CN103806272A - Animal hair fiber softening agent and preparation method thereof - Google Patents
Animal hair fiber softening agent and preparation method thereof Download PDFInfo
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- CN103806272A CN103806272A CN201410032206.2A CN201410032206A CN103806272A CN 103806272 A CN103806272 A CN 103806272A CN 201410032206 A CN201410032206 A CN 201410032206A CN 103806272 A CN103806272 A CN 103806272A
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Abstract
The invention discloses an animal hair fiber softening agent and a preparation method thereof. The animal hair fiber softening agent comprises the following raw materials in parts by weight: 45-50 parts of peanut oil, 20-30 parts of diethylenetriamine, 0.05-0.08 part of an activating agent, 0.5-1.2 parts of a microcapsule essence, 1-3 parts of a water-retaining agent, 0.5-0.8 part of an organic silicon defoaming agent, 1-2 parts of a bactericide and 2-3 parts of an antistatic finishing agent. The antistatic finishing agent, the bactericide and the water-retaining agent are simultaneously added into the softening agent, so that the functions of removing static electricity, sterilizing and guaranteeing fiber elasticity are really integrated in the softening agent, and the performance of animal hair fibers is effectively guaranteed; furthermore, natural plant oil is used as a raw material, so that the animal hair fiber softening agent has non-toxic and environment-friendly effects and is suitable for large-scale production.
Description
Technical field
The present invention relates to seed hair fiber softener and preparation method thereof.
Background technology
Along with the raising of people's living standard, people also improve accordingly to the quality requirement of wearing clothing.Especially the clothing of making for animal hair, although warming, wash the problem of protecting after of long duration and be just directly connected to clothing newness degree.Common softener has compliance function to the clothing of any material, but as sterilization, fluffy texts be inaccessiable, so need to develop a kind of multi-functional softener and meet people's needs.
Summary of the invention
For the deficiencies in the prior art, the invention provides seed hair fiber softener and preparation method thereof.
For solving prior art problem, the technical solution used in the present invention is: a seed hair fiber softener, comprise the following raw material of meter by weight: peanut oil 45-50 part, diethylenetriamines 20-30 part, activator 0.05-0.08 part, microcapsule essence 0.5-1.2 part, water retention agent 1-3 part, silicone defoaming agent 0.5-0.8 part, bactericide 1-2 part, antistatic finishing agent 2-3 part.
As improved, described activator is potassium hydroxide.
As improved, described bactericide is imidazoline quaternary ammonium salt.
The preparation method of a described seed hair fiber softener, comprises the following steps:
(1) take above-mentioned raw materials according to weight fraction;
(2) add peanut oil, diethylenetriamines and activator to being full of in the reactor of nitrogen, be heated to 160-180 ℃, heating duration be after 2-3 hour intermediate;
(3) in intermediate, add water retention agent, silicone defoaming agent, bactericide, antistatic finishing agent, be constantly stirred at 70-80 ℃ and heat 2-4 hour, after naturally cooling 1-2 hour, then at 50-60 ℃, heat after 30-50 minute to obtain softener.
Beneficial effect of the present invention: the present invention adds antistatic finishing agent, bactericide and water retention agent in the formula of softener simultaneously; really will destatic, sterilization and assurance fibrous elasticity merge in softener; effectively guarantee the performance of wool fibre; and raw material is natural plant grease; asepsis environment-protecting, is applicable to large-scale production.
The specific embodiment
Further explain the present invention below in conjunction with embodiment:
Embodiment 1
One seed hair fiber softener, comprises the following raw material of meter by weight: 45 parts of peanut oil, 20 parts of diethylenetriamines, 0.05 part, activator, 0.5 part of microcapsule essence, 1 part of water retention agent, 0.5 part of silicone defoaming agent, 1 part, bactericide, 2 parts of antistatic finishing agents.
As improved, described activator is potassium hydroxide.
As improved, described bactericide is imidazoline quaternary ammonium salt.
The preparation method of a described seed hair fiber softener, comprises the following steps:
(1) take above-mentioned raw materials according to weight fraction;
(2) add peanut oil, diethylenetriamines and activator to being full of in the reactor of nitrogen, be heated to 160 ℃, heating duration be after 2 hours intermediate;
(3) in intermediate, add water retention agent, silicone defoaming agent, bactericide, antistatic finishing agent again, be constantly stirred at 70 ℃ and heat 2 hours, after naturally cooling 1 hour, then at 50 ℃, heat after 30 minutes to obtain softener.
Embodiment 2
One seed hair fiber softener, comprises the following raw material of meter by weight: 50 parts of peanut oil, 30 parts of diethylenetriamines, 0.08 part, activator, 1.2 parts of microcapsule essences, 3 parts of water retention agents, 0.8 part of silicone defoaming agent, 2 parts, bactericide, 3 parts of antistatic finishing agents.
As improved, described activator is potassium hydroxide.
As improved, described bactericide is imidazoline quaternary ammonium salt.
The preparation method of a described seed hair fiber softener, comprises the following steps:
(1) take above-mentioned raw materials according to weight fraction;
(2) add peanut oil, diethylenetriamines and activator to being full of in the reactor of nitrogen, be heated to 180 ℃, heating duration be after 3 hours intermediate;
(3) in intermediate, add water retention agent, silicone defoaming agent, bactericide, antistatic finishing agent again, be constantly stirred at 70-80 ℃ and heat 4 hours, after naturally cooling 2 hours, then at 60 ℃, heat after 50 minutes to obtain softener.
Embodiment 3
48 parts of peanut oil, 25 parts of diethylenetriamines, 0.06 part, activator, 1.0 parts of microcapsule essences, 2 parts of water retention agents, 0.6 part of silicone defoaming agent, 1.5 parts, bactericide, 2.5 parts of antistatic finishing agents.
As improved, described activator is potassium hydroxide.
As improved, described bactericide is imidazoline quaternary ammonium salt.
The preparation method of a described seed hair fiber softener, comprises the following steps:
(1) take above-mentioned raw materials according to weight fraction;
(2) add peanut oil, diethylenetriamines and activator to being full of in the reactor of nitrogen, be heated to 170 ℃, heating duration be after 2.5 hours intermediate;
(3) in intermediate, add water retention agent, silicone defoaming agent, bactericide, antistatic finishing agent again, be constantly stirred at 75 ℃ and heat 3 hours, after naturally cooling 1.5 hours, then at 55 ℃, heat after 40 minutes to obtain softener.
According to relevant criterion, the present invention is carried out to index determining, utilizes after process clothes of the present invention relatively performance simultaneously:
Show by above-mentioned data, wool fibre softener antistatic effect of the present invention is strong, and compliance is good, and the antibacterial time is long, effectively guarantees clothing quality.
The above embodiment is only the preferred embodiment for absolutely proving that the present invention lifts, and protection scope of the present invention is not limited to this.What those skilled in the art did on basis of the present invention is equal to alternative or conversion, all within protection scope of the present invention.Protection scope of the present invention is as the criterion with claims.
Claims (4)
1. a seed hair fiber softener, it is characterized in that comprising the following raw material of meter by weight: peanut oil 45-50 part, diethylenetriamines 20-30 part, activator 0.05-0.08 part, microcapsule essence 0.5-1.2 part, water retention agent 1-3 part, silicone defoaming agent 0.5-0.8 part, bactericide 1-2 part, antistatic finishing agent 2-3 part.
2. a seed hair fiber softener according to claim 1, is characterized in that: described activator is potassium hydroxide.
3. a seed hair fiber softener according to claim 1, is characterized in that: described bactericide is imidazoline quaternary ammonium salt.
4. the preparation method of a seed hair fiber softener claimed in claim 1, is characterized in that comprising the following steps:
(1) take above-mentioned raw materials according to weight fraction;
(2) add peanut oil, diethylenetriamines and activator to being full of in the reactor of nitrogen, be heated to 160-180 ℃, heating duration be after 2-3 hour intermediate;
(3) in intermediate, add water retention agent, silicone defoaming agent, bactericide, antistatic finishing agent, be constantly stirred at 70-80 ℃ and heat 2-4 hour, after naturally cooling 1-2 hour, then at 50-60 ℃, heat after 30-50 minute to obtain softener.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410032206.2A CN103806272A (en) | 2014-01-24 | 2014-01-24 | Animal hair fiber softening agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410032206.2A CN103806272A (en) | 2014-01-24 | 2014-01-24 | Animal hair fiber softening agent and preparation method thereof |
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| CN103806272A true CN103806272A (en) | 2014-05-21 |
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| CN201410032206.2A Withdrawn CN103806272A (en) | 2014-01-24 | 2014-01-24 | Animal hair fiber softening agent and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105442315A (en) * | 2015-12-18 | 2016-03-30 | 张莘蔓 | Novel silk softening agent and preparation method thereof |
| CN105926282A (en) * | 2016-05-15 | 2016-09-07 | 沂水祥腾化工有限公司 | Preparing method of cationic softener |
| CN111471535A (en) * | 2020-05-13 | 2020-07-31 | 杭州炫墨生物科技有限公司 | Antistatic smooth washing powder |
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| CN101185614A (en) * | 2007-11-30 | 2008-05-28 | 华南理工大学 | Modified polyhydroxy cation quaternary ammonium salt thickening soft finishing agent and preparation and application thereof |
| CN101509192A (en) * | 2009-03-04 | 2009-08-19 | 深圳天鼎精细化工制造有限公司 | Method of preparing cation fatty acid softening agent |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105442315A (en) * | 2015-12-18 | 2016-03-30 | 张莘蔓 | Novel silk softening agent and preparation method thereof |
| CN105926282A (en) * | 2016-05-15 | 2016-09-07 | 沂水祥腾化工有限公司 | Preparing method of cationic softener |
| CN111471535A (en) * | 2020-05-13 | 2020-07-31 | 杭州炫墨生物科技有限公司 | Antistatic smooth washing powder |
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Application publication date: 20140521 |