CN104562686B - Waterproofing agent used for textiles that a kind of persistency is good and preparation method - Google Patents
Waterproofing agent used for textiles that a kind of persistency is good and preparation method Download PDFInfo
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- CN104562686B CN104562686B CN201510054121.9A CN201510054121A CN104562686B CN 104562686 B CN104562686 B CN 104562686B CN 201510054121 A CN201510054121 A CN 201510054121A CN 104562686 B CN104562686 B CN 104562686B
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Abstract
The waterproofing agent used for textiles that a kind of persistency is good, including the component of following mass parts: polyvinyl alcohol 15～20, epoxychloropropane 15～18, soap powder 10～14, fatty acid receives 8～12, acetic acid 5～10, ethanol 25～30, Colophonium 5～10, methylcellulose 2～3.The preparation method of the present invention is, weighs needed raw material, is placed in ethanol by Colophonium, is heated to 40～50 DEG C, stirs；In above-mentioned solution, insulation is sequentially added into acetic acid, soap powder, fatty acid are received, epoxy ethyl chloride, methylcellulose and polyvinyl alcohol, is uniformly mixed, be cooled to room temperature both finished product.The fabric waterproofing agent preparation technology of the present invention is simple, and raw material is easy to get, and production cost is low, impervious good seepage-proof property；Fabric after process is water-fastness and dry-cleans, and persistency is good；The fabric waterproofing agent of the present invention also has safe and harmless feature.
Description
Technical field
The present invention relates to waterproofing agent field used for textiles, be specifically related to good the spinning of a kind of persistency
Fabric waterproofing agent and preparation method thereof.
Background technology
Along with the raising of people's living standard, the requirement to properties of textile is more and more higher, not
Water-proof function is not possessed through the normal laundry of water-proofing treatment, after water suction, absorbing sweat, moisture penetration
Affect the outward appearance of fabric and the comfortableness of dress to fabric back, limit it at daily life
And the use under special weather.
The fabric waterproofing agent used the earliest in China is Oleum Verniciae fordii, and it is coated on articles for use and fabric,
Formation oiliness epithelium is in order to waterproof, and along with the development in epoch, fabric waterproofing agent is gradually by core of Caulis et Folium Lini
The functions such as the drier oils such as oil, Fructus Perillae oil and half drier oil, boiled oil, dry accelerator are preferably mixed
Join thing to substitute.Its water proofing property is excellent, and color is light, soft, once extensively applies for many years,
But after using alkalescence synthetic detergent washing, water resistance declines serious, makes the water proofing property of waterproofing agent
Limited to washing fastness.
Summary of the invention
Not enough for prior art, the invention provides the fabric waterproofing agent that a kind of persistency is good
And preparation method thereof, waterproofing agent prepared by the method has preferable water resistance and wash resistant
Property.
The present invention solves the technical scheme of above-mentioned technical problem employing: a kind of persistency is good
Waterproofing agent used for textiles, including the component of following mass parts: polyvinyl alcohol 15～20, epoxy chlorine
Propane 15～18, soap powder 10～14, fatty acid receives 8～12, acetic acid 5～10, ethanol 25～30,
Colophonium 5～10, methylcellulose 2～3.
The preparation method of the waterproofing agent used for textiles that described a kind of persistency is good includes walking as follows
Rapid:
A. needed raw material is weighed by above-mentioned mass parts；
B. Colophonium is placed in ethanol, is heated to 40～50 DEG C, stirs；
C. in above-mentioned solution, insulation is sequentially added into acetic acid, soap powder, fatty acid are received, epoxy
Ethyl chloride, methylcellulose and polyvinyl alcohol, be uniformly mixed, and is cooled to room temperature
Both finished product had been obtained.
Compared with prior art, present invention have the advantage that waterproofing agent preparation technology is simple,
Raw material is easy to get, and production cost is low；This waterproofing agent is used to process fabric, the most impervious anti-seepage effect
Preferably, and fabric possesses stronger flexibility；Fabric after process is water-fastness and dry-cleans, and holds
Property is good for a long time；The fabric waterproofing agent of the present invention also has safe and harmless feature.
Detailed description of the invention
Embodiment 1: the waterproofing agent used for textiles that a kind of persistency is good, including following mass parts
Component: polyvinyl alcohol 15, epoxychloropropane 15, soap powder 10, fatty acid receives 8, acetic acid 5,
Ethanol 25, Colophonium 5, methylcellulose 2.
Embodiment 2: the waterproofing agent used for textiles that a kind of persistency is good, including following mass parts
Component: polyvinyl alcohol 20, epoxychloropropane 18, soap powder 14, fatty acid receives 12, acetic acid 10,
Ethanol 30, Colophonium 10, methylcellulose 3.
Embodiment 3: the waterproofing agent used for textiles that a kind of persistency is good, including following mass parts
Component: polyvinyl alcohol 18, epoxychloropropane 16, soap powder 12, fatty acid receives 10, acetic acid
8, ethanol 28, Colophonium 8, methylcellulose 2.5.
Embodiment 4: the waterproofing agent used for textiles that a kind of persistency is good, including following mass parts
Component: polyvinyl alcohol 15, epoxychloropropane 18, soap powder 12, fatty acid receives 12, acetic acid
5, ethanol 30, Colophonium 5, methylcellulose 2.
The preparation method of above example is: weigh needed raw material by the mass parts in embodiment；
Colophonium is placed in ethanol, is heated to 40～50 DEG C, stirs；It is incubated in above-mentioned solution
Be sequentially added into acetic acid, soap powder, fatty acid are received, epoxy ethyl chloride, methylcellulose and polyethylene
Alcohol, is uniformly mixed, and is cooled to room temperature and had both obtained finished product.
In order to verify the waterproof effect of textile after waterproofing agent of the present invention processes, can pass through
The standard method of GB GB 4,745 1997 is investigated, in order to compare, and following table is embodiment
The test result of 1～4.
| Numbering | Waterproof effect | Waterproof effect after washing 10 times |
| Embodiment 1 | 5 | 5- |
| Embodiment 2 | 5- | 4+ |
| Embodiment 3 | 5 | 5 |
| Embodiment 4 | 5 | 5- |
This test evaluation criteria is up to 5 grades, i.e. waterproof effect is excellent.Tie from the test of upper table
Fruit can draw, the waterproofing agent of the present invention has preferable water proofing property and persistency.
It should be pointed out that, above example is only the better embodiment of the present invention, for this
Those skilled in the art, without departing from the inventive concept of the premise, are made some changing
Become, improvements and modifications also should be regarded as protection scope of the present invention.
Claims (5)
1. the waterproofing agent used for textiles that a persistency is good, it is characterised in that: include following
The component of mass parts:
Polyvinyl alcohol 15～20
Epoxychloropropane 15～18
Soap powder 10～14
Sodium soap 8～12
Acetic acid 5～10
Ethanol 25～30
Colophonium 5～10
Methylcellulose 2～3；
The good waterproofing agent used for textiles of described a kind of persistency is by following preparation method
Prepare:
Needed raw material is weighed by above-mentioned mass parts；
Colophonium is placed in ethanol, is heated to 40～50 DEG C, stirs；
In above-mentioned solution insulation be sequentially added into acetic acid, soap powder, sodium soap, epoxychloropropane,
Methylcellulose and polyvinyl alcohol, be uniformly mixed, and is cooled to room temperature and had both obtained finished product.
The waterproofing agent used for textiles that a kind of persistency the most according to claim 1 is good,
It is characterized in that: include the component of following mass parts: polyvinyl alcohol 15, epoxychloropropane 15,
Soap powder 10, sodium soap 8, acetic acid 5, ethanol 25, Colophonium 5, methylcellulose 2.
The waterproofing agent used for textiles that a kind of persistency the most according to claim 1 is good,
It is characterized in that: include the component of following mass parts: polyvinyl alcohol 20, epoxychloropropane 18,
Soap powder 14, sodium soap 12, acetic acid 10, ethanol 30, Colophonium 10, methylcellulose 3.
The waterproofing agent used for textiles that a kind of persistency the most according to claim 1 is good,
It is characterized in that: include the component of following mass parts: polyvinyl alcohol 18, epoxychloropropane 16,
Soap powder 12, sodium soap 10, acetic acid 8, ethanol 28, Colophonium 8, methylcellulose 2.5.
The waterproofing agent used for textiles that a kind of persistency the most according to claim 1 is good,
It is characterized in that: include the component of following mass parts: polyvinyl alcohol 15, epoxychloropropane 18,
Soap powder 12, sodium soap 12, acetic acid 5, ethanol 30, Colophonium 5, methylcellulose 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510054121.9A CN104562686B (en) | 2015-02-02 | 2015-02-02 | Waterproofing agent used for textiles that a kind of persistency is good and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510054121.9A CN104562686B (en) | 2015-02-02 | 2015-02-02 | Waterproofing agent used for textiles that a kind of persistency is good and preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104562686A CN104562686A (en) | 2015-04-29 |
| CN104562686B true CN104562686B (en) | 2017-01-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510054121.9A Active CN104562686B (en) | 2015-02-02 | 2015-02-02 | Waterproofing agent used for textiles that a kind of persistency is good and preparation method |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106087425A (en) * | 2016-07-18 | 2016-11-09 | 南通富之岛寝具发展有限公司 | A kind of waterproofing agent used for textiles and preparation method thereof |
| CN111139650A (en) * | 2020-03-03 | 2020-05-12 | 南通天梭纺织有限公司 | Preparation process of waterproof textile fabric |
| CN112323479A (en) * | 2020-10-29 | 2021-02-05 | 长兴卓恒新材料科技有限公司 | Preparation method of environment-friendly nano waterproof agent for textiles |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB882892A (en) * | 1957-09-16 | 1961-11-22 | Raduner & Co Ag | Process of producing foldable, highly water-resistant, stiffened sheet material of very high dimensional stability which can be printed by means of lithographic printing methods |
| GB1116150A (en) * | 1966-02-21 | 1968-06-06 | Procter & Gamble | Amine-epichlorhydrin reaction products and compositions containing same for use in the treatment of textiles |
| CN103243550A (en) * | 2013-05-16 | 2013-08-14 | 湖州厉华妤婕联合纺织有限公司 | Fabric waterproof agent |
| CN104047172A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | Long-acting waterproof agent for textiles |
| CN104047166A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | Environment-friendly long-acting weaving waterproof agent |
-
2015
- 2015-02-02 CN CN201510054121.9A patent/CN104562686B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB882892A (en) * | 1957-09-16 | 1961-11-22 | Raduner & Co Ag | Process of producing foldable, highly water-resistant, stiffened sheet material of very high dimensional stability which can be printed by means of lithographic printing methods |
| GB1116150A (en) * | 1966-02-21 | 1968-06-06 | Procter & Gamble | Amine-epichlorhydrin reaction products and compositions containing same for use in the treatment of textiles |
| CN103243550A (en) * | 2013-05-16 | 2013-08-14 | 湖州厉华妤婕联合纺织有限公司 | Fabric waterproof agent |
| CN104047172A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | Long-acting waterproof agent for textiles |
| CN104047166A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | Environment-friendly long-acting weaving waterproof agent |
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| CN104562686A (en) | 2015-04-29 |
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