CN103790034A - Dyeing method by use of pigment of the first case of red (peony pigment) - Google Patents
Dyeing method by use of pigment of the first case of red (peony pigment) Download PDFInfo
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- CN103790034A CN103790034A CN201410019380.3A CN201410019380A CN103790034A CN 103790034 A CN103790034 A CN 103790034A CN 201410019380 A CN201410019380 A CN 201410019380A CN 103790034 A CN103790034 A CN 103790034A
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- tree peony
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Abstract
The invention relates to a dyeing method by use of pigment of the first case of red (peony pigment), relating to a natural pigment dyeing method. The dyeing method comprises the steps of preparing a mordant (potassium sulphate solution) and pigment solution of the first case of red; heating the potassium sulphate solution to be at more than 85 DEG C and mordanting a fabric; and heating the pigment solution of the first case of red to be at more than 80 DEG C and dyeing the fabric. The natural plant (the first case of red) dyeing method is firstly developed based on the characteristics of color of the first case of red, the annual cultivation and good velamen red coloring stability, the dyeing process is environmentally friendly and reliable, the combining capacity of the pigment dyes and the fabric is strong, the color fastness is improved and the fabric can be dyed evenly.
Description
Technical field
The present invention relates to a kind of colouring method of natural colouring matter, relate in particular to a kind of method dyeing with SHOUANHONG tree peony pigment.
Background technology
Research of Paeonia suffruticosa from ancient times to the present aromatic sung praises of oneself by people always.The people of other countries also treasure tree peony very much.Luoyang Peony with its special geographic mark, is spent very large lovely luster especially, is signifying elegant and poised and excellent, is described as " flower king "." Luoyang Peony is unsurpassed ", Luoyang also creates new varieties as example take the artificial cultivation of research of Paeonia suffruticosa, and application " natural selection and theory of artificial selection " has realized the cultivation technique of hundreds thousand of mu of tree peony plants.In the Luoyang Peony of ancient capital, have two tradition names to plant, open name Yao Huang of chrysanthemum for one, another opens pale reddish brown name Wei Zi, the exploitation that tool vegetable colour is yellow and red natural colour is knitted dyestuff.Compatriots wear reigning beauty national flower state and take integrated clothing in addition, have more the glamour of beautiful distinct Chinese characteristics; Therefore the distinguishingly vegetable colour development of rationality mark of tree peony, is pushed to the seat of honour that natural plant dyeing is researched and developed in recent years.
Tree peony yellow dye has been fixed as the yellow petal of Yao dyes, and has solved the Fastness Problems of dyeing at present, but is subject to especially the originate bottleneck of in great shortage costliness of its stability, needs to be continued research and development.And peony element Fastness Problems is also unresolved, especially red color is extremely unstable, does not substantially possess any feasibility from peony petal development dyestuff haematochrome; And it is inhomogeneous that existing colouring method is easy to cause dyeing.
Tradition tree peony fine work " SHOUANHONG " is aubergine, is unique a kind of triploid kind in current known tree peony, its leaf, and petiole, stem and Huadu are red, are also the curiosas in tree peony, belong to traditional category.This kind growth is vigorous, and annual shoot is long, is mulberry, becomes flower rate high, and descendant is less, and root system is royal purple.At present the tree peony vegetable colour especially research of SHOUANHONG tree peony pigment dyeing method is still belonged to blank.
Summary of the invention
The technical problem to be solved in the present invention is: a kind of method dyeing with SHOUANHONG tree peony pigment is provided, can effectively solves existing colouring method tree peony pigmentary color fastness inadequate, easily fade, and the inhomogeneous problem that dyes.
To achieve these goals, the technical solution used in the present invention is: a kind of method dyeing with SHOUANHONG tree peony pigment, comprises the following steps:
Step 1, take mordant potassium sulfate and be dissolved in water, potassium sulfate solution is transferred in mordant dyeing cylinder, the concentration of potassium sulfate solution is 30 mg/mL, for subsequent use;
Step 2, take SHOUANHONG tree peony pigment and be first dissolved in absolute ethyl alcohol, use again distilled water diluting, regulate pH=3-6.5, the SHOUANHONG tree peony pigment solution obtaining is transferred in staining jar, in described SHOUANHONG tree peony pigment solution, the concentration of SHOUANHONG tree peony pigment is 10 mg/mL, for subsequent use;
Step 3, the potassium sulfate solution in mordant dyeing cylinder is first heated to more than 85 ℃, then the fabric after carrying out washing treatment is inserted in mordant dyeing cylinder, be jointly heated to 90-100 ℃ and carry out mordant dyeing, after mordant dyeing, take out fabric, clean, dry in the shade;
Step 4, the SHOUANHONG tree peony pigment solution in staining jar is first heated to more than 80 ℃, then the fabric after mordant dyeing is inserted in staining jar, jointly being heated to 90-100 ℃ dyes, after dyeing, take out fabric, cleaning, drying, then clean with cold running water or hot water, and wash after stranding with washing agent, dry.
In described step 2, in SHOUANHONG tree peony pigment solution, the concentration of volume percent of ethanol is 5-10%.
In described step 2, the pH value of SHOUANHONG tree peony pigment solution is 4-5.
In described step 3, the time of mordant dyeing is 12-15 minute.
The time of dyeing in described step 4 is 25-40 minute.
Carrying out washing treatment process to fabric in described step 3 is: first with detergent by fabric ultrasonic processing 15 minutes in 60-70 ℃ of water, impurity, grease, slurry are removed in washing, finally dry.
The beneficial effect that the present invention brings is:
The present invention is based on good looks and its feature that cultivation is annual and phloxin chromatic colorant is stable of tree peony SHOUANHONG kind, develop first the colouring method of natural plant dye tree peony SHOUANHONG, this dyestuff is strong to natural protein fiber and polyamide fibre binding ability, strong coloring force, fabric can be dyed to peony, dyeing environmental protection is reliable.
Adopt the process of first mordant dyeing poststaining, SHOUANHONG tree peony pigment is very sensitive to potassium sulfate mordant, and the use of potassium sulfate can make the binding ability of colouring substance and fabric stronger, has improved the COLOR FASTNESS of dyeing.
Prepare staining solution with SHOUANHONG tree peony pigment in staining procedure time, pigment is first fully dissolved in ethanol, arrive respective concentration with distilled water diluting again, this be because SHOUANHONG tree peony pigment in ethanol solubility than large in water, do solvent with ethanol, can dissolve more fully pigment, than the independent use amount that makes water do solvent to have saved pigment raw material, and can make the homogeneous transparent and stable of staining solution, make textile dyeing more even.
The pH of SHOUANHONG tree peony pigment solution is adjusted to 3-6.5, this is that maximum absorption wavelength and absorbance change hardly because SHOUANHONG tree peony pigment is stable under acid condition, and especially pH value is that 4 o'clock stability is best, pigment can not decompose, and then improves Color.
Mordant potassium sulfate solution is first heated to more than 85 ℃, then the fabric after carrying out washing treatment is inserted in mordant dyeing cylinder, jointly be heated to 90-100 ℃ and carry out mordant dyeing, it is that dissolving in order to make mordant is more abundant that mordant solution is heated in advance, when mordant dyeing, make mordant distribute on fabric more even, and then pigment and the even combination of mordant while making to dye, dye more even.Because be the aqueous solution of inorganic salts, there is not the unfavorable factor of decomposing with other.
SHOUANHONG tree peony pigment solution in staining jar is first heated to more than 80 ℃, and it is also that dissolving in order to make pigment is more abundant that SHOUANHONG tree peony pigment solution is preheated, and dyes more even; Fabric after mordant dyeing is inserted in staining jar, be jointly heated to 90-100 ℃ and dye, can improve the adhesion between pigment and fabric, improve COLOR FASTNESS.Ultraviolet spectra detects known, and SHOUANHONG tree peony pigment changes hardly at 50-100 ℃, illustrates that this pigment is stable between 50-100 ℃, that is to say that SHOUANHONG tree peony pigment is subject to hardly the impact of temperature and changes.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
The method dyeing with SHOUANHONG tree peony pigment, comprises the following steps:
Step 1, take mordant potassium sulfate and be dissolved in water, potassium sulfate solution is transferred in mordant dyeing cylinder, the concentration of potassium sulfate solution is 30 mg/mL, for subsequent use;
Step 2, take SHOUANHONG tree peony pigment and be first dissolved in absolute ethyl alcohol, use again distilled water diluting, regulate pH=3-6.5, the SHOUANHONG tree peony pigment solution obtaining is transferred in staining jar, in described SHOUANHONG tree peony pigment solution, the concentration of SHOUANHONG tree peony pigment is 10 mg/mL, for subsequent use;
Step 3, the potassium sulfate solution in mordant dyeing cylinder is first heated to more than 85 ℃, then the fabric after carrying out washing treatment is inserted in mordant dyeing cylinder, be jointly heated to 90-100 ℃ and carry out mordant dyeing, after mordant dyeing, take out fabric, clean, dry in the shade;
Step 4, the SHOUANHONG tree peony pigment solution in staining jar is first heated to more than 80 ℃, then the fabric after mordant dyeing is inserted in staining jar, jointly being heated to 90-100 ℃ dyes, after dyeing, take out fabric, cleaning, drying, then clean with cold running water or hot water, and wash after stranding with washing agent, dry.
In described step 2, in SHOUANHONG tree peony pigment solution, the concentration of volume percent of ethanol is 5-10%.
In described step 2, the pH value of SHOUANHONG tree peony pigment solution is 4-5.
In described step 3, the time of mordant dyeing is 12-15 minute.
The time of dyeing in described step 4 is 25-40 minute.
Carrying out washing treatment process to fabric in described step 3 is: first with detergent by fabric ultrasonic processing 15 minutes in 60-70 ℃ of water, impurity, grease, slurry are removed in washing, finally dry.
embodiment mono-
mordant preparation: take 3 grams of potassium sulfates and be dissolved in the aqueous solution of 100 mL, be transferred in mordant dyeing cylinder, for subsequent use.
The preparation of SHOUANHONG tree peony colouring substance solution: take 1 gram of SHOUANHONG tree peony pigment and be dissolved in the ethanol of 10mL, then with distilled water diluting to 100mL, be adjusted to pH=3, the SHOUANHONG tree peony pigment solution obtaining is transferred in staining jar, for subsequent use.
Take 5 grams of white pure Woolen yarns and first use detergent ultrasonic processing 15 minutes in 60-70 ℃ of hot water, impurity, grease, slurry are removed in washing, dry, insert again in the mordant dyeing cylinder of 85 ℃ of heating baths, jointly be heated to 90 ℃ of direct mordant dyeings 8 minutes, pull out rear with running water clean after, dry in the shade; Then be placed in temperature and be the staining jar of 80 ℃, in staining jar, the concentration of SHOUANHONG tree peony pigment is 10 mg/mL, is then heated to 90 ℃ and constantly stir, and dyeing time 25 minutes, takes out pollutant, cleans post-drying can be dyed to mauve fabric with clear water.Then clean with cold running water or hot water cleaning, and wash after stranding with washing agent, dry nondiscolouring after 3-5 days.
embodiment bis-
mordant preparation: take 30 grams of potassium sulfates and be dissolved in the aqueous solution of 1000 mL, be transferred in mordant dyeing cylinder, for subsequent use.
The preparation of SHOUANHONG tree peony colouring substance solution: take 10 grams of SHOUANHONG tree peony pigments and be dissolved in the ethanol of 50mL, then with distilled water diluting to 1000mL, be adjusted to pH=4, the SHOUANHONG tree peony pigment solution obtaining is transferred in staining jar, for subsequent use.
Take 13 grams of white pure wool fabrics and first use detergent ultrasonic processing 15 minutes in 60-70 ℃ of hot water, impurity, grease, slurry are removed in washing, dry, insert again in the mordant dyeing cylinder of 90 ℃ of heating baths, jointly be heated to 95 ℃ of direct mordant dyeings 15 minutes, pull out rear with running water clean after, dry in the shade; Then be placed in temperature and be the staining jar of 85 ℃, in staining jar, the concentration of SHOUANHONG tree peony pigment is 10 mg/mL, is then heated to 95 ℃ and constantly stir, and dyeing time 30 minutes, takes out pollutant, cleans post-drying can be dyed to red fabric with clear water.Then clean with cold running water or hot water cleaning, and wash after stranding with washing agent, dry nondiscolouring after 3-5 days.
embodiment tri-
mordant preparation: take 6 grams of potassium sulfates and be dissolved in the aqueous solution of 200 mL, be transferred in mordant dyeing cylinder, for subsequent use.
The preparation of SHOUANHONG tree peony colouring substance solution: take 5 grams of SHOUANHONG tree peony pigments and be dissolved in the ethanol of 50mL, then with distilled water diluting to 500mL, be adjusted to pH=6.5, the SHOUANHONG tree peony pigment solution obtaining is transferred in staining jar, for subsequent use.
Take the ultrasonic processing 15 minutes in 60-70 ℃ of hot water of 15 grams of white nylon fabrics detergent, washing remove impurity, grease,, dry, insert again in the mordant dyeing cylinder of 93 ℃ of heating baths, jointly be heated to 100 ℃ of direct mordant dyeings 12 minutes, pull out rear with running water clean after, dry in the shade; Then be placed in temperature and be the staining jar of 90 ℃, in staining jar, the concentration of SHOUANHONG tree peony pigment is 10 mg/mL, is then heated to 100 ℃ and constantly stir, and dyeing time 40 minutes, takes out pollutant, cleans post-drying can be dyed to red fabric with clear water.Then clean with cold running water or hot water cleaning, and wash after stranding with washing agent, dry nondiscolouring after 3-5 days.
Claims (6)
1. the method dyeing with SHOUANHONG tree peony pigment, is characterized in that: comprise the following steps:
Step 1, take mordant potassium sulfate and be dissolved in water, potassium sulfate solution is transferred in mordant dyeing cylinder, the concentration of potassium sulfate solution is 30 mg/mL, for subsequent use;
Step 2, take SHOUANHONG tree peony pigment and be first dissolved in absolute ethyl alcohol, use again distilled water diluting, regulate pH=3-6.5, the SHOUANHONG tree peony pigment solution obtaining is transferred in staining jar, in described SHOUANHONG tree peony pigment solution, the concentration of SHOUANHONG tree peony pigment is 10 mg/mL, for subsequent use;
Step 3, the potassium sulfate solution in mordant dyeing cylinder is first heated to more than 85 ℃, then the fabric after carrying out washing treatment is inserted in mordant dyeing cylinder, be jointly heated to 90-100 ℃ and carry out mordant dyeing, after mordant dyeing, take out fabric, clean, dry in the shade;
Step 4, the SHOUANHONG tree peony pigment solution in staining jar is first heated to more than 80 ℃, then the fabric after mordant dyeing is inserted in staining jar, jointly being heated to 90-100 ℃ dyes, after dyeing, take out fabric, cleaning, drying, then clean with cold running water or hot water, and wash after stranding with washing agent, dry.
2. a kind of method dyeing with SHOUANHONG tree peony pigment as claimed in claim 1, is characterized in that: in described step 2, in SHOUANHONG tree peony pigment solution, the concentration of volume percent of ethanol is 5-10%.
3. a kind of method dyeing with SHOUANHONG tree peony pigment as claimed in claim 1, is characterized in that: in described step 2, the pH value of SHOUANHONG tree peony pigment solution is 4.
4. a kind of method dyeing with SHOUANHONG tree peony pigment as claimed in claim 1, is characterized in that: in described step 3, the time of mordant dyeing is 12-15 minute.
5. a kind of method dyeing with SHOUANHONG tree peony pigment as claimed in claim 1, is characterized in that: the time of dyeing in described step 4 is 25-40 minute.
6. a kind of method dyeing with SHOUANHONG tree peony pigment as claimed in claim 1, it is characterized in that: the carrying out washing treatment process to fabric in described step 3 is: first with detergent by fabric ultrasonic processing 15 minutes in 60-70 ℃ of water, impurity, grease, slurry are removed in washing, finally dry.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410019380.3A CN103790034B (en) | 2014-01-16 | 2014-01-16 | A kind of SHOUANHONG tree peony pigment carries out the method dyeed |
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| CN201410019380.3A CN103790034B (en) | 2014-01-16 | 2014-01-16 | A kind of SHOUANHONG tree peony pigment carries out the method dyeed |
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| CN103790034B CN103790034B (en) | 2016-01-13 |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1900174A (en) * | 2006-07-27 | 2007-01-24 | 河南科技大学 | Method for extracting peony flower pigment |
| CN101469517A (en) * | 2007-12-27 | 2009-07-01 | 恒源祥（集团）有限公司 | Method for dyeing peony pigment on protein fibre fabric |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1900174A (en) * | 2006-07-27 | 2007-01-24 | 河南科技大学 | Method for extracting peony flower pigment |
| CN101469517A (en) * | 2007-12-27 | 2009-07-01 | 恒源祥（集团）有限公司 | Method for dyeing peony pigment on protein fibre fabric |
Non-Patent Citations (1)
| Title |
|---|
| 胡少刚: "天然植物染料在蛋白质纤维织物上的染色性研究", 《CNKI优秀硕士学位论文全文库》, 31 December 2008 (2008-12-31) * |
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