CN103859575B - A kind of moist-keeping agent for tobacco and application thereof - Google Patents

A kind of moist-keeping agent for tobacco and application thereof Download PDF

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Publication number
CN103859575B
CN103859575B CN201410037368.5A CN201410037368A CN103859575B CN 103859575 B CN103859575 B CN 103859575B CN 201410037368 A CN201410037368 A CN 201410037368A CN 103859575 B CN103859575 B CN 103859575B
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China
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tobacco
glycerol
moist
propylene glycol
sorbitol
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CN103859575A (en
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刘绍华
杨靖
白家峰
毛多斌
李志华
贾春晓
陈义昌
王花俊
田兆福
郑坚强
李小兰
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Zhengzhou University of Light Industry
China Tobacco Guangxi Industrial Co Ltd
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Zhengzhou University of Light Industry
China Tobacco Guangxi Industrial Co Ltd
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Abstract

The invention discloses a kind of moist-keeping agent for tobacco and using method thereof.Moist-keeping agent for tobacco is natural propolis extract, or natural propolis extract and propylene glycol, glycerol or the mixed solution of sorbitol, in mixed solution, natural propolis extract is 10 90%:90 10% with the part by weight of water, propylene glycol, glycerol or sorbitol.Being sprayed uniformly by moist-keeping agent for tobacco and be added on tobacco shred, spray adds 0.1 1.0% that ratio is tobacco shred weight.In tobacco shred, the method according to the middle regulation of YC/T28.8 1996 " the mensuration moisture of Medicated cigarette physical property " of moisture content measures, and result shows that humectation effect exceedes the traditional humectant of propylene glycol, glycerol or the sorbitol etc. commonly used at present.

Description

A kind of moist-keeping agent for tobacco and application thereof
Technical field
The present invention relates to a kind of moist-keeping agent for tobacco and application thereof, belong to technical field of tobacco processing.
Background technology
Along with improving constantly of our people's living standard, consumer is to the sucking quality of Medicated cigarette and safety the most increasingly Pay close attention to, improve the safety of smoking be increasingly becoming China's tobacco business can the common objective of survival and development.Along with current China Being greatly reduced of tobacco product tar content, the original flavouring essence quality of Nicotiana tabacum L. is by large effect, and the burnt technology fragrant with guarantor of fall becomes For the key of restriction Medicated cigarette development at present, particularly in the case of current tar content has had the biggest decline, Medicated cigarette to be kept The most significantly dropping Jiao while inhaling taste, its difficulty will be increasing.How while reducing tar content in cigarette, Medicated cigarette fragrance remains to be accepted by consumer, has become as the main attack problem of cigarette industry, is also to affect China cigarette product Jiao The key factor that oil reduces.Research and development over 10 years, China's tobacco business has generally been grasped and has been reduced coke tar in cigarette Technology, by reform tobacco formulation structure, uses high-air-permeability and the fireballing cigarette paper of quiet combustion and application filter tip ventilation dilution Etc. technical measures, it is possible on purpose reduce tar.But the current common problem of China's tobacco enterprise is: in order to reduce Tar and use the dry sensation on the sense organ that the technology such as reconstituted tobacco, filter tip ventilation dilution brought;And due to China north and south Climate difference is big, and the most northerly winter climate is dried, and the moisture of cigarette shreds is easy to scatter and disappear and causes Medicated cigarette not protect Card has preferably sucks effect.
Domestic tobacco business quickly grew in recent years, and research strength and innovation level are greatly improved, but increased at Medicated cigarette Fragrant humectation application, there is also gap with foreign well-known enterprise.The humectant that China's tobacco enterprise commonly uses at present is for many Hydroxy alcohols, such as: propylene glycol, glycerol, sorbitol etc., humectation effect is not ideal, along with constantly sending out of China's tobacco industry Exhibition, the expansion of product market scope, under different weather conditions, ensure that Medicated cigarette all has and preferably suck effect and compensate fall Jiao The loss of the fragrance brought is enterprise's urgent problem.
Research finds, the Main Ingredients and Appearance in propolis is: a flavone compound: mainly include flavonoid, flavonols and double Hydrogen flavonoid etc.;B terpene compound: mainly have monoterpene and sesquiterpenoids in propolis, minority is Diterpenes chemical combination Thing;C acid compounds: mainly include benzoic acid, P-hydroxybenzoic acid, cinnamic acid and derivant thereof;D alcohol compound: main Including benzoic acid, Z-betulenol, acetoxyl group-2-betulenol etc.;E phenol, aldehyde, ketone, ester, ether compound: mainly have fourth Fragrant phenol, vanillin, different 4-hydroxyl-3-methoxylbenxaldehyde, benzaldehyde, β-cyclocitral, 4,5-dimethyl-4 benzene, cyclohexenone, P-coumaric acid ester, Caffeic acid ester, ring alcohol benzoate, to tonquinol Rhizoma et radix valerianae acid esters, styrene ether, to methoxy styrene ether etc.;F enzyme thing Matter: such as various active enzymes such as amylase, cathepsin, lipase, trypsin;G vitamin: such as vitamin B1, vitamin P, provitamin A etc.;H macro-and trace-element: have aluminum, ferrum, calcium, silicon, strontium, zinc, cobalt, nickel, inscription, vanadium, stannum, barium, titanium, selenium, molybdenum, Antimony etc. are kind more than 30;Other material: several amino acids, polysaccharide compound etc..Composition in visible propolis is the abundantest, and these become The effect with humectation having in Fen, some composition also has rare natural anti-oxidation simultaneously, can effectively remove The free radical of flue gas, strengthen Medicated cigarette sucks safety, and propolis itself also has charming fragranced, these features All make propolis have preferable application prospect in Medicated cigarette, be worth further investigation further.
Summary of the invention
The purpose of the present invention develops a kind of new tobacco humectant natural propolis extract just, or is natural propolis Extract and propylene glycol, glycerol or sorbitol mixed solution.Natural propolis is used solvent extraction, supercritical extraction or surpasses Obtain propolis extract after sound extraction, extract is added into propylene glycol, glycerol or Pyrusussuriensis according to the ratio of 10 100% In alcohol, uniform spray is added on tobacco shred, and it is 0.1 1.0% that spray adds ratio, and in tobacco shred, the mensuration of moisture content is according to YC/T28.8 The method of regulation in 1996 " the mensuration moisture of Medicated cigarette physical property ", result shows that humectation effect exceedes third commonly used at present The tradition humectant such as glycol, glycerol or sorbitol.
The present invention is achieved through the following technical solutions:
A kind of moist-keeping agent for tobacco, for natural propolis extract, or be natural propolis extract and water, propylene glycol, Glycerol or sorbitol mixed solution.
Natural propolis extract is 10-90%:90-10% with the mass ratio of propylene glycol, glycerol or sorbitol.
Propolis extract of the present invention, preferably uses solvent extraction, supercritical extraction or ultrasonic by natural propolis Propolis extract is obtained after extraction.
The using method of above-mentioned moist-keeping agent for tobacco, is uniformly sprayed onto described humectant on tobacco shred, and adding proportion is Tobacco shred weight 0.1-1.5%.
In tobacco shred, the mensuration of moisture content is according to regulation in YC/T28.8 1996 " the mensuration moisture of Medicated cigarette physical property " Method, result shows that humectation effect exceedes the traditional humectant of propylene glycol, glycerol or the sorbitol etc. commonly used at present.
Additionally, moist-keeping agent for tobacco can effectively remove the free radical of flue gas, strengthen Medicated cigarette sucks safety.
Detailed description of the invention
Below by specific embodiment, the invention will be further described.With the moist-keeping agent for tobacco of the present invention with universal The tradition humectants such as propylene glycol, glycerol or the sorbitol used carry out use and compare, and result see table 1, specific embodiment As follows: extracting method can be filled into?Embodiment 1:
Weigh 50 grams of tobacco shreds, according to 0.1% addition humectant of tobacco shred weight, consisting of of humectant: the propolis of 40% carries Take thing+60% propylene glycol, the moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, with Time do controlled trial with the propylene glycol of identical weight.
Embodiment 2:
Weigh 50 grams of tobacco shreds, according to 0.3% addition humectant of tobacco shred weight, consisting of of humectant: the propolis of 30% carries Take thing+70% glycerol, the moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, with Time do controlled trial with the glycerol of identical weight.
Embodiment 3:
Weigh 50 grams of tobacco shreds, according to 1.5% addition humectant of tobacco shred weight, consisting of of humectant: the propolis of 10% carries Take thing+90% sorbitol, the moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, with Time with the sorbitol of identical weight for doing controlled trial.
Embodiment 4:
Weigh 50 grams of tobacco shreds, according to tobacco shred weight 0.1% addition humectant, consisting of of humectant: propolis extract, The moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, simultaneously with identical weight Propylene glycol does controlled trial.
Embodiment 5:
Weigh 50 grams of tobacco shreds, according to 0.7% addition humectant of tobacco shred weight, consisting of of humectant: the propolis of 70% carries Take thing+30% propylene glycol, the moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, with Time do controlled trial with the propylene glycol of identical weight.
Embodiment 6:
Weigh 50 grams of tobacco shreds, according to 0.5% addition humectant of tobacco shred weight, consisting of of humectant: the propolis of 60% carries Take thing+40% glycerol, the moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, with Time do controlled trial with the glycerol of identical weight.
Embodiment 7:
Weigh 50 grams of tobacco shreds, according to 0.3% addition humectant of tobacco shred weight, consisting of of humectant: the propolis of 80% carries Take thing+20% sorbitol, the moisture content of tobacco shred after measuring 96 hours under conditions of relative humidity 40% according to the method for standard, with Time do controlled trial with the sorbitol of identical weight.
Above example result shows: moist-keeping agent for tobacco of the present invention exceedes the most universal for the humectation effect of tobacco shred The tradition humectants such as propylene glycol, glycerol or the sorbitol used.
Table 1
Propolis-containing sample moisture content % Control sample moisture content %
Embodiment 1 13.83 13.07
Embodiment 2 14.28 13.29
Embodiment 3 13.91 13.34
Embodiment 4 14.61 13.51
Embodiment 5 14.37 13.56
Embodiment 6 14.58 13.63
Embodiment 7 14.76 13.65

Claims (1)

1. a moist-keeping agent for tobacco, it is characterised in that described humectant consists of natural propolis extract, or is natural Propolis extract and propylene glycol, glycerol or sorbitol mixed solution;
Described natural propolis extract be natural propolis is used solvent extraction, supercritical extraction or ultrasonic extraction after obtain honeybee Glue extract;
Natural propolis extract is 10-90%:90-10% with the mass ratio of propylene glycol, glycerol or sorbitol;
Uniformly being sprayed onto on tobacco shred by described humectant, adding proportion is tobacco shred weight 0.1-1.5%.
CN201410037368.5A 2014-01-26 2014-01-26 A kind of moist-keeping agent for tobacco and application thereof Active CN103859575B (en)

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Publication number Priority date Publication date Assignee Title
CN104138027B (en) * 2014-07-08 2016-01-13 山东津美生物科技有限公司 tobacco humectant
CN104305510A (en) * 2014-08-20 2015-01-28 云南中烟工业有限责任公司 Humectant for cigarettes and application thereof
CN104585872A (en) * 2015-01-20 2015-05-06 川渝中烟工业有限责任公司 Electronic cigarette liquid containing water soluble propolis and preparation method thereof
CN105029666B (en) * 2015-07-30 2017-05-31 湖南省烟草公司邵阳市公司隆回县分公司 Flue-cured tobacco upgrading flavouring NMF and its application method under a kind of arid low moisture environments
CN108013501B (en) * 2017-11-29 2020-09-29 广西中烟工业有限责任公司 Application of humectant for cigarettes

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US4802498A (en) * 1987-07-02 1989-02-07 Warren Ogren Resin-based chewing tobacco
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CN102240060B (en) * 2011-05-12 2013-01-02 重庆市超临界精细化工生产力促进中心有限公司 Food preservative and sausage using same
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