CN103922949A - Calcium leucine chelate powder and processing method thereof - Google Patents
Calcium leucine chelate powder and processing method thereof Download PDFInfo
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- CN103922949A CN103922949A CN201410177518.2A CN201410177518A CN103922949A CN 103922949 A CN103922949 A CN 103922949A CN 201410177518 A CN201410177518 A CN 201410177518A CN 103922949 A CN103922949 A CN 103922949A
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Abstract
The invention discloses calcium leucine chelate powder and a processing method thereof. The calcium leucine chelate powder is prepared by chelating the following components in parts by weight: 0.4 part of calcium, 3-4 parts of leucine, 1-2 parts of xylitol and 0.3-0.4 part of vitamin C. The concrete method comprises the steps of firstly, preparing calcium; secondly, preparing the calcium leucine chelate powder. The calcium leucine chelate powder has the beneficial effects that a calcium supplementing preparation is prepared by chelating calcium prepared by taking egg shells as raw materials and leucine, so that a novel approach is provided for the comprehensive utilization of bird egg processing wastes, and the double effects of supplementing leucine and calcium can be achieved.
Description
Technical field
The present invention relates to a kind of chelating calcium powder and working method, particularly a kind of leucine chelating calcium powder and working method.
Background technology
Leucic effect comprises with Isoleucine cooperation together with α-amino-isovaleric acid repairs muscle, controls blood sugar, and provides energy to bodily tissue.It can also improve the output of tethelin, and helps burning interior fat, and these fat are due in body interior, only by going on a diet and exercise is difficult to them to produce useful effect.Leucine chelating calcium is as a kind of novel calsium supplement, has good biological and chemical stability, good effect of supplemented calcium and higher biological value, can reach the double effects that not only supplements leucine but also supplement calcium.
Summary of the invention
A kind of leucine chelating calcium powder and the working method that in order to reach the double effects of not only supplementary leucine but also supplementary calcium, provide are provided.
Leucine chelating calcium powder of the present invention is comprised of calcium, leucine, Xylitol and vitamins C, and wherein 0.4 part of calcium, leucine 3-4 part, Xylitol 1-2 part and vitamins C 0.3-0.4 part make through chelating by weight.
Leucine is that food grade purity is 99%.
The working method of leucine chelating calcium powder of the present invention, its concrete grammar is as described below:
The preparation of the first step, calcium: Ovum crusta Gallus domesticus removes shell membrane, after oven dry, pulverized 160 mesh sieves, and by weight 1 part of Ovum crusta Gallus domesticus powder was added in 100 parts of glacial acetic acid solutions, the mass concentration of glacial acetic acid solution is 37%, stir 30min, the calcium ion content of measuring in mixed solution is 30%-35%;
The preparation of second step, leucine chelating calcium powder: by weight 3-4 part leucine is added in the mixed solution that the first step makes, uniform stirring, huge legendary turtle is closed 1h, add by weight 20 parts of precipitations of dehydrated alcohol, then by 8000r/min, carry out centrifugal 30min, measure respectively calcium ion content and aforementioned centrifugal rear supernatant liquor Free Calcium ion content in the mixed solution making in the first step, record the huge legendary turtle rate of closing and will reach 80%-85%; Then add huge legendary turtle to close liquid 1-2 part Xylitol and 0.3-0.4 part vitamins C by weight and carry out mixing and stirring, dry and make leucine chelating calcium powder.
Beneficial effect of the present invention:
The calcium that the eggshell of take is prepared as raw material is prepared into calcium-supplementing preparation with leucine chelating again, for the comprehensive utilization of birds, beasts and eggs processing waste provides new way, can reach the double effects that not only supplements leucine but also supplement calcium.
Embodiment
Embodiment mono-:
Leucine chelating calcium powder of the present invention is comprised of calcium, leucine, Xylitol and vitamins C, and wherein 0.3 part of 0.4 part of calcium, 3 parts of leucines, 1 part of Xylitol and vitamins C make through chelating by weight.
Leucine is that food grade purity is 99%.
Its concrete working method is as described below:
The preparation of the first step, calcium: Ovum crusta Gallus domesticus removes shell membrane, after oven dry, pulverized 160 mesh sieves, and by weight 1 part of Ovum crusta Gallus domesticus powder was added in 100 parts of glacial acetic acid solutions, the mass concentration of glacial acetic acid solution is 37%, stir 30min, the calcium ion content of measuring in mixed solution is 32%;
The preparation of second step, leucine chelating calcium powder: by weight 3 parts of leucines are added in the mixed solution that the first step makes, uniform stirring, huge legendary turtle is closed 1h, add by weight 20 parts of precipitations of dehydrated alcohol, then by 8000r/min, carry out centrifugal 30min, measure respectively calcium ion content and aforementioned centrifugal rear supernatant liquor Free Calcium ion content in the mixed solution making in the first step, record the huge legendary turtle rate of closing and will reach 82%; Then add huge legendary turtle to close liquid 1 part of Xylitol and 0.3 part of vitamins C by weight and carry out mixing and stirring, dry and make leucine chelating calcium powder.
Embodiment bis-:
Leucine chelating calcium powder of the present invention is comprised of calcium, leucine, Xylitol and vitamins C, and wherein 0.4 part of 0.4 part of calcium, 4 parts of leucines, 2 parts of Xylitols and vitamins C make through chelating by weight.
Leucine is that food grade purity is 99%.
Its concrete working method is as described below:
The preparation of the first step, calcium: Ovum crusta Gallus domesticus removes shell membrane, after oven dry, pulverized 160 mesh sieves, and by weight 1 part of Ovum crusta Gallus domesticus powder was added in 100 parts of glacial acetic acid solutions, the mass concentration of glacial acetic acid solution is 37%, stir 30min, the calcium ion content of measuring in mixed solution is 32%;
The preparation of second step, leucine chelating calcium powder: by weight 4 parts of leucines are added in the mixed solution that the first step makes, uniform stirring, huge legendary turtle is closed 1h, add by weight 20 parts of precipitations of dehydrated alcohol, then by 8000r/min, carry out centrifugal 30min, measure respectively calcium ion content and aforementioned centrifugal rear supernatant liquor Free Calcium ion content in the mixed solution making in the first step, record the huge legendary turtle rate of closing and will reach 83%; Then add huge legendary turtle to close liquid 2 parts of Xylitols and 0.4 part of vitamins C by weight and carry out mixing and stirring, dry and make leucine chelating calcium powder.
Embodiment tri-:
Leucine chelating calcium powder of the present invention is comprised of calcium, leucine, Xylitol and vitamins C, and wherein 0.4 part of 0.4 part of calcium, 3.5 parts of leucines, 1.5 parts of Xylitols and vitamins C make through chelating by weight.
Leucine is that food grade purity is 99%.
Its concrete working method is as described below:
The preparation of the first step, calcium: Ovum crusta Gallus domesticus removes shell membrane, after oven dry, pulverized 160 mesh sieves, and by weight 1 part of Ovum crusta Gallus domesticus powder was added in 100 parts of glacial acetic acid solutions, the mass concentration of glacial acetic acid solution is 37%, stir 30min, the calcium ion content of measuring in mixed solution is 33%;
The preparation of second step, leucine chelating calcium powder: by weight 3.5 parts of leucines are added in the mixed solution that the first step makes, uniform stirring, huge legendary turtle is closed 1h, add by weight 20 parts of precipitations of dehydrated alcohol, then by 8000r/min, carry out centrifugal 30min, measure respectively calcium ion content and aforementioned centrifugal rear supernatant liquor Free Calcium ion content in the mixed solution making in the first step, record the huge legendary turtle rate of closing and will reach 85%; Then add huge legendary turtle to close liquid 1.5 parts of Xylitols and 0.4 part of vitamins C by weight and carry out mixing and stirring, dry and make leucine chelating calcium powder.
Claims (3)
1. a leucine chelating calcium powder, is characterized in that: calcium, leucine, Xylitol and vitamins C, consist of, wherein 0.4 part of calcium, leucine 3-4 part, Xylitol 1-2 part and vitamins C 0.3-0.4 part make through chelating by weight.
2. a kind of leucine chelating calcium powder according to claim 1, is characterized in that: described leucine is that food grade purity is 99%.
3. a working method for leucine chelating calcium powder, is characterized in that: concrete grammar is as described below:
The preparation of the first step, calcium: Ovum crusta Gallus domesticus removes shell membrane, after oven dry, pulverized 160 mesh sieves, and by weight 1 part of Ovum crusta Gallus domesticus powder was added in 100 parts of glacial acetic acid solutions, the mass concentration of glacial acetic acid solution is 37%, stir 30min, the calcium ion content of measuring in mixed solution is 30%-35%;
The preparation of second step, leucine chelating calcium powder: by weight 3-4 part leucine is added in the mixed solution that the first step makes, uniform stirring, huge legendary turtle is closed 1h, add by weight 20 parts of precipitations of dehydrated alcohol, then by 8000r/min, carry out centrifugal 30min, measure respectively calcium ion content and aforementioned centrifugal rear supernatant liquor Free Calcium ion content in the mixed solution making in the first step, record the huge legendary turtle rate of closing and will reach 80%-85%; Then add huge legendary turtle to close liquid 1-2 part Xylitol and 0.3-0.4 part vitamins C by weight and carry out mixing and stirring, dry and make leucine chelating calcium powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410177518.2A CN103922949A (en) | 2014-04-29 | 2014-04-29 | Calcium leucine chelate powder and processing method thereof |
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| CN201410177518.2A CN103922949A (en) | 2014-04-29 | 2014-04-29 | Calcium leucine chelate powder and processing method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5071874A (en) * | 1989-06-14 | 1991-12-10 | Lonza Ltd. | L-carnitine magnesium citrate |
| CN1187991A (en) * | 1998-02-23 | 1998-07-22 | 张经坤 | Calcium tablet |
| CN1931828A (en) * | 2006-09-29 | 2007-03-21 | 华侨大学 | Prepn process of amino acid-calcium chelate |
| CN101659625A (en) * | 2009-09-04 | 2010-03-03 | 黄继红 | Method for preparing amino acid chelated calcium by utilizing egg shells |
| CN102150776A (en) * | 2011-01-17 | 2011-08-17 | 吉林大学 | Eggshell calcium malate chewable tablets and preparation method thereof |
-
2014
- 2014-04-29 CN CN201410177518.2A patent/CN103922949A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5071874A (en) * | 1989-06-14 | 1991-12-10 | Lonza Ltd. | L-carnitine magnesium citrate |
| CN1187991A (en) * | 1998-02-23 | 1998-07-22 | 张经坤 | Calcium tablet |
| CN1931828A (en) * | 2006-09-29 | 2007-03-21 | 华侨大学 | Prepn process of amino acid-calcium chelate |
| CN101659625A (en) * | 2009-09-04 | 2010-03-03 | 黄继红 | Method for preparing amino acid chelated calcium by utilizing egg shells |
| CN102150776A (en) * | 2011-01-17 | 2011-08-17 | 吉林大学 | Eggshell calcium malate chewable tablets and preparation method thereof |
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Application publication date: 20140716 |