CN103860871A - Traditional Chinese medicinal composition for treating upper respiratory infections and preparation method thereof - Google Patents
Traditional Chinese medicinal composition for treating upper respiratory infections and preparation method thereof Download PDFInfo
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- CN103860871A CN103860871A CN201410098611.4A CN201410098611A CN103860871A CN 103860871 A CN103860871 A CN 103860871A CN 201410098611 A CN201410098611 A CN 201410098611A CN 103860871 A CN103860871 A CN 103860871A
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Abstract
The invention discloses a traditional Chinese medicinal composition for treating upper respiratory infections and a preparation method thereof. The composition consists of the following medicinal materials: 10-30g of rehmannia, 10-30g of radix scrophulariae, 5-20g of radix ophiopogonis, 5-20g of colla corii asini, 20-40g of rheum officinale, 5-20g of polygonum multiflorum, 20-60g of root of Chinese trichosanthes, 20-60g of gypsum, 10-30g of seaweed, 5-20g of rhizoma corydalis, 5-20g of loquat leaf and 5-20g of fructus cannabis. The preparation method comprises the following steps: grinding and sieving the medicinal materials except for colla corii asini, decocting twice and mixing filtrates; centrifuging and taking supernatant liquid; adding the colla corii asini and condensing; filling an extracting solution; and cooling to normal temperature and preserving. The medicinal composition disclosed by the invention can diminish inflammation and relieve cough; meanwhile, the medicinal composition, due to addition of other traditional Chinese medicines, can enhance body resistance and bring about benefit for dispelling diseases; the medicinal composition can effectively treat upper respiratory infections; the medicinal composition is cheap in cost, hardly causes toxic and side effect, and has obvious curative effect on such upper respiratory infections as chronic pharyngitis, amygdalitis and trachitis.
Description
Technical field
The present invention relates to a kind of Chinese medicine composition for the treatment of upper respiratory tract infection and preparation method thereof, belong to Chinese medicine technical field.
Background technology
Upper respiratory tract infection is one of mankind's commonly encountered diseases, is mainly in winter in spring, of all ages, the sex of falling ill, occupation, area, immunologic hypofunction person susceptible.70% ?80% caused by virus, 20% ?30% caused by antibacterial.Symptom mainly contains heating, nasal obstruction, cough, headache, pharyngalgia, myalgia, tired etc.Belonged to " flu ", " hypopyretic laryngalgia " category in Chinese medicine, the primary disease cause of disease is conceived to dirty deficient of lung, kidney two more.Think lung, deficiency of the kidney yin, Xiang Huowu system, hyperactivity of deficient fire, stifling throat, throat loses in moistening and supports and falls ill.Imbalance of YIN and YANG is the basis that causes sore throat to occur.Hyperactivity of deficient fire and causing a disease, the record of the method treatment sore throat of useful YIN nourishing yin nourishing tonify deficiency pathogenic fire reducing, in long-term clinical practice, finds that Chinese medicine has unique advantage preventing and treating aspect upper respiratory tract infection, but much only only limits to relieving cough and diminishing inflammation lung qi dispersing.
Summary of the invention
The object of the invention is to provide a kind of Chinese medicine composition for the treatment of upper respiratory tract infection and preparation method thereof, have and extract the feature complete, preparation method is quick, assay is simple and efficient, evident in efficacy, with low cost, toxic and side effects is little, to overcome the deficiencies in the prior art.
The Chinese medicine composition for the treatment of upper respiratory tract infection of the present invention is made up of following a few taste medical materials: Radix Rehmanniae 10g ?30g; Radix Scrophulariae 10g ?30g; Radix Ophiopogonis 5g ?20g; Colla Corii Asini 5g ?20g; Radix Et Rhizoma Rhei 20g ?40g; Radix Polygoni Multiflori 5g ?20g; Radix Trichosanthis 20g ?60g; Gypsum Fibrosum 20g ?60g; Sargassum 10g ?30g; Rhizoma Corydalis 5g ?20g; Folium Eriobotryae 5g ?20g; Fructus Cannabis 5g ?20g.
Analyze: upper respiratory tract infection belongs to syndrome of flaring up of deficient fire asthenia of pulmonosplenic qi card, expectorant heat syndrome, expectorant stasis of blood mutual resistance card according to traditional Chinese medical science traditional theory.12 taste Chinese medicine effects are as follows:
Radix Rehmanniae: clearing away heat and cooling blood, YIN nourishing and the production of body fluid promoting.Enter nutrient blood for heat, maculae caused by violent heat pathogen, hematemesis and epistaxis, consumption of YIN caused by febrile disease, crimson tongue excessive thirst, constipation is hindered in Tianjin, fever due to yin deficiency, hectic fever due to YIN-deficiency consumptive disease heat, interior-heat is quenched one's thirst.
Radix Scrophulariae: clearing away heat and cooling blood, nourishing YIN to lower pathogenic fire, detoxicating and resolving stagnation of pathogens, enters nutrient blood for heat, maculae caused by violent heat pathogen, consumption of YIN caused by febrile disease, crimson tongue excessive thirst, constipation is hindered in Tianjin, hectic fever due to YIN-deficiency chronic cough, conjunctival congestion, pharyngalgia, diphtheria.
Radix Ophiopogonis: YIN nourishing and the production of body fluid promoting: lung moistening clears away heart-fire.For dryness of the lung dry cough, deficiency of YIN chronic cough, sore throat pharyngalgia, Tianjin wound is thirsty, and interior-heat is quenched one's thirst, vexed insomnia, dryness of the intestine constipation.
Colla Corii Asini: the YIN nourishing of enriching blood, moisturize, stop blooding.For blood deficiency and yellow complexion, dizzy cardiopalmus, flesh withers unable, dysphoria and insomnia, stirring-up of pathogenic wind in the interior resulting from deficiency, xeropulmonary cough, the consumptive disease hemoptysis of coughing.
Radix Et Rhizoma Rhei: heat and toxic materials clearing away, clearing away heat-fire, removing pathogenic heat from blood and toxic substance from the body, eliminating blood stasis and inducing menstruation, dampness removing jaundice eliminating.For the stagnant constipation of excess-heat, heat in blood is told nosebleed, conjunctival congestion pharyngeal swelling.
Radix Polygoni Multiflori: removing toxic substances, eliminating carbuncle, preventing the attack (or recurrence) of malaria.
Radix Trichosanthis: clearing away heat-fire, promoting the production of body fluid to quench thirst, detumescence and apocenosis.For calentura excessive thirst, lung-heat type cough, interior-heat is quenched one's thirst.
Gypsum Fibrosum: clearing away heat-fire, relieving restlessness is quenched the thirst, for fever caused by exogenous pathogenic factors, high hot excessive thirst, dyspnea and cough due to lung-heat.
Sargassum: bitter in the mouth, salty, cold.Return liver, stomach, kidney channel.Eliminating phlegm and softening indurated mass eliminating stagnation, inducing diuresis to remove edema.For goiter, phlegm retention edema.
Rhizoma Corydalis: acrid in the mouth, hardship, temperature.Return liver, spleen channel.Invigorate blood circulation, circulation of qi promoting, pain relieving.For the breast side of body, epigastric pain, obstruction of qi in the chest and cardialgia, treating swelling and pain by traumatic injury.
Folium Eriobotryae: bitter in the mouth, is slightly cold.Attach to the lung and stomach meridians.Clearing away lung-heat to relieve cough, stopping nausea and vomiting by lowering the adverse flow of QI.For cough due to lung-heat, QI rising in reverse order dyspnea with rapid respiration, gastric heat vomiting, dysphoria with smothery sensation is thirsty.
Fructus Cannabis: sweet in the mouth is flat.Return spleen, stomach, large intestine channel.Loosening bowel to relieve constipation.For blood deficiency and depleted fluid, dryness of the intestine constipation.
Treat a preparation method for the medicine of upper respiratory tract infection, it is characterized in that comprising the following steps:
1, by the ten above-mentioned Herba indigoferae Pseudotinctoriae except Colla Corii Asini, pulverize, cross 65 mesh sieves, accurately take in pot for boiling chinese traditional medicine, add 2 times of amount pure water, decoct 2 hours with being steam heated to boil, leach medicinal liquid;
2, in filtering residue, add 1 times of amount purified water, being heated to boil decocts 1 hour, leaches medicinal liquid;
3, merge twice filtrate, add centrifuge centrifugal, rotating speed is 1000r/min, takes out supernatant, and Colla Corii Asini is added in supernatant, and it is fully dissolved, and heating is concentrated into 1000ml; Conventional semi-finished product inspection is carried out in sampling; (remarks: if defective, cancel);
4, vial and bottle stopper are cleaned, controlled and do with pure water, the extracting solution quantitative filling of after the assay was approved, in vial, is tamping to bottle stopper;
5, the medicinal liquid of embedding is put into sterilizing cabinet, flowing steam sterilization 30 minutes;
6, the medicinal liquid after sterilizing being cooled to room temperature preserves.
Except conventional semi-finished product inspection, this method also can adopt the method for following semi-finished product inspection:
Semi-finished product content measuring standard: every 1ml contains Radix Et Rhizoma Rhei with emodin (C
15h
10o
5) and chrysophanol (C
15h
10o
4) total, must not be less than 15 μ g;
1, chromatographic condition and system suitability octadecylsilane chemically bonded silica are filler; Jia Chun ?0.1% phosphoric acid solution (64 ?90: 36 ?10) be mobile phase; Detect wavelength be 250 ?258nm; Number of theoretical plate calculates and should be not less than 1500 by emodin peak;
2, the preparation of reference substance solution respectively precision take emodin, chrysophanol reference substance each 5 ?10mg, put in 50ml measuring bottle, add methanol constant volume, shake up; Precision measures emodin reference substance solution, the each 1ml of chrysophanol reference substance, puts in 25ml measuring bottle, adds methanol constant volume, shakes up, and to obtain final product;
3, the preparation precision of need testing solution measures this product 10ml, puts in flask, add 30% Yi Chun ?hydrochloric acid (10: 1) 15ml, put in water-bath heating hydrolysis 1 hour, cooling immediately, extract 4 times with the powerful jolting of chloroform, each 15ml, combined chloroform liquid, puts evaporate to dryness in water-bath, residue with Wu Shui Yi Chun ?ethyl acetate (2: 1) dissolve, in dislocation 25ml measuring bottle, and be diluted to scale, shake up, with microporous filter membrane filtration, get subsequent filtrate, to obtain final product;
4, algoscopy accurate reference substance solution and the each 10 μ l of need testing solution of drawing respectively, injection liquid chromatography, measures, and whether qualifiedly obtains sample; If underproof words product can not use.
Invention advantage
In the present invention, comprise the 12 taste medical materials such as Radix Rehmanniae, Radix Scrophulariae, Radix Ophiopogonis, Colla Corii Asini, Radix Et Rhizoma Rhei, Radix Polygoni Multiflori, Radix Trichosanthis, Gypsum Fibrosum, Sargassum, Rhizoma Corydalis, Folium Eriobotryae, Fructus Cannabis, Radix Rehmanniae, Radix Scrophulariae, Radix Et Rhizoma Rhei, Radix Trichosanthis, Gypsum Fibrosum etc. have effect of clearing away heat and cooling blood pathogenic fire purging, Colla Corii Asini nourishing blood YIN nourishing, Radix Ophiopogonis YIN nourishing and the production of body fluid promoting, Rhizoma Corydalis blood-activating and qi-promoting, Radix Polygoni Multiflori energy removing toxicity for eliminating carbuncles, Sargassum eliminating phlegm and softening indurated mass eliminating stagnation, inducing diuresis to remove edema, Folium Eriobotryae clearing away lung-heat to relieve cough, stopping nausea and vomiting by lowering the adverse flow of QI, Fructus Cannabis loosening bowel to relieve constipation.Chinese medicine composition of the present invention has increased other a few herbs in inflammation-diminishing and cough-controlling, strengthens resistance of human body, is more conducive to dispelling of disease, and according to theory of Chinese medical science prescription, ingredients is prepared from according to certain weight proportion and priority addition sequence.Can effectively treat upper respiratory tract infection, with low cost, toxic and side effects is little, evident in efficacy for upper respiratory tract infection such as chronic pharyngitis, tonsillitis, bronchitis.
The specific embodiment
The Chinese medicine composition for the treatment of upper respiratory tract infection of the present invention comprises following a few taste medical material: Radix Rehmanniae 10g ?30g; Radix Scrophulariae 10g ?30g; Radix Ophiopogonis 5g ?20g; Colla Corii Asini 5g ?20g; Radix Et Rhizoma Rhei 20g ?40g; Radix Polygoni Multiflori 5g ?20g; Radix Trichosanthis 20g ?60g; Gypsum Fibrosum 20g ?60g; Sargassum 10g ?30g; Rhizoma Corydalis 5g ?20g; Folium Eriobotryae 5g ?20g; Fructus Cannabis 5g ?20g.
Prioritization scheme of the present invention:
1, prescription: Radix Rehmanniae 20g Radix Scrophulariae 20g 10g Radix Ophiopogonis Colla Corii Asini 10g Radix Et Rhizoma Rhei 30g Radix Polygoni Multiflori 10g Radix Trichosanthis 40g Gypsum Fibrosum 40g Sargassum 20g Rhizoma Corydalis 10g Folium Eriobotryae 10g Fructus Cannabis 10g
2, chromatographic condition and system suitability octadecylsilane chemically bonded silica are filler; Jia Chun ?0.1% phosphoric acid solution (85: 15) be mobile phase; Detection wavelength is 254nm; Number of theoretical plate calculates and should be not less than 1500 by emodin peak;
3, the preparation of reference substance solution respectively precision take emodin, the each 5mg of chrysophanol reference substance, put in 50ml measuring bottle, add methanol to scale, shake up; Precision measures emodin reference substance solution, the each 1ml of chrysophanol reference substance, puts in 25ml measuring bottle, adds methanol to scale, shakes up, and obtains and (in emodin, the every 1ml of chrysophanol, respectively contains 4 μ g).
Typical case 1, patient, female, 23 years old, one week mainly with front starting cough, more and more severe, and often cough the whole night, has cold symptoms, and the symptom of nasal obstruction slowly increases the weight of, and uses this law to treat during this, oral, each serving 125ml, every day 2 times.Within 7 days, be a course for the treatment of, treat after 3 courses for the treatment of, recovery from illness.
Typical case 2, patient, man, 29 years old, pharyngeal excitement (comprise foreign body sensation, burn feeling, be dried, itch, hypodynia etc.); The chronic diffusivity hyperemia of pharyngeal inspection pharyngeal mucosa, attached a little viscous secretion.During this, use this law to treat after 3 courses for the treatment of, recovery from illness.
Typical case 3, patient, female, 35 years old, long stimulus is flat to be coughed; Vocal cords fatiguability, snoring etc.Use this law to treat after 3 courses for the treatment of, recovery from illness.
Typical case 4, patient, man, 32 years old, foreign body in pharynx sense, long stimulus is flat to be coughed.Use this law to treat after 3 courses for the treatment of, recovery from illness.
Typical case 5, patient, man, 36 years old, foreign body in pharynx sense, long stimulus is flat to be coughed.Use this law to treat after 3 courses for the treatment of, recovery from illness.
Typical case 6, patient, man, 34 years old, pharyngeal discomfort, pain, itch or dry sensation, time have burning sensation, sootiness sense, a foreign body sensation etc.; Irritable cough, plays firmly expectoration secretions morning, even exerts one's utmost effort.Use this law to treat after 3 courses for the treatment of, recovery from illness.
Claims (5)
1. treat a Chinese medicine composition for upper respiratory tract infection, it is characterized in that this Chinese medicine composition is made up of following a few taste medical materials: Radix Rehmanniae 10g ?30g; Radix Scrophulariae 10g ?30g; Radix Ophiopogonis 5g ?20g; Colla Corii Asini 5g ?20g; Radix Et Rhizoma Rhei 20g ?40g; Radix Polygoni Multiflori 5g ?20g; Radix Trichosanthis 20g ?60g; Gypsum Fibrosum 20g ?60g; Sargassum 10g ?30g; Rhizoma Corydalis 5g ?20g; Folium Eriobotryae 5g ?20g; Fructus Cannabis 5g ?20g.
2. the Chinese medicine composition for the treatment of upper respiratory tract infection as claimed in claim 1, is characterized in that this Chinese medicine composition is made up of following medical material: Radix Rehmanniae 20g; Radix Scrophulariae 20g; Radix Ophiopogonis 10g; Colla Corii Asini 10g; Radix Et Rhizoma Rhei 30g; Radix Polygoni Multiflori 10g; Radix Trichosanthis 40g; Gypsum Fibrosum 40g; Sargassum 20g; Rhizoma Corydalis 10g; Folium Eriobotryae 10g; Fructus Cannabis 10g.
3. treat a preparation method for the medicine of upper respiratory tract infection, it is characterized in that comprising the following steps:
1, by ten Herba indigoferae Pseudotinctoriae claimed in claim 1 except Colla Corii Asini, pulverize, cross 65 mesh sieves, accurately take in pot for boiling chinese traditional medicine, add 2 times of amount pure water, decoct 2 hours with being steam heated to boil, leach medicinal liquid;
2, in filtering residue, add 1 times of amount purified water, being heated to boil decocts 1 hour, leaches medicinal liquid.
3, merge twice filtrate, add centrifuge centrifugal, rotating speed is 1000r/min, takes out supernatant, and Colla Corii Asini is added in supernatant, and it is fully dissolved, and heating is concentrated into 1000ml, and conventional semi-finished product inspection is carried out in sampling;
4, vial and bottle stopper are cleaned, controlled and do with pure water, the extracting solution quantitative filling of after the assay was approved, in vial, is tamping to bottle stopper;
5, the medicinal liquid of embedding is put into sterilizing cabinet, flowing steam sterilization 30 minutes;
6, the medicinal liquid after sterilizing being cooled to room temperature preserves.
4. the preparation method of the medicine for the treatment of upper respiratory tract infection as claimed in claim 3, is characterized in that after step 3, described semi-finished product following methods being checked:
Semi-finished product content measuring standard: every 1ml contains Radix Et Rhizoma Rhei with emodin (C
15h
10o
5) and chrysophanol (C
15h
10o
4) total, must not be less than 15 μ g;
1, chromatographic condition and system suitability octadecylsilane chemically bonded silica are filler; Jia Chun ?0.1% phosphoric acid solution (64 ?90: 36 ?10) be mobile phase; Detect wavelength be 250 ?258nm; Number of theoretical plate calculates and should be not less than 1500 by emodin peak;
2, the preparation of reference substance solution respectively precision take emodin, chrysophanol reference substance each 5 ?10mg, put in 50ml measuring bottle, add methanol constant volume, shake up; Precision measures emodin reference substance solution, the each 1ml of chrysophanol reference substance, puts in 25ml measuring bottle, adds methanol constant volume, shakes up, and to obtain final product;
3, the preparation precision of need testing solution measures this product 10ml, puts in flask, add 30% Yi Chun ?hydrochloric acid (10: 1) 15ml, put in water-bath heating hydrolysis 1 hour, cooling immediately, extract 4 times with the powerful jolting of chloroform, each 15ml, combined chloroform liquid, puts evaporate to dryness in water-bath, residue with Wu Shui Yi Chun ?ethyl acetate (2: 1) dissolve, in dislocation 25ml measuring bottle, and be diluted to scale, shake up, with microporous filter membrane filtration, get subsequent filtrate, to obtain final product;
4, algoscopy accurate reference substance solution and the each 10 μ l of need testing solution of drawing respectively, injection liquid chromatography, measures, and to obtain final product; If underproof words product can not use.
5. the preparation method of the medicine for the treatment of upper respiratory tract infection as claimed in claim 4, is characterized in that above-mentioned chromatographic condition and system suitability are as follows:
With octadecylsilane chemically bonded silica be filler; Jia Chun ?0.1% phosphoric acid solution (85: 15) be mobile phase; Detection wavelength is 254nm; Number of theoretical plate calculates and should be not less than 1500 by emodin peak;
Being prepared as follows of above-mentioned reference substance solution:
Precision takes emodin, the each 5mg of chrysophanol reference substance respectively, puts in 50ml measuring bottle, adds methanol to scale, shakes up; Precision measures emodin reference substance solution, the each 1ml of chrysophanol reference substance, puts in 25ml measuring bottle, adds methanol to scale, shakes up, and obtains and (in emodin, the every 1ml of chrysophanol, respectively contains 4 μ g).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410098611.4A CN103860871A (en) | 2014-03-16 | 2014-03-16 | Traditional Chinese medicinal composition for treating upper respiratory infections and preparation method thereof |
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|---|---|---|---|
| CN201410098611.4A CN103860871A (en) | 2014-03-16 | 2014-03-16 | Traditional Chinese medicinal composition for treating upper respiratory infections and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101085198A (en) * | 2007-06-29 | 2007-12-12 | 王海锋 | Internal-applied traditional Chinese medicine composition for treating chronic pharyngitis |
| CN101773603A (en) * | 2010-03-04 | 2010-07-14 | 李伟华 | Chinese medicine preparation for treating acute pharyngitis |
| CN102698216A (en) * | 2012-04-21 | 2012-10-03 | 王伟良 | Formula and preparation method of medicament for preventing and treating cold and cough |
-
2014
- 2014-03-16 CN CN201410098611.4A patent/CN103860871A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101085198A (en) * | 2007-06-29 | 2007-12-12 | 王海锋 | Internal-applied traditional Chinese medicine composition for treating chronic pharyngitis |
| CN101773603A (en) * | 2010-03-04 | 2010-07-14 | 李伟华 | Chinese medicine preparation for treating acute pharyngitis |
| CN102698216A (en) * | 2012-04-21 | 2012-10-03 | 王伟良 | Formula and preparation method of medicament for preventing and treating cold and cough |
Non-Patent Citations (1)
| Title |
|---|
| 姜惠卿等: "中药治疗慢性咽炎37例效果观察", 《齐鲁医学杂志》, vol. 18, no. 3, 30 September 2003 (2003-09-30), pages 357 * |
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Application publication date: 20140618 |