor vehicle is 283r/min;
(d) sizing: the slurry of warping base yarn later being put into Sizing machines floods, described slurry comprises following percentage by weight material: modified starch slurry 6g/L, solid propenoic acid resin 8g/L, wax disk(-sc) 1.5g/L, antistatic additive 1.3g/L, anti-UV auxiliary agent 2.4g/L, smooth agent SPT-90 3.5g/L, 82 DEG C of slurry temperatures, the Sizing machines speed of a motor vehicle is 45r/min, the rate of sizing is 10%, and regain is 6.5%;
(e) weave cotton cloth: base yarn is manufactured to grey cloth through sword loom;
(f) flame-proof treatment: comprise the following steps,
1. pad: grey cloth is immersed in flame retardant solution, and described solution comprises fire retardant 3g/L, buffer 1.8g/L, stabilizing agent 5.2g/L, catalyst 2.5g/L, softener 6g/L, sticking agent 4.3g/L;
2. dry: above-mentioned grey cloth is put into dryer, and bake out temperature is 85 DEG C;
3. bake: the grey cloth after drying is cured to processing, and stoving temperature is 160 DEG C;
(g) washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, water lotion in liquid stream cylinder is containing degreaser 2.3g/L, chelated dispersants 3.5g/L, softener 3.2g/L, first grey cloth is cleaned to 25min in the water lotion of 85 DEG C, clean 13min with the water lotion of 50 DEG C again, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 35 DEG C again cleans 12min;
(h) dehydration;
(i) arrange afterwards: the grey cloth of drying after dehydration is carried out to antibiotic finish, shaping process, complete arrangement; Wherein antibiotic finish comprises the following steps:
1. pad: grey cloth is immersed in antiseptic solution, and described antiseptic solution comprises: nano-silver antibacterial finishing agent 3.6g/L, stabilizing agent 2.5g/L, urea 1.4g/L, solution temperature is 85 DEG C, and dip time is 29min, and pick-up is 100%;
2. dry: the grey cloth after padding is sent into drying machine drying, and bake out temperature is 80 DEG C, and the time is 2.5min;
3. cure: the grey cloth after drying is cured to processing, and stoving temperature is 142 DEG C, and the time of curing is 7min;
Described sizing need to be immersed grey cloth in sizing solution, and described sizing solution comprises following components by weight percent:
100 parts of epoxy resin
4 parts of organic silicone oils
Nanocatalyst TiO
23 parts
30 parts of hydrophilic solubility organosilicons;
(j) inspection;
(k) packaging.
Embodiment 3
A production method for antimicrobial form virtue sulfone synthetic fibre fabric, comprises step:
(a) prepare material: select percentage by weight to be respectively 90% 15tex polysulphonamide fiber, 9% 10tex Sheng-bast fiber, 1% conductive fiber;
(b) base yarn: successively to above-mentioned fiber carry out blowing, comb and parallel cotton fibers prior to spinning, mixed also, rove, spun yarn processing, form base yarn;
(c) warping: the base yarn in step (b) is put into warping machines warping, and described warping Bigpian yarn is even, and the speed of a motor vehicle is 285r/min;
(d) sizing: the slurry of warping base yarn later being put into Sizing machines floods, described slurry comprises following percentage by weight material: modified starch slurry 8g/L, solid propenoic acid resin 10g/L, wax disk(-sc) 2g/L, antistatic additive 2g/L, anti-UV auxiliary agent 3g/L, smooth agent SPT-90 4g/L, 85 DEG C of slurry temperatures, the Sizing machines speed of a motor vehicle is 50r/min, the rate of sizing is 10%, and regain is 6.5%;
(e) weave cotton cloth: base yarn is manufactured to grey cloth through sword loom;
(f) flame-proof treatment: comprise step
1. pad: grey cloth is immersed in flame retardant solution, and described solution comprises fire retardant 5g/L, buffer 1.9/L, stabilizing agent 6g/L, catalyst 3g/L, softener 8g/L, sticking agent 5g/L;
2. dry: above-mentioned grey cloth is put into dryer, and bake out temperature is 90 DEG C;
3. bake: the grey cloth after drying is cured to processing, and stoving temperature is 170 DEG C;
(g) washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, the water lotion in liquid stream cylinder is containing degreaser 3g/L, chelated dispersants 5g/L, softener 3.8g/L, first grey cloth is cleaned to 30min in the water lotion of 85 DEG C, then clean 15min with the water lotion of 50 DEG C, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 40 DEG C again cleans 15min;
(h) dehydration;
(i) arrange afterwards: the grey cloth of drying after dehydration is carried out to antibiotic finish, shaping process, complete arrangement; Wherein antibiotic finish comprises step:
1. pad: grey cloth is immersed in antiseptic solution, and described antiseptic solution comprises: nano-silver antibacterial finishing agent 5g/L, stabilizing agent 2.8g/L, urea 2g/L, solution temperature is 90 DEG C, and dip time is 40min, and pick-up is 100%;
2. dry: the grey cloth after padding is sent into drying machine drying, and bake out temperature is 90 DEG C, and the time is 3min;
3. cure: the grey cloth after drying is cured to processing, and stoving temperature is 145 DEG C, and the time of curing is 10min.
Described sizing need to be immersed grey cloth in sizing solution, and described sizing solution comprises following components by weight percent:
100 parts of epoxy resin
5 parts, paraffin
Citric acid, maleic anhydride, nanocatalyst TiO
2mix 2.5 parts 5 parts of dressing liquids
35 parts of low molecular polyethylene emulsions;
(j) inspection;
(k) packaging.
Above-described embodiment is only explanation technical conceive of the present invention and feature, its objective is to allow to be familiar with these those skilled in the art and can to understand content of the present invention enforcement according to this, can not limit the scope of the invention with this.All equivalents that Spirit Essence has been done according to the present invention or modification, within all should being encompassed in protection scope of the present invention.
Claims (6)
1. a production method for antimicrobial form virtue sulfone synthetic fibre fabric, is characterized in that: comprise step
(a) prepare material: select percentage by weight to be respectively 90% 15tex polysulphonamide fiber, 9% 10tex Sheng-bast fiber, 1% conductive fiber;
(b) base yarn: successively to above-mentioned fiber carry out blowing, comb and parallel cotton fibers prior to spinning, mixed also, rove, spun yarn processing, form base yarn;
(c) warping: the base yarn in step (b) is put into warping machines warping, and described warping Bigpian yarn is even, and the speed of a motor vehicle is 280-285r/min;
(d) sizing: the slurry of warping base yarn later being put into Sizing machines floods, described slurry comprises following percentage by weight material: modified starch slurry 5-8g/L, solid propenoic acid resin 6-10g/L, wax disk(-sc) 1-2g/L, antistatic additive 1-2g/L, anti-UV auxiliary agent 2-3g/L, smooth agent SPT-90 3-4g/L, slurry temperature 80-85 DEG C, the Sizing machines speed of a motor vehicle is 40-50r/min, the rate of sizing is 9-10%, and regain is 5-6.5%;
(e) weave cotton cloth: base yarn is manufactured to grey cloth through sword loom;
(f) washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, water lotion in liquid stream cylinder is containing degreaser 1-3g/L, chelated dispersants 3-5g/L, softener 3-4g/L, first grey cloth is cleaned to 20-30min in the water lotion of 85 DEG C, clean 10-15min with the water lotion of 50 DEG C again, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 30-40 DEG C again cleans 10-15min;
(g) dehydration;
(h) after, arrange: the grey cloth of drying after dehydration is carried out to antibiotic finish, shaping process, complete arrangement; Wherein sizing need to be immersed grey cloth in sizing solution, and described sizing solution comprises following components by weight percent:
100 parts of epoxy resin
Smooth agent 3-5 part
Catalyst 1-5 part
Softener 25-35 part;
(i) inspection;
(j) packaging.
2. the production method of antimicrobial form virtue sulfone synthetic fibre fabric according to claim 1, is characterized in that: the antibiotic finish described in step (h) is for adopting nano-silver antibacterial finishing agent to carry out antibiotic finish to grey cloth.
3. the production method of antimicrobial form virtue sulfone synthetic fibre fabric according to claim 1, is characterized in that: the smooth agent described in step (h) is any in KGS-9068, organic silicone oil, paraffin.
4. the production method of antimicrobial form virtue sulfone synthetic fibre fabric according to claim 1, is characterized in that: the softener described in step (h) is one or more compositions in ammoniacal liquor modified organic silicon, hydrophilic solubility organosilicon, low molecular polyethylene emulsion.
5. in order to improve the anti-flammability of antimicrobial form virtue sulfone synthetic fibre fabric, increase flame-proof treatment operation after described step (e), the technique of described flame-proof treatment comprises the following steps:
(a) pad: grey cloth is immersed in flame retardant solution, and described solution comprises fire retardant 2-5g/L, buffer 1-2g/L, stabilizing agent 3-6g/L, catalyst 2-3g/L, softener 5-8g/L, sticking agent 4-5g/L;
(b) dry: above-mentioned grey cloth is put into dryer, and bake out temperature is 80-90 DEG C;
(c) bake: the grey cloth after drying is cured to processing, and stoving temperature is 160-170 DEG C;
(d) washing: above-mentioned grey cloth is put into liquid stream cylinder and wash, water lotion in liquid stream cylinder is containing degreaser 1-3g/L, and chelated dispersants 3-5g/L first cleans 20-30min by grey cloth in the water lotion of 85 DEG C, clean 10-15min with the water lotion of 50 DEG C again, repeat twice of above-mentioned steps; The clear water of grey cloth being put into 30-40 DEG C again cleans 10-15min.
6. the production method of antimicrobial form virtue sulfone synthetic fibre fabric according to claim 1, is characterized in that: the catalyst described in step (h) is nano-TiO
2, nanometer SiO
2in any.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410161646.8A CN103938448A (en) | 2014-04-22 | 2014-04-22 | Production method of antibacterial polysulfonamide fabric |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410161646.8A CN103938448A (en) | 2014-04-22 | 2014-04-22 | Production method of antibacterial polysulfonamide fabric |
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Family
ID=51186306
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| CN105803786A (en) * | 2016-05-09 | 2016-07-27 | 江苏苏扬服帽有限公司 | Antistatic agent and method for processing textile by using same |
| CN106861292A (en) * | 2017-02-27 | 2017-06-20 | 辽宁鸿盛环境技术集团有限公司 | A kind of woven filtrate of organic fiber and preparation method |
| CN107254773A (en) * | 2017-06-27 | 2017-10-17 | 太仓市玛雅针织有限公司 | A kind of preparation method of anti-flammability fabric |
| CN111493473A (en) * | 2020-06-15 | 2020-08-07 | 杭州天龙手袋股份有限公司 | Waterproof antibacterial soft material handbag |
| CN111559127A (en) * | 2020-06-03 | 2020-08-21 | 席梦思床褥家具（苏州）有限公司 | Medium flame-retardant copper ion fiber composite fabric and manufacturing method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105803786A (en) * | 2016-05-09 | 2016-07-27 | 江苏苏扬服帽有限公司 | Antistatic agent and method for processing textile by using same |
| CN106861292A (en) * | 2017-02-27 | 2017-06-20 | 辽宁鸿盛环境技术集团有限公司 | A kind of woven filtrate of organic fiber and preparation method |
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| CN111559127A (en) * | 2020-06-03 | 2020-08-21 | 席梦思床褥家具（苏州）有限公司 | Medium flame-retardant copper ion fiber composite fabric and manufacturing method thereof |
| CN111493473A (en) * | 2020-06-15 | 2020-08-07 | 杭州天龙手袋股份有限公司 | Waterproof antibacterial soft material handbag |
| CN111493473B (en) * | 2020-06-15 | 2022-07-12 | 杭州天龙手袋股份有限公司 | Waterproof antibacterial soft material handbag |
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Application publication date: 20140723 |