CN103893366B - A kind of Chinese medicinal granule and method of inspection thereof being used for the treatment of cerebral ischemia - Google Patents
A kind of Chinese medicinal granule and method of inspection thereof being used for the treatment of cerebral ischemia Download PDFInfo
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- CN103893366B CN103893366B CN201410123541.3A CN201410123541A CN103893366B CN 103893366 B CN103893366 B CN 103893366B CN 201410123541 A CN201410123541 A CN 201410123541A CN 103893366 B CN103893366 B CN 103893366B
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Abstract
The invention discloses a kind of Chinese medicinal granule being used for the treatment of cerebral ischemia, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 10 ~ 12 grams, Radix Angelicae Sinensis 10 ~ 12 grams, Radix Paeoniae Rubra 10 ~ 12 grams, 13 ~ 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 8 ~ 10 grams, Radix Cyathulae 10 ~ 12 grams, Gypsum Fibrosum 25 ~ 30 grams, Radix Scutellariae 10 ~ 12 grams, Spica Prunellae 8 ~ 10 grams, Bombyx Batryticatus 10 ~ 12 grams, 2 ~ 4 grams, Flos Carthami, Herba Erigerontis 0 ~ 5 gram, Herba Pentanematis Indici 0 ~ 5 gram.Adopt TLC Identification to test to above-mentioned Chinese medicinal granule, detection method is simple, and testing result is reliable, more contributes to clinical diagnosis and treatment.Clinical trial certificate, the present invention, by selecting suitable medical material and proportioning thereof, reaches the remarkable efficacy for the treatment of cerebral ischemia, and safe without toxic side effect.
Description
Technical field
The present invention relates to a kind of Chinese medicine, be specifically related to a kind of Chinese medicinal granule and the method for inspection thereof that are used for the treatment of cerebral ischemia.
Background technology
Cerebral ischemia is internal carotid artery or vertebra---the transience blood supply of basilar artery system is not enough, and shows a kind of disease of paralysis, aphasia in various degree.Because clinical signs is reversibility sudden onset, and interiorly 24 time can to recover completely, therefore also known as transient ischemic attack, also be called " transient apoplexy ".Primary disease is mainly in more than 50 years old patient, and M-F is 3.9: 1.Because of the early warning that primary disease is often complete apoplexy, so early prevention, diagnosis, treatment primary disease, in the work of control acute cerebrovascular disease, are very important links.The traditional Chinese medical science thinks that daily life is not normal, intemperance of taking food, overstrain internal injury, so that wind, gas, the stasis of blood, the stagnant brain network of stagnation of phlegm because feelings will hindered more than primary disease generation; Or liver-wind is held under the arm on expectorant and disturbed, heart spleen caused by liver and kidney deficiency makes brain network lose to support.Primary disease belongs to the category such as the traditional Chinese medical science " apoplexy ", " dizzy ".Treatment for cerebral ischemia still lacks the effective medicine of generally recognized as safe at present.
Summary of the invention
The present invention aims to provide a kind of Chinese medicinal granule and the method for inspection thereof that are used for the treatment of cerebral ischemia, by selecting suitable medical material and proportioning thereof, reaches the remarkable efficacy contributing to patients with cerebral ischemic rehabilitation, and safe without toxic side effect.
In order to achieve the above object, the present invention is by the following technical solutions: a kind of Chinese medicinal granule being used for the treatment of cerebral ischemia, is prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 10 ~ 12 grams, Radix Angelicae Sinensis 10 ~ 12 grams, Radix Paeoniae Rubra 10 ~ 12 grams, 13 ~ 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 8 ~ 10 grams, Radix Cyathulae 10 ~ 12 grams, Gypsum Fibrosum 25 ~ 30 grams, Radix Scutellariae 10 ~ 12 grams, Spica Prunellae 8 ~ 10 grams, Bombyx Batryticatus 10 ~ 12 grams, 2 ~ 4 grams, Flos Carthami, Herba Erigerontis 0 ~ 5 gram, Herba Pentanematis Indici 0 ~ 5 gram.
As preferably, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami.
As preferably, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams.
As preferably, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Pentanematis Indici 5 grams.
As preferably, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams, Herba Pentanematis Indici 5 grams.
A kind of preparation method being used for the treatment of the Chinese medicinal granule of cerebral ischemia, comprise the steps: 1 successively) get this product powder 0.5g, solubilizer 25 ~ 35ml, reflux 25 ~ 35 minutes, filter, collect filtrate solvent evaporated, the residue 20ml that adds water dissolves, and extracts 2 times adding 15 ~ 25ml ethyl acetate at every turn, merge extractive liquid, evaporate to dryness ethyl acetate, residue adds methanol 1ml and dissolves, as need testing solution; 2) separately get control medicinal material 5g, add water 45 ~ 55ml, boils 30 minutes, and filter, filtrate water bath method, residue solubilizer 25 ~ 35ml, is made in the same way of control medicinal material solution; 3) according to thin layer chromatography test, draw each 5 μ l of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, with toluene-ethyl acetate-formic acid for developing solvent, launch, take out, dry, spray, with 10% ethanol solution of sulfuric acid, is heated to spot development at 105 DEG C clear, inspects under putting ultra-violet lamp; 4) in test sample chromatograph, on the position corresponding to control medicinal material chromatograph, blueness, the green fluorescence speckle of aobvious same color.
The pharmacology analysis of each Chinese medicinal ingredients of the present invention is as follows:
Radix Gentianae Macrophyllae [source] is gentianaceae plant gentiana macrophylla, the root of thick stem Radix Gentianae or Tibet Radix Gentianae.[nature and flavor] are pungent, bitter, flat.[return through] returns stomach, liver, gallbladder meridian.[function cures mainly] wind-damp dispelling, clearing away damp-heat, stopping numbness pain.For rheumatic arthralgia, the contracture of muscle arteries and veins, joint is ached, afternoon fever, and infantile malnutrition generates heat.
The dry root of Radix Angelicae Sinensis [source] umbelliferae angelica.[nature and flavor] sweet, acrid, warm.[return through] returns liver, the heart, spleen channel.[function cures mainly] is enriched blood and is invigorated blood circulation, menstruction regulating and pain relieving, loosening bowel to relieve constipation.For blood deficiency and yellow complexion, dizzy cardiopalmus, menoxenia, amenorrhea dysmenorrhea, asthenia cold abdominalgia, dryness of the intestine constipation, rheumatic arthralgia, injury from falling down, ulcer sores.Radix Angelicae Sinensis (processed with wine) promoting blood circulation to restore menstrual flow.For amenorrhea dysmenorrhea, rheumatic arthralgia, injury from falling down.
The dry root of Radix Paeoniae Rubra [source] ranunculaceae plant Radix Paeoniae or river Radix Paeoniae Rubra.[nature and flavor] are bitter, are slightly cold.[return through] returns Liver Channel.[function cures mainly] clearing away heat and cooling blood, eliminating stasis to stop pain.For maculae caused by violent heat pathogen, hematemesis and epistaxis, conjunctival congestion and swelling pain, hypochondriac pain due to stagnation of liverQI, amenorrhea dysmenorrhea, lump in the abdomen is suffered from abdominal pain, injury from falling down, carbuncle skin infection.
Fresh or the dried root of the Radix Rehmanniae [source] scrophulariaceae rehmannia glutinosa plant.[nature and flavor] Radix Rehmanniae: sweet, cold.[return through] GUIXIN, liver, kidney channel.[function cures mainly] clearing away heat and cooling blood, yin nourishing, promotes the production of body fluid.For calentura crimson tongue excessive thirst, yin asthenia generating intrinsic heat, hectic fever due to YIN-deficiency consumptive fever, interior-heat is quenched one's thirst, and spits blood, and epistaxis sends out speckle dermexanthesis.
The dry root of the Radix Angelicae Dahuricae [source] the umbellate form section plant Radix Angelicae Dahuricae.[nature and flavor] are pungent, temperature.[return through] returns stomach, large intestine, lung meridian.[function cures mainly] loose wind dehumidifying, understand things pain-stopping, detumescence and apocenosis.
The dry root of Radix Cyathulae [source] amaranthaceous plant Radix Cyathulae.[nature and flavor] sweet, micro-hardship, flat.[return through] returns liver, kidney channel.[function cures mainly] eliminating blood stasis and inducing menstruation, easing joint movement, inducing diuresis for treating stranguria syndrome.
Gypsum Fibrosum [source] Sulfates mineral anhydrite race Gypsum Fibrosum, main containing hydrous calcium sulfate (CaSO42H2O), after excavating, removing silt and assorted stone.[nature and flavor] are sweet, pungent, Great Cold.[return through] attaches to the lung and stomach meridians.[function cures mainly] clearing away heat-fire, relieving restlessness is quenched the thirst.For fever caused by exogenous pathogenic factors, high hot excessive thirst, dyspnea and cough due to lung-heat, the high Sheng of stomach-fire, headache, toothache.
The dry root of Radix Scutellariae [source] labiate Radix Scutellariae.[function cures mainly] heat clearing and damp drying, eliminating fire and detoxication, hemostasis, antiabortive.For hygropyrexia, fever disease in summer vomiting and nausea uncomfortable in chest, damp and hot feeling of fullness, dysentery, jaundice, cough due to lung-heat, high hot excessive thirst, heat in blood tells nosebleed, carbuncle sore tumefacting virus, frequent fetal movement.
Spica Prunellae [source] this product is the dry fruit ear of labiate Spica Prunellae.[nature and flavor] are pungent, bitter, cold.[return through] returns liver, gallbladder meridian.[function cures mainly] relieves inflammation or internal heat, improving eyesight, eliminating stagnation, detumescence.For conjunctival congestion and swelling pain, order pearl nyctalgia, has a headache dizzy, scrofula, goiter, and acute mastitis swells and ache; Thyromegaly, tuberculous lymphadenitis, cyclomastopathy, hypertension.
Larva that Bombyx Batryticatus [source] is Bombycidae insecticide bombyx mori infects muscardine and ossified dry Scorpio.[nature and flavor] are pungent salty, flat.[return through] enters liver, lung, stomach warp.[function cures mainly] expelling wind to relieve convulsion, dissipating phlegm and resolving masses.Control apoplectic aphasia, infantile convulsion, wind syndrome of head, acute throat trouble.Sore throat, scrofula tuberculosis.Wind skin ulcer urticaria, erysipelas, mastitis.
The dried floral of Flos Carthami [source] feverfew Flos Carthami.[nature and flavor] are pungent, temperature.[return through] GUIXIN, Liver Channel.[function cures mainly] promoting blood circulation to restore menstrual flow, eliminating stasis to stop pain.
Herba Erigerontis [source] Compositae Herba Erigerontis aceris platymiscium Erigeron breviscapus (Vant.) Hand.-Mazz., is used as medicine with herb or root.[nature and flavor] pungent, micro-hardship, temperature.[function cures mainly] expelling cold and relieving exterior syndrome, expelling wind and removing dampness, activating collaterals to relieve pain.For headache due to common cold, toothache, stomachache, rheumatalgia, the paralysis that cerebrovas-cularaccident causes, osteomyelitis.
Herba Pentanematis Indici [source] is for feverfew is from the herb of back of the body reed millet straw.Summer, autumn adopt, and clean, dry or using fresh herb.[function cures mainly] heat-clearing and toxic substances removing, relieving stranguria by diuresis.Control infantile malnutrition.
Below in conjunction with clinical laboratory data, beneficial effect of the present invention is described:
Accept patients with cerebral ischemic 144 example for medical treatment through clinical, take the oral agents made according to embodiment 1, every day two doses, use 3-20 days continuously.Therapeutic evaluation: cure: transference cure; Effective: symptom alleviates, but do not disappear completely; Invalid: symptom does not disappear, without obviously changing.
Therapeutic outcome: cure and effective totally 128 examples, effective percentage, up to 88.8%, is followed up a case by regular visits to after June again, all without recurrence.
Detailed description of the invention
In order to understand better and implement the present invention, further illustrate the present invention below in conjunction with specific embodiment.
Embodiment 1
Take: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams, Herba Pentanematis Indici 5 grams, insert in container, add 8 times of water gagings, decoct 1.5 hours, filter; Filtering residue adds 6 times of water gagings, decocts 1 hour, filters; Merging filtrate, concentrated, dry, dry, then add appropriate dextrin and correctives, granulate according to this area common process.
The method of inspection: comprise the steps: 1 successively) get this product powder 0.5g, solubilizer 25 ~ 35ml, reflux 25 ~ 35 minutes, filter, collect filtrate solvent evaporated, residue add water 20ml dissolve, extract 2 times, merge extractive liquid, evaporate to dryness ethyl acetate adding 15 ~ 25ml ethyl acetate at every turn, residue adds methanol 1ml and dissolves, as need testing solution; 2) separately get control medicinal material 5g, add water 45 ~ 55ml, boils 30 minutes, and filter, filtrate water bath method, residue solubilizer 25 ~ 35ml, is made in the same way of control medicinal material solution; 3) according to thin layer chromatography test, draw each 5 μ l of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, with toluene-ethyl acetate-formic acid for developing solvent, launch, take out, dry, spray, with 10% ethanol solution of sulfuric acid, is heated to spot development at 105 DEG C clear, inspects under putting ultra-violet lamp; 4) in test sample chromatograph, on the position corresponding to control medicinal material chromatograph, blueness, the green fluorescence speckle of aobvious same color.
Be used for the treatment of cerebral ischemia.Oral, every day two doses.
Embodiment 2
Take: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams, Herba Pentanematis Indici 5 grams, insert in container, add 8 times of water gagings, decoct 1.5 hours, filter; Filtering residue adds 6 times of water gagings, decocts 1 hour, filters; Merging filtrate, concentrated, dry, dry, then add appropriate dextrin and correctives, granulate according to this area common process.
Be used for the treatment of cerebral ischemia.Oral, every day two doses.
The method of inspection is with embodiment 1.
Embodiment 3
Take: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams, Herba Pentanematis Indici 5 grams, insert in container, add 8 times of water gagings, decoct 1.5 hours, filter; Filtering residue adds 6 times of water gagings, decocts 1 hour, filters; Merging filtrate, concentrated, dry, dry, then add appropriate dextrin and correctives, granulate according to this area common process.
Be used for the treatment of cerebral ischemia.Oral, every day two doses.
The method of inspection is with embodiment 1.
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here cannot give exhaustive to all embodiments.Every belong to technical scheme of the present invention the apparent change of extending out or variation be still in the row of protection scope of the present invention.
Claims (5)
1. one kind is used for the treatment of the Chinese medicinal granule of cerebral ischemia, it is characterized in that, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 10 ~ 12 grams, Radix Angelicae Sinensis 10 ~ 12 grams, Radix Paeoniae Rubra 10 ~ 12 grams, 13 ~ 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 8 ~ 10 grams, Radix Cyathulae 10 ~ 12 grams, Gypsum Fibrosum 25 ~ 30 grams, Radix Scutellariae 10 ~ 12 grams, Spica Prunellae 8 ~ 10 grams, Bombyx Batryticatus 10 ~ 12 grams, 2 ~ 4 grams, Flos Carthami, Herba Erigerontis 0 ~ 5 gram, Herba Pentanematis Indici 0 ~ 5 gram.
2. a kind of Chinese medicinal granule being used for the treatment of cerebral ischemia according to claim 1, it is characterized in that, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami.
3. a kind of Chinese medicinal granule being used for the treatment of cerebral ischemia according to claim 1, it is characterized in that, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams.
4. a kind of Chinese medicinal granule being used for the treatment of cerebral ischemia according to claim 1, it is characterized in that, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Pentanematis Indici 5 grams.
5. a kind of Chinese medicinal granule being used for the treatment of cerebral ischemia according to claim 1, it is characterized in that, be prepared from by the medical material of following weight proportion: Radix Gentianae Macrophyllae 12 grams, Radix Angelicae Sinensis 12 grams, Radix Paeoniae Rubra 12 grams, 15 grams, the Radix Rehmanniae, the Radix Angelicae Dahuricae 10 grams, Radix Cyathulae 12 grams, Gypsum Fibrosum 30 grams, Radix Scutellariae 12 grams, Spica Prunellae 10 grams, Bombyx Batryticatus 12 grams, 2 grams, Flos Carthami, Herba Erigerontis 5 grams, Herba Pentanematis Indici 5 grams.
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