CN103757890B - A kind of western-style clothes finishing agent and preparation method thereof - Google Patents
A kind of western-style clothes finishing agent and preparation method thereof Download PDFInfo
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- CN103757890B CN103757890B CN201310751659.6A CN201310751659A CN103757890B CN 103757890 B CN103757890 B CN 103757890B CN 201310751659 A CN201310751659 A CN 201310751659A CN 103757890 B CN103757890 B CN 103757890B
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Abstract
A kind of western-style clothes finishing agent and preparation method thereof, western-style clothes finishing agent is made up of according to weight ratio following composition: ethyoxyl aminopropyl dimethyl silicone polymer is 4 ~ 6 parts, ammonium dihydrogen phosphate (ADP) is 2 ~ 4 parts, calcium monohydrogen phosphate is 3 ~ 5 parts, sodium carboxymethylcellulose is 7 ~ 9 parts, mannosan is 5 ~ 6 parts, OPEO is 3 ~ 5 parts, ethanol is 35 ~ 55 parts, water is 210 ~ 220 parts.Carry out the heating of finishing agent composition by regulating after temperature, the step such as mixer carries out stirring, inflated with nitrogen, the refusing water, refuse oil of the western-style clothes finishing agent prepared, anti-wrinkle effect are better, western-style clothes can be allowed to possess and refuse water, refuse oil, crease-resistant performance.
Description
Technical field
The present invention relates to a kind of possess refuse water, refuse oil, the finishing agent of crease-resistant character and preparation method thereof, particularly relate to a kind of possess refuse water, refuse oil, the western-style clothes finishing agent of crease-resistant character and preparation method thereof.
Background technology
Western-style clothes is a kind of clothes that business people needs often dress.Western-style clothes material mostly is cotton, hair and silk etc.Western-style clothes is in wearing process, and water repellency, oil repellent energy, wrinkle resistance have important effect to it.Conventional Western-style clothes is after repeatedly wearing, and Western-style clothes there will be fold, affects the attractive in appearance of Western-style clothes.If when attending the dinner, when having oily matter to fall on Western-style clothes, the performance of oil refused by common Western-style clothes owing to not having, oily matter just can be adsorbed on western-style clothes, not easily removes.Aqueous substance drops and does not have on the western-style clothes of waterproofing function, makes troubles also can to the work of people.Therefore, be necessary to develop a kind of finishing agent, improve the wrinkle resistance of western-style clothes, water repellency, oil repellent energy.
Summary of the invention
The technical problem solved: common western-style clothes fold after repeatedly wearing is more, common western-style clothes is refused water and is refused the problem of oily poor-performing simultaneously.
Technical scheme: the invention discloses a kind of western-style clothes finishing agent and preparation method thereof, western-style clothes finishing agent is made up of according to weight ratio following composition: ethyoxyl aminopropyl dimethyl silicone polymer is 4 ~ 6 parts, ammonium dihydrogen phosphate (ADP) is 2 ~ 4 parts, calcium monohydrogen phosphate is 3 ~ 5 parts, sodium carboxymethylcellulose is 7 ~ 9 parts, mannosan is 5 ~ 6 parts, OPEO is 3 ~ 5 parts, ethanol is 35 ~ 55 parts, water is 210 ~ 220 parts.
A preparation method for western-style clothes finishing agent, preparation method comprises the following steps: (1) gets airtight reactor, temperature of reaction kettle is set as 66 DEG C ~ 70 DEG C; (2) airtight reactor is opened, in reactor, add that water is 210 ~ 220 parts, ethanol is 35 ~ 55 parts, ammonium dihydrogen phosphate (ADP) is 2 ~ 4 parts, calcium monohydrogen phosphate is 3 ~ 5 parts, sodium carboxymethylcellulose is 7 ~ 9 parts, stir with mixer, speed of agitator is 200r/min; (3) in reactor, add after stirring that ethyoxyl aminopropyl dimethyl silicone polymer is 4 ~ 6 parts, mannosan is 5 ~ 6 parts, OPEO is 3 ~ 5 parts again, stir with mixer, speed of agitator is 150r/min, stirs; (4) loaded in storage bucket by the finishing agent after stirring, after being filled with nitrogen, sealing is preserved.
The sodium carboxymethylcellulose added during preparation is preferably 9 parts.The calcium monohydrogen phosphate added during preparation is preferably 4 ~ 5 parts.The OPEO added during preparation is preferably 3 ~ 4 parts.
beneficial effect:cotton western-style clothes is after arranging through finishing agent of the present invention, and refusing water grade is 5 grades, and refuse wet goods level and be 6 to 7 grades, cotton western-style clothes also has good wrinkle resistance.
Detailed description of the invention
Embodiment 1
(1) get airtight reactor, temperature of reaction kettle is set as 70 DEG C; (2) open airtight reactor, add that water is 210kg, ethanol is 55kg, ammonium dihydrogen phosphate (ADP) is 4kg, calcium monohydrogen phosphate is 3kg, sodium carboxymethylcellulose is 9kg in reactor, stir with mixer, speed of agitator is 200r/min; (3) in reactor, add after stirring that ethyoxyl aminopropyl dimethyl silicone polymer is 4kg, mannosan is 6kg, OPEO is 3kg again, stir with mixer, speed of agitator is 150r/min, stirs; (4) loaded in storage bucket by the finishing agent after stirring, after being filled with nitrogen, sealing is preserved.
Embodiment 2
(1) get airtight reactor, temperature of reaction kettle is set as 66 DEG C; (2) open airtight reactor, add that water is 215kg, ethanol is 35kg, ammonium dihydrogen phosphate (ADP) is 3kg, calcium monohydrogen phosphate is 5kg, sodium carboxymethylcellulose is 7kg in reactor, stir with mixer, speed of agitator is 200r/min; (3) in reactor, add after stirring that ethyoxyl aminopropyl dimethyl silicone polymer is 5kg, mannosan is 5kg, OPEO is 4kg again, stir with mixer, speed of agitator is 150r/min, stirs; (4) loaded in storage bucket by the finishing agent after stirring, after being filled with nitrogen, sealing is preserved.
Embodiment 3
(1) get airtight reactor, temperature of reaction kettle is set as 68 DEG C; (2) open airtight reactor, add that water is 220kg, ethanol is 45kg, ammonium dihydrogen phosphate (ADP) is 2kg, calcium monohydrogen phosphate is 4kg, sodium carboxymethylcellulose is 8kg in reactor, stir with mixer, speed of agitator is 200r/min; (3) in reactor, add after stirring that ethyoxyl aminopropyl dimethyl silicone polymer is 6kg, mannosan is 6kg, OPEO is 5kg again, stir with mixer, speed of agitator is 150r/min, stirs; (4) loaded in storage bucket by the finishing agent after stirring, after being filled with nitrogen, sealing is preserved.
Soak 1h by the finishing agent being dipped into embodiment 1, embodiment 2, embodiment 3 under cotton western-style clothes room temperature, after a leaching one is rolled, pick-up is 65%, dries at 95 DEG C.Refusing water, refusing oily measure of merit standard is AATCC22-2010, AATCC118, and result is as following table.
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Refuse water grade | 5 grades | 5 grades | 5 grades |
| Refuse wet goods level | 7 grades | 7 grades | 6 grades |
| Anti-wrinkle effect | Fold is not had after wearing 5 times | Fold is not had after wearing 3 times | Fold is not had after wearing 4 times |
Western-style clothes after finishing agent of the present invention arranges, has good water repellency and oil repellent energy, also has good anti-wrinkle effect simultaneously.
Claims (4)
1. a western-style clothes finishing agent, is characterized in that western-style clothes finishing agent is made up of according to weight ratio following composition: ethyoxyl aminopropyl dimethyl silicone polymer is 4 ~ 6 parts, ammonium dihydrogen phosphate (ADP) is 2 ~ 4 parts, calcium monohydrogen phosphate is 3 ~ 5 parts, sodium carboxymethylcellulose is 7 ~ 9 parts, mannosan is 5 ~ 6 parts, OPEO is 3 ~ 5 parts, ethanol is 35 ~ 55 parts, water is 210 ~ 220 parts;
The preparation method of described a kind of western-style clothes finishing agent, comprises the following steps: (1) gets airtight reactor, temperature of reaction kettle is set as 66 DEG C ~ 70 DEG C; (2) airtight reactor is opened, in reactor, add that water is 210 ~ 220 parts, ethanol is 35 ~ 55 parts, ammonium dihydrogen phosphate (ADP) is 2 ~ 4 parts, calcium monohydrogen phosphate is 3 ~ 5 parts, sodium carboxymethylcellulose is 7 ~ 9 parts, stir with mixer, speed of agitator is 200r/min; (3) in reactor, add after stirring that ethyoxyl aminopropyl dimethyl silicone polymer is 4 ~ 6 parts, mannosan is 5 ~ 6 parts, OPEO is 3 ~ 5 parts again, stir with mixer, speed of agitator is 150r/min, stirs; (4) loaded in storage bucket by the finishing agent after stirring, after being filled with nitrogen, sealing is preserved.
2. a kind of western-style clothes finishing agent according to claim 1, is characterized in that the sodium carboxymethylcellulose added when preparing is 9 parts.
3. a kind of western-style clothes finishing agent according to claim 1, is characterized in that the calcium monohydrogen phosphate added when preparing is 4 ~ 5 parts.
4. a kind of western-style clothes finishing agent according to claim 1, is characterized in that the OPEO added when preparing is 3 ~ 4 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310751659.6A CN103757890B (en) | 2013-12-31 | 2013-12-31 | A kind of western-style clothes finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310751659.6A CN103757890B (en) | 2013-12-31 | 2013-12-31 | A kind of western-style clothes finishing agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
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| CN103757890A CN103757890A (en) | 2014-04-30 |
| CN103757890B true CN103757890B (en) | 2015-12-09 |
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| CN201310751659.6A Expired - Fee Related CN103757890B (en) | 2013-12-31 | 2013-12-31 | A kind of western-style clothes finishing agent and preparation method thereof |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104452292A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of silk-like fabric |
| CN105297403A (en) * | 2015-12-07 | 2016-02-03 | 苏州庄爵服饰有限公司 | Finishing method of anti-wrinkle fabric |
| CN105648769B (en) * | 2016-04-01 | 2017-11-21 | 吴江市林旺纺织厂 | A kind of preparation method of waterproof oil resistant type finishing agent |
| CN106319971A (en) * | 2016-08-19 | 2017-01-11 | 常熟市龙飞针纺织有限公司 | After-finishing process for polar fleece fabrics |
| CN106319952A (en) * | 2016-08-19 | 2017-01-11 | 常熟市鑫博伟针纺织有限公司 | After-finishing process of brushed fabric |
| CN107747226A (en) * | 2017-11-30 | 2018-03-02 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of dress ornament antibacterial finish agent |
| CN108004763A (en) * | 2017-11-30 | 2018-05-08 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of the moisture-proof looped fabric of insect prevention |
| CN112391839B (en) * | 2020-11-18 | 2023-01-24 | 湖南派意特服饰有限公司 | Western-style clothes finishing agent and preparation method thereof |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2772608B2 (en) * | 1993-04-08 | 1998-07-02 | ライオン株式会社 | Spray type water / oil repellent composition |
| CN101326321A (en) * | 2005-12-12 | 2008-12-17 | 美利肯公司 | Stain repellant and release fabric conditioner |
| CN101760967A (en) * | 2008-11-14 | 2010-06-30 | 杨玉生 | Waterproof and oilproof finishing agent for fabric and leather and preparation thereof |
| CN101435160B (en) * | 2008-12-18 | 2010-12-15 | 浙江闰土股份有限公司 | Organosilicon fluorine multifunctional fabric finishing agent and preparing method thereof |
| CN103469585A (en) * | 2013-08-21 | 2013-12-25 | 昆山铁牛衬衫厂 | Finishing agent for water and oil proofing of fabric |
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| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Luo Wenliang Inventor after: Zhou Fenghua Inventor after: Tan Xiangyu Inventor after: Liu Jianlan Inventor after: Wen Ming Inventor after: Huang Jieying Inventor after: Tan Jinan Inventor after: Deng Hongmei Inventor after: Zhou Chongen Inventor after: Lai Qionghua Inventor after: Deng Bo Inventor after: Lu Guangfeng Inventor after: Pang Jianying Inventor after: Long Yuansheng Inventor before: Zhang Dexuan |
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Effective date of registration: 20151026 Address after: 410699, No. 016, Jinzhou Avenue, Jinzhou new district, Ningxiang County, Changsha, Hunan Applicant after: Hunan Dongfang Fashion Co., Ltd. Address before: 7 groups of friendship village Songling town of Wujiang District of Suzhou City, Jiangsu province 215200 split eight community Applicant before: SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY CO., LTD. |
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