Background technology
The bark of eucommia is warm in nature, and taste is sweet, has filling liver kidney, strong waist knee, strengthening the bones and muscles, antiabortive effect.The bark of eucommia has regulating action in various degree to immune system, internal system, central nervous system, the circulatory system and urinary system, and the excited Pituitary Adrenal cortex system of bark of eucommia energy, strengthens adrenal cortex function.Dry bark, is smooth en plaque or roll film shape, and big or small thickness differs, and general thick approximately 3~10 millimeters, is about 40~100 centimetres.Outer surface taupe brown, coarse, there are irregular lobe groove line and rhomboid transverse fissure hole skin, sometimes visible light gray lichens spot.But how commodity the rough skin of truncated section, therefore outer surface light brown is more level and smooth.Inner surface is smooth, mulberry.The crisp frangibility of matter, section has silvery white filiform to be connected, fine and closely woven, slightly retractility.Gas is micro-, and taste is slightly bitter, and that chews has a gummy residue.Large with skin depth, rough skin scraping, outside yellowish-brown, inner face pitchy and light, the many persons of the Shi Baisi that fractures are for good.Bark is containing gutta-percha 6~10%, and Gen Piyue is containing 10~12%, and leaf is containing gutta-percha 2%~4%.In addition, go back 0.142 milligram of % of glucoside-containing, 0.066 milligram of % of alkaloid, 6.5 milligrams of % of pectin, fat 2.9 milligrams of %, 1.76 milligrams of % of resin, 0.25 milligram of % of organic acid, ketose (be hydrolyzed front 2.15 milligrams of %, be hydrolyzed rear 3.5 milligrams of %), 0.7 milligram of % of Catergen, in addition.Contain vitamin E, Cobastab and beta carotene etc., also contain the necessary trace element of a lot of human bodies, aldose, chlorogenic acid.The aliphatic acid of the contained fat oil of seed consists of leukotrienes 67.38%, linoleic acid 9.97%, oleic acid 15.81%, stearic acid 2.15%. palmitic acid 4.68%.Fruit gel content can reach 27%, is soluble in ethanol, acetone and other organic solvent.
Publication number is that the Chinese patent of CN1098918 discloses a kind of leaves-of-eucommia natural health-care products and production technology thereof, take folium cortex eucommiae as primary raw material, then is equipped with hawthorn, sea-buckthorn, honey, tealeaves etc. and makes.Utilize the method for normal temperature extraction to extract the medicinal ingredient of folium cortex eucommiae, do not destroy its active material.This product takes full advantage of the medicine resource of folium cortex eucommiae, has the functions such as hypotensive, filling liver kidney, strengthening the bones and muscles, antiulcer, reducing blood lipid.
Publication number is that the Chinese patent of CN1400199 discloses a kind of method of extracting continuously bioactivator take folium cortex eucommiae as raw material, comprise (one), take water, methyl alcohol or ethanol as extractant, extract or heat the operation such as extraction, macroporous resin adsorption and ethanol elution and extract the method for eucommia total glycosides and eucommiae total flavones by sonic oscillation; (2), take water, methyl alcohol or ethanol as extractant, by macroreticular resin separate, the method for the operation chlorogenic acid extracting such as ethyl acetate extraction and mixed solvent recrystallization and eucommiae total flavones and (three), take acidic aqueous solution as extractant, from extracted the Eucommia ulmoides leave dregs other active ingredient, extract the method for eucommia acidic polysaccharose by operations such as macroreticular resin separation, decolorizing with activated carbon and ethanol precipitations.Technical process of the present invention is simple, cost is low, product yield is high, improved the comprehensive utilization ratio in folium cortex eucommiae with health care and medical active ingredient, has increased the economic worth of folium cortex eucommiae.
Publication number is that the Chinese patent of CN1335178 discloses a kind of eucommia ulmoides extract extracting from Eucommia ulmoides Oliv. leaves and production method thereof, be characterized in extracting raw material and have selected folium cortex eucommiae, demineralized water, calcium hydroxide 6kg, ferric trichloride 6kg and resin, its advantage is to extract market eucommia ulmoides extract in short supply without the Eucommia ulmoides Oliv. leaves of value by being considered in the past, the simple science of extracting method, the eucommia ulmoides extract of producing can be with the eucommia ulmoides extract that extracts in eucommia bark than beautiful, both saved resource, protect again environment, a kind of desirable eucommia ulmoides extract and the production method extracted from Eucommia ulmoides Oliv. leaves thereof.
Publication number is a kind of method that the Chinese patent of CN1293104 discloses barked eucommia, comprises the following steps: it is first that bacterial classification is cultivated; Next is to extract metabolin; The 3rd is to measure valid density; The 4th is the preparation of biologic product; The 5th is bark band girdle; The 6th is to spray pelt position; The 7th is film bundling, wraps up and after 30 days, opens film, spraying preparation again.The inventive method is easily gone, production technology and simple to operate, and with low cost, easy to use, peeling position neonatal cell obviously thickens, and regeneration is rapidly.
Publication number is that the Chinese patent of CN1593188 discloses a kind of eucommia ulmoides feed additive, it is eucommia leaf extract, mainly through by Fresh Folium Eucommiae drying and crushing, folium cortex eucommiae after pulverizing is joined in multifunctional dynamic extraction pot to lixiviate in forced refluence circulation, quick desuperheat to 20~25 ℃ of leaching liquor, through precipitation, centrifugation, Vacuum Concentration, dry and obtain.In eucommia ulmoides extracts, at least contain 3.5~10% chlorogenic acid, eucommia bark flavone 20~30%, eucommia bark polycose 25~45%.The present invention can be able to be absorbed by livestock and poultry more fully, can obviously improve the immunity of livestock and poultry, does not affect the adaptability of feed, can combine use with common feedstuffs additive and veterinary drug, have no drug resistance and hazard residue, animal and human's body is had no side effect, free from environmental pollution.
Publication number is that the Chinese patent of CN1568833 discloses a kind of eucommia instant tea, by Bark of Eucommia Ulmoides leaf, through the lixiviate of water low temperature, removal of impurities, filtration, ultrafiltration, filtrate concentrate drying and the bark of eucommia water-soluble extractive making, table sugar or starch, maltodextrin, cycloheptaamylose, citric acid, ISOASCORBIC ACID-sodium etc. are formulated in addition.Eucommia instant tea provided by the invention, major ingredient is bark of eucommia water-soluble extractive, the elite of its concentrated bark of eucommia, active ingredient can be soluble in water fully rapidly, drinks conveniently, and effect is more outstanding and obvious, and good without astringent taste, mouthfeel.
Publication number is that the Chinese patent of CN101138374 discloses a kind of cortex encomia bag tea particles and preparation method thereof, belongs to people natural health care, the particularly health food take plant as raw material, and its preparation method.The raw material of preparing its active component comprises Bark of Eucommia Ulmoides or folium cortex eucommiae, mulberry leaf, lophatherum gracile etc.Preparation method decocts these raw materials to extract, concentrated, and extract dry is pulverized, and granulates and get final product.Its advantage is that product has the blood fat of adjusting, regulates blood pressure, clearing heat and detoxicating effect.Can effectively reduce cholesterol, triglyceride levels in blood sugar, softening blood vessel, reduction blood, fatty liver and hypertension are all had to good effect.Particularly there is good health-care effect for the various symptoms of current sub-health population.
Publication number is that the Chinese patent of CN101223928 discloses a kind of eucommia Bark male flower instant tea and preparation method thereof, raw material adopts eucommia Bark male flower, folium cortex eucommiae, hawthorn, the root of kudzu vine, its preparation comprise clearly choose, 9 technical process such as drip washing, heat treatment, heat radiation, extraction, filtration, concentrated, granulation, pack.Eucommia Bark male flower instant tea prepared by the present invention, eucommia Bark male flower in its raw material, folium cortex eucommiae, hawthorn, the root of kudzu vine have hypotensive, reducing blood lipid, prevention cerebral thrombus and miocardial infarction, the prevention senile dementia that effect direction is consistent, antitumor, anti-ageing, strengthen the functions such as immunity.Therefore the stack of four taste effects, has compound synergistic effect; And long-pendingization that disappear of hawthorn is stagnant, tonifying spleen stomach strengthening function, the function of the filling liver kidney that improves cardiac function and eucommia Bark male flower, folium cortex eucommiae of the root of kudzu vine reaches complementation, makes its health care more outstanding.And be rich in calcium, phosphorus, magnesium, potassium etc., nutritious, pleasant to the palate.
Publication number is that the Chinese patent of CN101559092 discloses a kind of eucommia ulmoides extracts and has the application in the composition of sedative-hypnotic effect in preparation, also disclose eucommia ulmoides extracts in the application for the preparation of in Cure for insomnia, anxiety or convulsions composition, this eucommia ulmoides extracts is to extract and form continuously through benzinum, ethyl acetate, n-butanol, second alcohol and water from Bark of Eucommia Ulmoides, folium cortex eucommiae, eucommia Bark male flower and or bark of eucommia complete stool.The present invention extracts and obtains eucommia ulmoides extracts from the plant bark of eucommia, and it is carried out to the research in the application of tranquilizing soporific field, result shows: eucommia ulmoides extracts has significant sedative-hypnotic effect and anticonvulsant action, the wherein successful of bark of eucommia ethyl acetate extract and bark of eucommia n-butanol extract, to develop to there is the novel healthy food of hypnosis sedation and the natural active matter of new drug, can be used for the nervous system diseases such as Cure for insomnia, anxiety or convulsions, and have no side effect and psychic dependence.
Publication number is that the Chinese patent of CN102144706A discloses a kind of eucommia ulmoides extract feed additive and preparation method thereof, and this preparation is evenly mixed in carrier after repeatedly extracting by skin and the leaf of the bark of eucommia.Its preparation method is: step 1, tentatively extract the Pi Heye of the bark of eucommia; Residue after step 2, secondary cycle extraction step 1 extract, the medicinal extract of gained is uniformly mixed to form a kind of eucommia ulmoides extract feed additive with carrier after spray drying treatment.The present invention has filling liver kidney benefit gas, strengthening the bones and muscles, anti-inflammation, meat improvement, improves the function of animal immunizing power.
Publication number is that the Chinese patent of CN102640910A discloses a kind of bark of eucommia sweet potato powder and production method thereof, by raw material warp and the face of following percentage by weight, squeezing, maturing, aging, freezing, the powder that thaws out forms: eucommia leaf extract 0.5~2.5%, starch from sweet potato 96.0~98%, salt 0.5~1.2%, food additives 0.3~0.6%, described eucommia leaf extract is the alcohol extract of folium cortex eucommiae, described food additives are zinc sulfate and Sodium Polyacrylate, the mixture of one or more in acetate starch and sodium alginate, the present invention is added with eucommia ulmoides extracts, making this traditional food of sweet potato noodles increase health care is worth, special raw material proportioning and production technology can effectively keep the active ingredient of eucommia ulmoides extracts, make product there is good perception and mouthfeel, there is stronger toughness, boil for a long time not rotten, and can in the situation that not add the harmful substances such as alum, more easily realize and open silk.
Publication number is method and the drink thereof that the Chinese patent of CN1480067 discloses a kind of removing saline foreign taste by fermenting folium cortex encommiae, comprise folium cortex eucommiae pretreatment and two technical process of fermentation, the folium cortex eucommiae cleaning is toasted 10~30 minutes in 40~120 ℃ of temperature ranges, or put it in boiling water and steam 1~20 minute, after being taken out, folium cortex eucommiae packs immediately compacting in container, sealing into, under 20~60 ℃ of constant temperature, place 3~20 minutes, to the de-green blackening of leaf fermentation, take out, must remove the folium cortex eucommiae of pained peculiar smell.Not only can effectively remove the pained peculiar smell of folium cortex eucommiae but also can make original active component in folium cortex eucommiae not run off by this fermentation technique, greatly improve the comprehensive utilization ratio in folium cortex eucommiae raw material with health care and medicinal active ingredient, increase the economic worth of folium cortex eucommiae.The advantages such as that the eucommia bark coffee drink of preparing take fermentation folium cortex eucommiae extract as raw material and bark of eucommia date juice drinks have is natural, nutrition, agreeable to the taste sense are good.
At present, after In Guangdong Province adopts folium cortex eucommiae directly to pulverize, raising chicken and duck can greatly reduce the generation of pestilence, long-time a large amount of chicken and duck of feeding can cause the feed to feed to reduce, folium cortex eucommiae mouthfeel is poor, the advantage of the bark of eucommia itself is a lot, and adopting at present the bark of eucommia is raw material, makes single tea beverage or be simply mixed and made into the documents and materials of mixed feed a lot, but these modes are processed the function composition that all can not make full use of the bark of eucommia, therefore process technology needs further to be solved.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of technique of carrying out feed addictive processing for folium cortex eucommiae and skin.
It is the mouthfeel that makes full use of starch material enzymolysis in Ipomoea batatas and regulate bark of eucommia product that one of object of this technique is provided, to change the sensory issues such as pained peculiar smell of existing single raw material.
Another object that this technique is provided is to realize the bark of eucommia in process, to retain as far as possible its function composition, prevents from process, losing or changing into other material.
Another object that this technique is provided is that the product energy practical function composition obtaining by this technique is more comprehensive, in case the problem such as products obtained therefrom composition is single.
Another object that this technique is provided is that the product obtaining by this technique can be realized preservation more for a long time, and function composition is difficult for changing.
For solving the problems of the technologies described above, realize above-mentioned purpose, product of a kind of feed addictive of substitute antibiotics and preparation method thereof, the technical scheme that this case provides is: fresh feed through completing, be dried, the step such as enzymolysis, fermentation, lixiviate, granulation is prepared from.
The microorganism fungus kind that the present invention adopts, Hansenula anomala (Hansenula anomala) derives from China Committee for Culture Collection of Microorganisms's common micro-organisms center, and numbering is respectively CGMCC No.2.297; Fermentative lactobacillus (Lactobacillus fermentium) derives from China Committee for Culture Collection of Microorganisms's common micro-organisms center, and numbering is respectively CGMCC No.1.2029.
The preparation of Hansenula anomala powder: cultivate by saccharomycete CGMCC No.2.297 cultural method, centrifugation medium obtains yeast thalline, is wet yeast thalline.
The preparation of lactic acid bacteria: cultivate by lactic acid bacteria CGMCC No.1.2029 cultural method, centrifugation medium obtains wet lactic acid thalline, is wet lactic acid thalline.
Procedure of processing in the technology of the present invention solution is as follows:
(1) fresh leaf: the Fresh Folium Eucommiae that adopts 1 bud 1 leaf, 1 bud 2 leaves or the equal tender degree of 1 bud 3 leaf;
(2) complete: adopt conventional continuous dryer to dry fresh leaf folium cortex eucommiae, temperature control 60-70 ℃, thickness 1.0-1.5cm, time 10-15min, when oven dry, vaned water content is controlled at 15-20%, spreading for cooling 20min;
(3) extracting: after 50 ℃, carry out lixiviate folium cortex eucommiae 1-3h with benzinum, remove benzinum, the folium cortex eucommiae that obtains degreasing and come unstuck, then it is crushed to 1-15 order;
(4) enzymolysis: dry sweet potato is pulverized, added water to make it water content and reach about 40-55%, then add carbohydrase to carry out partially saccharifying 5-8h, filter once with three layers of gauze;
(5) mix: get folium cortex eucommiae, wet thallus and the wheat flour processed a certain amount of filtrate adding and mix placement 1-3h;
(6) granulation: mixture is inserted in comminutor, and granulation under 50 ℃~60 ℃ temperature and 45rpm~55rpm condition, obtains the particle of 0.8mm~0.90mm;
(7) dry: to obtained particle vacuum drier heat drying, 40 ℃~50 ℃ of temperature, vacuum 620mmHg~630mmHg, dry 3h~5h, obtains electuary particle, and pellet moisture is between 2.5%~3%.
In a specific embodiments, the amount (L) of benzinum described in step (3) is 2-4:1 with folium cortex eucommiae weight (KG) ratio.
In a specific embodiments, carbohydrase described in step (4), enzyme activity reaches 5000U/g, and adding enzyme amount (KG) and weight (KG) ratio of dry sweet potato is 1-3:50.
In a specific embodiments, described in step (5), adding folium cortex eucommiae (KG), wet thallus (KG) and the wheat flour (KG) processed is 1:1-3:6-7:10-15 with filtrate volume (L) ratio.
In a specific embodiments, wet thallus described in step (5) refer to by yeast thalline and wet lactic acid thalline by etc. weight mix and obtain.
Beneficial effect
1, by yeast and lactobacillus-fermented, greatly improve the mouthfeel of feed, farthest retained in folium cortex eucommiae effective efficiency composition if chlorogenic acid is at the content of feed simultaneously.
2, this method makes full use of starch in Ipomoea batatas, and rapidly gelatinization in pyroprocess, for embedding folium cortex eucommiae provides condition, provides sugared source by saccharification for yeast and lactic acid bacteria again, for feed provides the more nutrition of horn of plenty simultaneously.
3, pass through fermentation process, effectively improve fragrance and the flavour of feed, chlorogenic acid isoreactivity composition does not affect growth of microorganism simultaneously, has overcome the common shortcoming of traditional handicraft product flavour, aspect product fragrance, be also improved, fragrant and sweet taste is stronger lasting simultaneously.
The specific embodiment
Below, the present invention will be further detailed with embodiment, but it is not limited to any or the similar example of these embodiment.
Embodiment 1
Adopt the Fresh Folium Eucommiae of 1 bud 1 leaf, 1 bud 2 leaves or the equal tender degree of 1 bud 3 leaf; Adopt conventional continuous dryer to dry fresh leaf folium cortex eucommiae, temperature control 60-70 ℃, thickness 1.0-1.5cm, time 10-15min, when oven dry, vaned water content is controlled at 15-20%, spreading for cooling 20min; After 50 ℃, carry out lixiviate 100kg folium cortex eucommiae 2h with 300L benzinum, remove benzinum, the folium cortex eucommiae that obtains degreasing and come unstuck, then it is crushed to 1-15 order; 200kg dry sweet potato is pulverized, added water to make it water content and reach 45% left and right, then add 5kg carbohydrase to carry out partially saccharifying 6h, filter once with three layers of gauze; Measuring in 100L filtrate adds folium cortex eucommiae, 20kg wet thallus and the 70kg wheat flour that 10kg processed to mix placement 2h; Mixture is inserted in comminutor, granulation under 50 ℃~60 ℃ temperature and 45rpm~55rpm condition, obtains the particle of 0.8mm~0.90mm again; To obtained particle vacuum drier heat drying, 40 ℃~50 ℃ of temperature, vacuum 620mmHg~630mmHg, dry 3h~5h, obtains electuary particle, and pellet moisture is between 2.5%~3%.
Embodiment 2
Adopt the Fresh Folium Eucommiae of 1 bud 1 leaf, 1 bud 2 leaves or the equal tender degree of 1 bud 3 leaf; Adopt conventional continuous dryer to dry fresh leaf folium cortex eucommiae, temperature control 60-70 ℃, thickness 1.0-1.5cm, time 10-15min, when oven dry, vaned water content is controlled at 15-20%, spreading for cooling 20min; After 50 ℃, carry out lixiviate 200kg folium cortex eucommiae 2h with 500L benzinum, remove benzinum, the folium cortex eucommiae that obtains degreasing and come unstuck, then it is crushed to 1-15 order; 200kg dry sweet potato is pulverized, added water to make it water content and reach 55% left and right, then add 6kg carbohydrase to carry out partially saccharifying 8, filter once with three layers of gauze; Measuring in 200L filtrate adds folium cortex eucommiae, 35kg wet thallus and the 130kg wheat flour that 15kg processed to mix placement 2h; Mixture is inserted in comminutor, granulation under 50 ℃~60 ℃ temperature and 45rpm~55rpm condition, obtains the particle of 0.8mm~0.90mm again; To obtained particle vacuum drier heat drying, 40 ℃~50 ℃ of temperature, vacuum 620mmHg~630mmHg, dry 3h~5h, obtains electuary particle, and pellet moisture is between 2.5%~3%.
Embodiment 3
Adopt the Fresh Folium Eucommiae of 1 bud 1 leaf, 1 bud 2 leaves or the equal tender degree of 1 bud 3 leaf; Adopt conventional continuous dryer to dry fresh leaf folium cortex eucommiae, temperature control 60-70 ℃, thickness 1.0-1.5cm, time 10-15min, when oven dry, vaned water content is controlled at 15-20%, spreading for cooling 20min; After 50 ℃, carry out lixiviate 300kg folium cortex eucommiae 2h with 800L benzinum, remove benzinum, the folium cortex eucommiae that obtains degreasing and come unstuck, then it is crushed to 1-15 order; 200kg dry sweet potato is pulverized, added water to make it water content and reach 40% left and right, then add 10kg carbohydrase to carry out partially saccharifying 5h, filter once with three layers of gauze; Measuring in 200L filtrate adds folium cortex eucommiae, 40kg wet thallus and the 100kg wheat flour that 25kg processed to mix placement 1h; Mixture is inserted in comminutor, granulation under 50 ℃~60 ℃ temperature and 45rpm~55rpm condition, obtains the particle of 0.8mm~0.90mm again; To obtained particle vacuum drier heat drying, 40 ℃~50 ℃ of temperature, vacuum 620mmHg~630mmHg, dry 3h~5h, obtains electuary particle, and pellet moisture is between 2.5%~3%.
Embodiment 4
Adopt the Fresh Folium Eucommiae of 1 bud 1 leaf, 1 bud 2 leaves or the equal tender degree of 1 bud 3 leaf; Adopt conventional continuous dryer to dry fresh leaf folium cortex eucommiae, temperature control 60-70 ℃, thickness 1.0-1.5cm, time 10-15min, when oven dry, vaned water content is controlled at 15-20%, spreading for cooling 20min; After 50 ℃, carry out lixiviate 400kg folium cortex eucommiae 2h with 1100L benzinum, remove benzinum, the folium cortex eucommiae that obtains degreasing and come unstuck, then it is crushed to 1-15 order; 200kg dry sweet potato is pulverized, added water to make it water content and reach 55% left and right, then add 8kg carbohydrase to carry out partially saccharifying 7h, filter once with three layers of gauze; Measuring in 300L filtrate adds folium cortex eucommiae, 60kg wet thallus and the 140kg wheat flour that 25kg processed to mix placement 3h; Mixture is inserted in comminutor, granulation under 50 ℃~60 ℃ temperature and 45rpm~55rpm condition, obtains the particle of 0.8mm~0.90mm again; To obtained particle vacuum drier heat drying, 40 ℃~50 ℃ of temperature, vacuum 620mmHg~630mmHg, dry 3h~5h, obtains electuary particle, and pellet moisture is between 2.5%~3%.