CN103741461A - Acrylic fabric finishing agent and preparation method thereof - Google Patents

Acrylic fabric finishing agent and preparation method thereof Download PDF

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Publication number
CN103741461A
CN103741461A CN201310749092.9A CN201310749092A CN103741461A CN 103741461 A CN103741461 A CN 103741461A CN 201310749092 A CN201310749092 A CN 201310749092A CN 103741461 A CN103741461 A CN 103741461A
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parts
finishing agent
acrylic fabric
sodium
fabric finishing
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CN201310749092.9A
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Chinese (zh)
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CN103741461B (en
Inventor
张德轩
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JIANGSU HUACHAO TEXTILE INDUSTRIAL CO., LTD.
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SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY Co Ltd
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Abstract

The invention discloses an acrylic fabric finishing agent and a preparation method thereof. The acrylic fabric finishing agent consists of the following components in parts by weight: 9-12 parts of cetyl sodium sulfate, 4-5 parts of alkyl diphenyl ether disulfonate, 6-9 parts of sodium dichloroisocyanurate, 3-4 parts of calcium chloride, 5-9 parts of tributyl phosphate, 1-2 parts of tryptophan, 22-26 parts of glycerin and 210-220 parts of water. The acrylic fabric finishing agent is prepared by stirring, mixing and heating. By using the obtained acrylic fabric finishing agent, the pilling resistance flame retardation of an acrylic fabric can be enhanced.

Description

A kind of acrylic fabric finishing agent and preparation method thereof
Technical field
The present invention relates to a kind of fabric finishing agent and preparation method thereof, particularly relate to a kind of acrylic fabric finishing agent that possesses ANTIPILLING, fire resistance and preparation method thereof.
Background technology
The material of acrylic fibers is polyacrylonitrile, is the material of chemical synthesis.Acrylic fabric, after friction repeatedly, can produce a large amount of thread balls, affects the dress of acrylic fibers material clothing.Conventional finishing agent was arranging after acrylic fabric, the balling-up situation of acrylic fabric is not effectively taken on a new look, in addition, the common function of finishing agent is comparatively single, and the finishing agent that possesses raising acrylic fabric anti-pilling property does not have fire-retardant performance conventionally, and fire-retardant performance is also for the very important a kind of character of acrylic fabric, if therefore finishing agent possesses this two kinds of functions simultaneously, at fabric, by after arranging, can possess good ANTIPILLING and fire-retardant effect, there is extraordinary prospect.
Summary of the invention
The technical problem solving: the problem that ANTIPILLING ability is poor, its flame retardant effect is poor of clothing prepared by conventional acrylic fabric.
Technical scheme: the invention discloses a kind of acrylic fabric finishing agent and preparation method thereof, acrylic fabric finishing agent is comprised of according to weight ratio following composition: sodium hexadecyl sulfate is that 9~12 parts, alkyl diphenyl ether disulphonic acid sodium are that 4~5 parts, sodium laurate are that 6~9 parts, calcium chloride are that 3~4 parts, tributyl phosphate are that 5~9 parts, tryptophan are that 1~2 part, glycerine are that 22~26 parts, water are 210~220 parts.
A kind of preparation method of acrylic fabric finishing agent, preparation method comprises the following steps: under (1) room temperature, getting sodium hexadecyl sulfate and be 9~12 parts, alkyl diphenyl ether disulphonic acid sodium and be 4~5 parts, sodium laurate and be 6~9 parts, water is 210~220 parts, and sodium hexadecyl sulfate, alkyl diphenyl ether disulphonic acid sodium, sodium laurate water are uniformly dissolved as mixed solution; (2) to adding tributyl phosphate in mixed solution, be that 5~9 parts, tryptophan are that 1~2 part, glycerine are 22~26 parts again, be uniformly dissolved after being heated to 55 ℃; (3) getting calcium chloride is 3~4 parts, and calcium chloride is pulverized as powder, and powder order number is 250 order~350 orders; (4) calcium chloride powder is joined in mixed solution, after stirring, prepare acrylic fabric finishing agent.
The sodium hexadecyl sulfate adding during preparation is 12 parts.
The sodium laurate adding during preparation is 9 parts.
The calcium chloride powder adding during preparation is 3 parts.
beneficial effect:the clothes that 80% acrylic fabric is made is after arranging through finishing agent of the present invention, and its ANTIPILLING grade is 4 to 5 grades, and its flame retardant rating is B1 level.
The specific embodiment
Embodiment 1
(1) under room temperature, getting sodium hexadecyl sulfate is that 9kg, alkyl diphenyl ether disulphonic acid sodium are that 5kg, sodium laurate are that 9kg, water are 210kg, and sodium hexadecyl sulfate, alkyl diphenyl ether disulphonic acid sodium, sodium laurate water are uniformly dissolved as mixed solution; (2) to adding tributyl phosphate in mixed solution, be that 9kg, tryptophan are that 1kg, glycerine are 22kg again, be uniformly dissolved after being heated to 55 ℃; (3) getting calcium chloride is 3kg, and calcium chloride is pulverized as powder, and powder order number is 250 orders; (4) calcium chloride powder is joined in mixed solution, after stirring, prepare acrylic fabric finishing agent.
Embodiment 2
(1) under room temperature, getting sodium hexadecyl sulfate is that 11kg, alkyl diphenyl ether disulphonic acid sodium are that 5kg, sodium laurate are that 6kg, water are 220kg, and sodium hexadecyl sulfate, alkyl diphenyl ether disulphonic acid sodium, sodium laurate water are uniformly dissolved as mixed solution; (2) to adding tributyl phosphate in mixed solution, be that 7kg, tryptophan are that 2kg, glycerine are 26kg again, be uniformly dissolved after being heated to 55 ℃; (3) getting calcium chloride is 4kg, and calcium chloride is pulverized as powder, and powder order number is 350 orders; (4) calcium chloride powder is joined in mixed solution, after stirring, prepare acrylic fabric finishing agent.
Embodiment 3
(1) under room temperature, getting sodium hexadecyl sulfate is that 12kg, alkyl diphenyl ether disulphonic acid sodium are that 4kg, sodium laurate are that 7kg, water are 215kg, and sodium hexadecyl sulfate, alkyl diphenyl ether disulphonic acid sodium, sodium laurate water are uniformly dissolved as mixed solution; (2) to adding tributyl phosphate in mixed solution, be that 5kg, tryptophan are that 1kg, glycerine are 24kg again, be uniformly dissolved after being heated to 55 ℃; (3) getting calcium chloride is 3kg, and calcium chloride is pulverized as powder, and powder order number is 300 orders; (4) calcium chloride powder is joined in mixed solution, after stirring, prepare acrylic fabric finishing agent.
The clothes that acrylic fibers content is 80%, cotton content is 20% is at room temperature dipped in the finishing agent of embodiment 1, embodiment 2, embodiment 3 and soaks 3h, two soak two rolls, and pick-up is to dry at 75%, 100 ℃.Its anti-pilling property and fire resistance assay method are respectively GB/T4802.2-1997 and GB/T5455-1997, and result is as follows.
? Embodiment 1 Embodiment 2 Embodiment 3
ANTIPILLING grade 5 grades 4 grades 5 grades
Flame retardant rating B1 level B1 level B1 level
The clothes of 80% acrylic fibers content is after finishing agent arranges, and its anti-pilling property and fire resistance are all higher, have good technique effect, can be in the arrangement of acrylic fabric.

Claims (5)

1. an acrylic fabric finishing agent, is characterized in that acrylic fabric finishing agent is comprised of according to weight ratio following composition: sodium hexadecyl sulfate is that 9~12 parts, alkyl diphenyl ether disulphonic acid sodium are that 4~5 parts, sodium laurate are that 6~9 parts, calcium chloride are that 3~4 parts, tributyl phosphate are that 5~9 parts, tryptophan are that 1~2 part, glycerine are that 22~26 parts, water are 210~220 parts.
2. the preparation method of a kind of acrylic fabric finishing agent according to claim 1, it is characterized in that preparation method comprises the following steps: under (1) room temperature, getting sodium hexadecyl sulfate and be 9~12 parts, alkyl diphenyl ether disulphonic acid sodium and be 4~5 parts, sodium laurate and be 6~9 parts, water is 210~220 parts, and sodium hexadecyl sulfate, alkyl diphenyl ether disulphonic acid sodium, sodium laurate water are uniformly dissolved as mixed solution; (2) to adding tributyl phosphate in mixed solution, be that 5~9 parts, tryptophan are that 1~2 part, glycerine are 22~26 parts again, be uniformly dissolved after being heated to 55 ℃; (3) getting calcium chloride is 3~4 parts, and calcium chloride is pulverized as powder, and powder order number is 250 order~350 orders; (4) calcium chloride powder is joined in mixed solution, after stirring, prepare acrylic fabric finishing agent.
3. the preparation method of a kind of acrylic fabric finishing agent according to claim 2, the sodium hexadecyl sulfate adding while it is characterized in that preparing is 12 parts.
4. the preparation method of a kind of acrylic fabric finishing agent according to claim 2, the sodium laurate adding while it is characterized in that preparing is 9 parts.
5. the preparation method of a kind of acrylic fabric finishing agent according to claim 2, the calcium chloride powder adding while it is characterized in that preparing is 3 parts.
CN201310749092.9A 2013-12-31 2013-12-31 A kind of acrylic fibers material treatment agent and its preparation method Active CN103741461B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104452280A (en) * 2014-12-24 2015-03-25 湖州市菱湖重兆金辉丝织厂 Preparation method of novel flame-retardant antibacterial acrylic fabric
CN107938353A (en) * 2017-11-30 2018-04-20 英泰时尚服饰(苏州)有限公司 A kind of acrylic fabric and its soft fire-retardant composite finishing method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1737245A (en) * 2004-08-19 2006-02-22 中国石化上海石油化工股份有限公司 Finishing agent for reducing balling-up property of acrylic fibre
CN101654864A (en) * 2009-09-25 2010-02-24 厦门大学 Fire-retardant polypropylene non-woven fabric and preparation method thereof
CN102319499A (en) * 2011-07-19 2012-01-18 南京理工大学 Built-up synergetic class-A/B water extinguishing agent series
CN103114449A (en) * 2012-11-08 2013-05-22 吴江市钱氏纺织有限公司 Antistatic finishing agent for wool and wool blended fabrics and preparation method thereof
CN103170082A (en) * 2011-12-20 2013-06-26 陕西坚瑞消防股份有限公司 Fire-extinguishing composition containing amino acid compounds
CN103437182A (en) * 2013-09-02 2013-12-11 徐文 Improved fireproof flame retardant for textiles

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1737245A (en) * 2004-08-19 2006-02-22 中国石化上海石油化工股份有限公司 Finishing agent for reducing balling-up property of acrylic fibre
CN101654864A (en) * 2009-09-25 2010-02-24 厦门大学 Fire-retardant polypropylene non-woven fabric and preparation method thereof
CN102319499A (en) * 2011-07-19 2012-01-18 南京理工大学 Built-up synergetic class-A/B water extinguishing agent series
CN103170082A (en) * 2011-12-20 2013-06-26 陕西坚瑞消防股份有限公司 Fire-extinguishing composition containing amino acid compounds
CN103114449A (en) * 2012-11-08 2013-05-22 吴江市钱氏纺织有限公司 Antistatic finishing agent for wool and wool blended fabrics and preparation method thereof
CN103437182A (en) * 2013-09-02 2013-12-11 徐文 Improved fireproof flame retardant for textiles

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
曹堃等: "腈纶阻燃研究进展", 《腈纶阻燃研究进展》, vol. 24, no. 9, 30 September 2008 (2008-09-30), pages 1 - 5 *
潘国辉: "织物抗起毛起球新技术现状分析", 《科技信息》, no. 27, 30 September 2011 (2011-09-30), pages 418 - 419 *
秦泗霞等: "纺织品抗起球测试及常见起球原因分析", 《轻纺工业与技术》, vol. 41, no. 2, 30 April 2012 (2012-04-30), pages 23 - 25 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104452280A (en) * 2014-12-24 2015-03-25 湖州市菱湖重兆金辉丝织厂 Preparation method of novel flame-retardant antibacterial acrylic fabric
CN107938353A (en) * 2017-11-30 2018-04-20 英泰时尚服饰(苏州)有限公司 A kind of acrylic fabric and its soft fire-retardant composite finishing method

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Address after: 215200 group 5, Qizhuang village, Shengze Town, Wujiang District, Suzhou City, Jiangsu Province

Patentee after: JIANGSU HUACHAO TEXTILE INDUSTRIAL CO., LTD.

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