CN103757898A - Polyester fiber finishing agent and preparation method thereof - Google Patents
Polyester fiber finishing agent and preparation method thereof Download PDFInfo
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- CN103757898A CN103757898A CN201310751318.9A CN201310751318A CN103757898A CN 103757898 A CN103757898 A CN 103757898A CN 201310751318 A CN201310751318 A CN 201310751318A CN 103757898 A CN103757898 A CN 103757898A
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Abstract
The invention discloses a polyester fiber finishing agent and a preparation method thereof. The polyester fiber finishing agent is prepared from the following components by weight ratio: 2-5 parts of dimethyl silicone oil, 3-5 parts of ammonium chloride, 3-7 parts of palm wax, 4-7 parts of polypropylene glycol, 5-10 parts of ethyl acetate, 2-4 parts of diethylenetriamine, 2-3 parts of triethylene tetramine and 130-145 parts of water. The preparation method of the polyester fiber finishing agent comprises the steps of heating, stirring, shearing and the like, and polyester fiber fabric has high color fastness to washing, and is softer and more comfortable after being finished by using the prepared finishing agent.
Description
Technical field
The present invention relates to a kind of finishing agent and preparation method thereof, particularly relate to finishing agent of a kind of dacron fabric and preparation method thereof.
Background technology
Polyester fiber is a large amount of a kind of synthetic fiber that use in field of textiles at present, and the use amount of polyester fiber is primary in the use amount of various synthetic fiber, in life neutralization work, often can touch polyester fiber.Polyester fiber can be used to be made into clothing etc.Polyester fiber textiles, by using finishing agent to arrange it, can improve the various resistance to fastness of polyester fiber, as wash resistance to fastness, the resistance to fastness that rubs, the resistance to fastness of sweat stain etc.In the middle of this, wash resistance to fastness very crucial, if the resistance to fastness of the washing of polyester fiber is lower, after repeatedly cleaning, the fabric of polyester fiber there will be the phenomenon that significantly fades, and has a strong impact on normal use.
Summary of the invention
The technical problem solving: conventional dacron fabric is having the large-area problem fading after repeatedly cleaning, and it is not high not pass through its soft degree of polyester fiber of Special Finishing.
Technical scheme: the invention discloses a kind of polyester fiber finishing agent and preparation method thereof, polyester fiber finishing agent is comprised of according to weight ratio following composition: dimethicone is that 2～5 parts, ammonium chloride are that 3～5 parts, palm wax are that 3～7 parts, polypropylene glycol are that 4～7 parts, ethyl acetate are that 5～10 parts, diethylenetriamine are that 2～4 parts, triethylene tetramine are that 2～3 parts, water are 130～145 parts.
A preparation method for polyester fiber finishing agent, comprises the following steps: (1) is 60 ℃～65 ℃ by retort Temperature Setting; (2) to dropping into water in retort, be that 130～145 parts, polypropylene glycol are that 4～7 parts, ethyl acetate are 5～10 parts, three kinds of compositions are stirred; (3) to adding dimethicone in retort, be that 2～5 parts, ammonium chloride are that 3～5 parts, palm wax are 3～7 parts again after stirring, stir; (4) retort is cooled to after room temperature, adding diethylenetriamine is that 2～4 parts, triethylene tetramine are 2～3 parts, with cutter, shears, and shearing rotating speed is 400rpm, and the time is 3min～5min.Wherein, prepare the dimethicone that finishing agent adds and be preferably 2 parts.Prepare the diethylenetriamine that finishing agent adds and be preferably 3～4 parts.Prepare the ammonium chloride that finishing agent adds and be preferably powder.
Beneficial effect: after dacron fabric arranges with finishing agent of the present invention, color fastness to washing (GB/T3921.1-1997) grade of dacron fabric is higher, COLOR FASTNESS is 5 grades, has promoted the soft degree of polyester fiber simultaneously, has promoted the quality of polyester fiber.
The specific embodiment
Embodiment 1
(1) by retort Temperature Setting, it is 60 ℃; (2) to dropping into water in retort, be that 130kg, polypropylene glycol are that 7kg, ethyl acetate are 10kg, three kinds of compositions are stirred; (3) to adding dimethicone in retort, be that 2kg, ammonium chloride are that 3kg, palm wax are 7kg again after stirring, stir; (4) retort is cooled to after room temperature, adding diethylenetriamine is that 4kg, triethylene tetramine are 2kg, with cutter, shears, and shearing rotating speed is 400rpm, and the time is 5min, after shearing finishes, prepares polyester fiber finishing agent.
Embodiment 2
(1) by retort Temperature Setting, it is 65 ℃; (2) to dropping into water in retort, be that 140kg, polypropylene glycol are that 4kg, ethyl acetate are 7kg, three kinds of compositions are stirred; (3) to adding dimethicone in retort, be that 3kg, ammonium chloride are that 5kg, palm wax are 5kg again after stirring, stir; (4) retort is cooled to after room temperature, adding diethylenetriamine is that 2kg, triethylene tetramine are 3kg, with cutter, shears, and shearing rotating speed is 400rpm, and the time is 3min, after shearing finishes, prepares polyester fiber finishing agent.
Embodiment 3
(1) by retort Temperature Setting, it is 62 ℃; (2) to dropping into water in retort, be that 145kg, polypropylene glycol are that 5kg, ethyl acetate are 5kg, three kinds of compositions are stirred; (3) to adding dimethicone in retort, be that 5kg, ammonium chloride are that 4kg, palm wax are 3kg again after stirring, stir; (4) retort is cooled to after room temperature, adding diethylenetriamine is that 3kg, triethylene tetramine are 2kg, with cutter, shears, and shearing rotating speed is 400rpm, and the time is 4min, after shearing finishes, prepares polyester fiber finishing agent.
Get the clothing of 100% polyester fiber, soak 3h with the finishing agent of embodiment 1, embodiment 2, embodiment 3, one soaks one rolls, and pick-up is 75%, is dried to dry at 95 ℃.Measured its color fastness to washing, testing standard is GB/T3921.1-1997, the results are shown in following table.
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Color fastness to washing | 5 grades | 5 grades | 5 grades |
| Soft degree | Be significantly improved | Be significantly improved | Be significantly improved |
Dacron fabric is after arranging through finishing agent of the present invention, and its color fastness to washing and soft degree are all significantly improved, and have promoted the quality of dacron fabric, have expanded the scope of application of dacron fabric.
Claims (5)
1. a polyester fiber finishing agent, is characterized in that polyester fiber finishing agent is comprised of according to weight ratio following composition: dimethicone is that 2～5 parts, ammonium chloride are that 3～5 parts, palm wax are that 3～7 parts, polypropylene glycol are that 4～7 parts, ethyl acetate are that 5～10 parts, diethylenetriamine are that 2～4 parts, triethylene tetramine are that 2～3 parts, water are 130～145 parts.
2. the preparation method of a kind of polyester fiber finishing agent according to claim 1, is characterized in that preparation method comprises the following steps: (1) is 60 ℃～65 ℃ by retort Temperature Setting; (2) to dropping into water in retort, be that 130～145 parts, polypropylene glycol are that 4～7 parts, ethyl acetate are 5～10 parts, three kinds of compositions are stirred; (3) to adding dimethicone in retort, be that 2～5 parts, ammonium chloride are that 3～5 parts, palm wax are 3～7 parts again after stirring, stir; (4) retort is cooled to after room temperature, adding diethylenetriamine is that 2～4 parts, triethylene tetramine are 2～3 parts, with cutter, shears, and shearing rotating speed is 400rpm, and the time is 3min～5min.
3. the preparation method of a kind of polyester fiber finishing agent according to claim 2, it is characterized in that preparing the dimethicone that finishing agent adds is 2 parts.
4. the preparation method of a kind of polyester fiber finishing agent according to claim 2, it is characterized in that preparing the diethylenetriamine that finishing agent adds is 3～4 parts.
5. the preparation method of a kind of polyester fiber finishing agent according to claim 2, it is characterized in that preparing the ammonium chloride that finishing agent adds is powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310751318.9A CN103757898B (en) | 2013-12-31 | 2013-12-31 | A kind of polyester fiber finishing agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310751318.9A CN103757898B (en) | 2013-12-31 | 2013-12-31 | A kind of polyester fiber finishing agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103757898A true CN103757898A (en) | 2014-04-30 |
| CN103757898B CN103757898B (en) | 2015-11-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310751318.9A Active CN103757898B (en) | 2013-12-31 | 2013-12-31 | A kind of polyester fiber finishing agent and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105463852A (en) * | 2016-01-08 | 2016-04-06 | 湖州市千金丝织厂 | Novel soft finishing agent and preparation method thereof |
| CN107956124A (en) * | 2017-11-30 | 2018-04-24 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of polyester fiber antibacterial and deodouring finishing agent |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101768867A (en) * | 2009-01-07 | 2010-07-07 | 卢爱华 | Fiber softening finishing agent |
| CN102418268A (en) * | 2010-09-27 | 2012-04-18 | 石拥民 | Color fixative for fabric treatment |
-
2013
- 2013-12-31 CN CN201310751318.9A patent/CN103757898B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101768867A (en) * | 2009-01-07 | 2010-07-07 | 卢爱华 | Fiber softening finishing agent |
| CN102418268A (en) * | 2010-09-27 | 2012-04-18 | 石拥民 | Color fixative for fabric treatment |
Non-Patent Citations (2)
| Title |
|---|
| 华文: "柔软剂的生产应用与技术进展", 《精细化工原料及中间体》 * |
| 张治国等: "织物用柔软剂研究进展", 《纺织学报》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105463852A (en) * | 2016-01-08 | 2016-04-06 | 湖州市千金丝织厂 | Novel soft finishing agent and preparation method thereof |
| CN107956124A (en) * | 2017-11-30 | 2018-04-24 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of polyester fiber antibacterial and deodouring finishing agent |
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| Publication number | Publication date |
|---|---|
| CN103757898B (en) | 2015-11-04 |
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Inventor after: Zhao Zhexue Inventor after: Chen Guoqing Inventor after: Sun Jie Inventor before: Zhang Dexuan |
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Effective date of registration: 20191225 Address after: 224300 Dongshou, Fuda Road, Xintan Town, Sheyang County, Yancheng City, Jiangsu Province (within the original Sheyang Tongchuang Cotton Industry Co., Ltd.) Patentee after: Yancheng Haiwei cotton Co., Ltd Address before: 7 groups of friendship village Songling town of Wujiang District of Suzhou City, Jiangsu province 215200 split eight community Patentee before: SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY CO., LTD. |