CN103752035A - Extracting device - Google Patents

Extracting device Download PDF

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Publication number
CN103752035A
CN103752035A CN201310741123.6A CN201310741123A CN103752035A CN 103752035 A CN103752035 A CN 103752035A CN 201310741123 A CN201310741123 A CN 201310741123A CN 103752035 A CN103752035 A CN 103752035A
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flabellum
staving
transport vehicle
bung
extraction equipment
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CN201310741123.6A
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CN103752035B (en
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傅宏征
张云新
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Abstract

The invention relates to a chemical reagent and traditional Chinese medicine reagent preparation device and particularly relates to a large-scale and automatic extracting device. The invention aims to provide the extracting device which is simple to operate, can protect experimenters and is suitable for a plurality of extracting solutions. According to the extracting device, a barrel body and a discharging valve are used for replacing a separating funnel in a laboratory, and the barrel body and an electric heating wire are used for replacing a beaker and an alcohol lamp; a spiral blade is used for replacing a glass rod and an ultrasonic generator is mounted, so that complicated chemical experiment equipment is integrated; the extracting device is convenient to use and simple and convenient to operate; the trouble of repeatedly replacing the chemical experiment equipment in the process of preparing the plurality of extracting solutions is omitted and the extracting device is suitable for large-quantity extraction. According to the extracting device, a barrel cover is arranged so as to prevent the solutions from being sprayed out due to boiling and the safety of the experimenters is protected.

Description

Extraction equipment
Technical field
The present invention relates to a kind of chemical reagent, Chinese medicine reagent preparation equipment, particularly relate to a kind of for extensive, automatization abstraction device.
Background technology
Extraction, claims again solvent extraction or liquid-liquid extraction, also claims extracting, is to utilize component in system in solvent, to have different solubility to carry out the unit operations of separating mixture.The difference of utilizing compound solubility or distribution coefficient in the solvent of two kinds immiscible (or slightly soluble, emulsification), makes compound in a kind of solvent, transfer to the method another solvent.
Chemical experiment often adopts emulsified solution heating or/and add different material in hyperacoustic method layering extraction solution in extraction process, common R&D institution and laboratory often adopt the experiment appliances such as small-sized beaker, graduated cylinder to operate, but the preparation for a large amount of extractants is difficult for producing, and operating process is complicated, also need artificial guard, increased the possibility that experimenter is endangered by chemical preparation product.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of simple to operate, Protection personnel, is applicable to the extraction equipment of a large amount of extraction solutions.
Extraction equipment of the present invention, comprises staving, bung and motor.Described staving opening part seals by bung.On described bung, be fixed with motor.The output of described motor is fixed by shaft coupling and flabellum bar.Described flabellum bar periphery is fixed with spiral fan.Described spiral fan is positioned at staving.Described staving periphery is provided with a barrel shell, asbestos layer, heating wire and bucket inner bag from outside to inside successively.Described staving bottom surface is provided with a barrel shell, supersonic generator and bucket inner bag from outside to inside successively, and staving bottom surface is provided with discharging opening.Described discharging opening and discharge nozzle are tightly connected.Described discharge nozzle is provided with outlet valve.
Extraction equipment of the present invention, wherein said staving opening part is provided with buckle, and staving is fixing by buckle and bung sealing.Described buckle comprises buckle handle, card, screw rod, locking spring, nut shaft and buckle connecting rod.Under described buckle handle, be fixed with screw rod.Described screw rod coordinates with the via clearance at card middle part, and screw rod bottom is threaded with nut shaft.The periphery of described nut shaft is provided with screwed hole, and screw rod is by nut shaft and buckle connecting rod one end chain connection.The described buckle connecting rod other end is fixedly connected with staving, is provided with locking spring between buckle connecting rod and card.Described locking spring housing is contained on the periphery of screw rod.Described bung is provided with and covers flange.Described card is provided with and the draw-in groove that covers flange and match.
Extraction equipment of the present invention, wherein said bung and flabellum bar is rotatable is tightly connected.Described bung upper surface is provided with inlet valve, air bleeding valve, peephole and safety valve.
Extraction equipment of the present invention, wherein said spiral fan comprises flabellum, middle flabellum and lower flabellum.Described upper flabellum, middle flabellum are identical with the shape and structure of lower flabellum, and upper flabellum, middle flabellum and lower flabellum are fixed on the periphery of flabellum bar from top to bottom successively, and the flabellum of spiral fan and the angle of horizontal plane are 1-89 °.
Extraction equipment of the present invention, wherein also comprises transport vehicle.Also comprise transport vehicle.On described transport vehicle, be fixed with staving, transport vehicle is provided with transport vehicle discharge opening.Described transport vehicle discharge opening and discharge nozzle matched in clearance, transport vehicle upper surface is provided with platform table, and the transportation guide wheel of transport vehicle is provided with brake apparatus, and transport vehicle is provided with transport vehicle handle.
Extraction equipment of the present invention, wherein said staving bottom surface is provided with temperature sensor.Described temperature sensor is connected with electronic controller.Described electronic controller is connected with heating wire, and electronic controller is connected with contact panel.Described contact panel is positioned at transport vehicle front end face.
Extraction equipment of the present invention, wherein said staving bottom surface is provided with ultrasonic sensor.Described ultrasonic sensor is connected with electronic controller.Described electronic controller is connected with supersonic generator, and electronic controller is connected with contact panel.
Extraction equipment of the present invention, wherein said bung is fixedly connected with motor by covering projection.Described lid projection is positioned at bung middle part, in lid projection, is provided with flabellum bar, and lid projection is provided with peep hole.
Extraction equipment of the present invention, wherein said staving periphery is provided with water level peep hole.
Extraction equipment difference from prior art of the present invention is that extraction equipment of the present invention replaces the separatory funnel in laboratory by staving and outlet valve, by staving and heating wire, replace beaker and alcolhol burner, by spiral fan, replace glass bar, and installation supersonic generator, thereby complicated equipment of chemical industry is rolled into one, make it easy to use, easy and simple to handle, and saved the trouble of repeatedly changing equipment of chemical industry in the process of preparing a large amount of extraction solutions, be applicable to a large amount of extractions.The present invention can avoid solution because of outwards splash of boiling, Protection personnel's safety by bung.
In extraction equipment of the present invention, by the locking spring on buckle, can guarantee the self-locking performance of buckle.And buckle and staving chain connection, the situation that can avoid buckle to lose.The present invention, by be provided with inlet valve and outlet valve on bung, need not open bung and just can in staving, pour chemical solution into.Peephole can facilitate experimenter to observing in staving.Safety valve can be avoided the blast situation of the excessive initiation of staving pressure.The present invention is by upper flabellum, middle flabellum and lower flabellum agitating solution more fully.The present invention can clearly measure temperature and the ultrasonic intensity in bucket by temperature sensor and ultrasonic sensor, and utilizes contact panel display measurement data and control heating wire and supersonic generator.The present invention can clearly learn by building protruding peep hole whether flabellum bar rotates, thereby learns whether spiral fan rotates.The present invention is provided with water level peep hole by staving periphery, can clearly learn the volume of pouring solution into.The present invention is by the platform desktop on transport vehicle, facilitate scientific research personnel for the record of data and put experimental article, pass through brake apparatus, the displacement of having avoided transport vehicle to produce because of processes such as self vibration, screws in the course of the work, can facilitate transporting of transport vehicle by transport vehicle handle.
Below in conjunction with accompanying drawing, extraction equipment of the present invention is described further.
Accompanying drawing explanation
Fig. 1 is the axonometric drawing of extraction equipment;
Fig. 2 is the partial enlarged drawing at the bung of extraction equipment shown in Fig. 1 place;
Fig. 3 is the partial enlarged drawing of buckle in Fig. 2;
Fig. 4 is the partial sectional view of staving in Fig. 1.
The specific embodiment
As Figure 1-Figure 4, extraction equipment of the present invention comprises transport vehicle 1, staving 2, bung 3 and motor 4.Described transport vehicle 1 upper surface is provided with platform table 13, and the transportation guide wheel 14 of transport vehicle 1 is provided with brake apparatus, and transport vehicle 1 is provided with transport vehicle handle 12.On transport vehicle 1, be fixed with staving 2.Described staving 2 opening parts are provided with buckle 22.
As shown in Figure 3, buckle 22 of the present invention comprises buckle handle 221, card 222, screw rod 223, locking spring 224, nut shaft 225 and buckle connecting rod 226.Described buckle handle is fixed with screw rod 223 221 times.Described screw rod 223 coordinates with the via clearance at card 222 middle parts, and screw rod 223 bottoms are threaded with nut shaft 225.The periphery of described nut shaft 225 is provided with screwed hole, and screw rod 223 is by nut shaft 225 and buckle connecting rod 226 one end chain connections.Described buckle connecting rod 226 other ends are fixedly connected with staving 2, are provided with locking spring 224 between buckle connecting rod 226 and card 222.Described locking spring 224 is sleeved on the periphery of screw rod 223.Described bung 3 is provided with and covers flange 30.Described card 222 is provided with and the draw-in groove 2221 that covers flange 30 and match.Staving 2 is fixing with bung 3 sealings by buckle 22.
As shown in Figure 2, bung 3 of the present invention is tightly connected with flabellum bar 42 is rotatable.Described bung 3 upper surfaces are provided with inlet valve 31, air bleeding valve 32, peephole 33 and safety valve 34.Described inlet valve 31 is connected with the feed pipe being positioned on bung 3.Described air bleeding valve 32 is connected with the blast pipe being positioned on bung 3, when staff need to observe staving 2 inside, directly by peephole 33, just can see staving 2 inside, when staving 2 internal pressures surpass safe pressure, flame-arrester vent plug automatic spring in safety valve 34, discharges the pressure in staving 2.
As shown in Figure 1 and Figure 4, on bung 3 of the present invention, be fixed with motor 4.Described bung 3 is fixedly connected with motor 4 by covering projection 36.Described lid projection 36 is positioned at bung 3 middle parts.The output of described motor 4 is fixing by shaft coupling and flabellum bar 42, in lid projection 36, is provided with flabellum bar 42, and lid projection 36 is provided with peep hole 35.Described flabellum bar 42 peripheries are fixed with spiral fan 421.Described spiral fan 421 is positioned at staving 2.Spiral fan 421 comprises flabellum 4211, middle flabellum 4212 and lower flabellum 4213.Described upper flabellum 4211, middle flabellum 4212 are identical with the shape and structure of lower flabellum 4213, upper flabellum 4211, middle flabellum 4212 and lower flabellum 4213 are fixed on the periphery of flabellum bar 42 from top to bottom successively, and the flabellum of spiral fan 421 and the angle of horizontal plane are 45 °.
As shown in Figure 4, staving 2 peripheries of the present invention are provided with barrel shell 20, asbestos layer 201, heating wire 202 and bucket inner bag 203 from outside to inside successively, and staving 2 peripheries are provided with water level peep hole 21.Described staving 2 bottom surfaces are provided with barrel shell 20, supersonic generator 204 and bucket inner bag 203 from outside to inside successively.Described staving 2 bottom surfaces are provided with temperature sensor 111.Described temperature sensor 111 is connected with electronic controller 113, and electronic controller 113 is connected with supersonic generator 204 with heating wire 202, and electronic controller 113 is connected with contact panel 11.Described contact panel 11 is positioned at transport vehicle 1 front end face.Staving 2 bottom surfaces are provided with ultrasonic sensor 112.Described ultrasonic sensor 112 is connected with electronic controller 113.Described electronic controller 113 is connected with contact panel 11.Staving 2 bottom surfaces are provided with discharging opening 205.Described discharging opening 205 and discharge nozzle 206 are tightly connected.Described discharge nozzle 206 is provided with outlet valve 2061.Transport vehicle 1 is provided with transport vehicle discharge opening, transport vehicle discharge opening and discharge nozzle 206 matched in clearance.
During use, inlet valve 31 and air bleeding valve 32 are opened, utilized funnel will treat that extraction solution pours in staving 2.If treat, extraction solution is volatile solution or poisonous solution, can close inlet valve and air bleeding valve.And utilize contact panel starter motor 4, heating wire 202 and supersonic generator 204, the upper flabellum in flabellum bar 42, middle flabellum 4212 and lower flabellum 4213 will treat that extraction solution flows and spiral stirring from top to bottom in staving 2 central authorities.By heating, ultrasonic wave and stirring, make emulsified solution layering.By outlet valve 2061, solution extraction is gone out again.Operating process utilizes electronic controller 113 automatically to control, and without experimenter, guards.
Above-described embodiment is described the preferred embodiment of the present invention; not scope of the present invention is limited; design under the prerequisite of spirit not departing from the present invention; various distortion and improvement that those of ordinary skills make technical scheme of the present invention, all should fall in the definite protection domain of the claims in the present invention book.

Claims (9)

1. an extraction equipment, is characterized in that: comprise staving (2), bung (3) and motor (4);
Described staving (2) opening part is by bung (3) sealing, on described bung (3), be fixed with motor (4), the output of described motor (4) is fixing by shaft coupling and flabellum bar (42), described flabellum bar (42) periphery is fixed with spiral fan (421), and described spiral fan (421) is positioned at staving (2);
Described staving (2) periphery is provided with a barrel shell (20), asbestos layer (201), heating wire (202) and bucket inner bag (203) from outside to inside successively, described staving (2) bottom surface is provided with a barrel shell (20), supersonic generator (204) and bucket inner bag (203) from outside to inside successively, staving (2) bottom surface is provided with discharging opening (205), described discharging opening (205) and discharge nozzle (206) are tightly connected, and described discharge nozzle (206) is provided with outlet valve (2061).
2. extraction equipment according to claim 1, it is characterized in that: described staving (2) opening part is provided with buckle (22), staving (2) is fixing with bung (3) sealing by buckle (22), described buckle (22) comprises buckle handle (221), card (222), screw rod (223), locking spring (224), nut shaft (225) and buckle connecting rod (226), under described buckle handle (221), be fixed with screw rod (223), described screw rod (223) coordinates with the via clearance at card (222) middle part, screw rod (223) bottom is threaded with nut shaft (225), the periphery of described nut shaft (225) is provided with screwed hole, screw rod (223) is by nut shaft (225) and buckle connecting rod (226) one end chain connection, described buckle connecting rod (226) other end is fixedly connected with staving (2), between buckle connecting rod (226) and card (222), be provided with locking spring (224), described locking spring (224) is sleeved on the periphery of screw rod (223), described bung (3) is provided with and covers flange (30), described card (222) is provided with and the draw-in groove (2221) that covers flange (30) and match.
3. extraction equipment according to claim 2, it is characterized in that: described bung (3) and rotatable being tightly connected of flabellum bar (42), described bung (3) upper surface is provided with inlet valve (31), air bleeding valve (32), peephole (33) and safety valve (34).
4. extraction equipment according to claim 3, it is characterized in that: described spiral fan (421) comprises flabellum (4211), middle flabellum (4212) and lower flabellum (4213), described upper flabellum (4211), middle flabellum (4212) are identical with the shape and structure of lower flabellum (4213), upper flabellum (4211), middle flabellum (4212) and lower flabellum (4213) are fixed on the periphery of flabellum bar (42) from top to bottom successively, and the flabellum of spiral fan (421) and the angle of horizontal plane are 1-89 °.
5. extraction equipment according to claim 4, it is characterized in that: also comprise transport vehicle (1), on described transport vehicle (1), be fixed with staving (2), transport vehicle (1) is provided with transport vehicle discharge opening, described transport vehicle discharge opening and discharge nozzle (206) matched in clearance, transport vehicle (1) upper surface is provided with platform table (13), and the transportation guide wheel (14) of transport vehicle (1) is provided with brake apparatus, and transport vehicle (1) is provided with transport vehicle handle (12).
6. extraction equipment according to claim 5, it is characterized in that: described staving (2) bottom surface is provided with temperature sensor (111), described temperature sensor (111) is connected with electronic controller (113), described electronic controller (113) is connected with heating wire (202), electronic controller (113) is connected with contact panel (11), and described contact panel (11) is positioned at transport vehicle (1) front end face.
7. extraction equipment according to claim 6, it is characterized in that: described staving (2) bottom surface is provided with ultrasonic sensor (112), described ultrasonic sensor (112) is connected with electronic controller (113), described electronic controller (113) is connected with supersonic generator (204), and electronic controller (113) is connected with contact panel (11).
8. extraction equipment according to claim 7, it is characterized in that: described bung (3) is fixedly connected with motor (4) by lid projection (36), described lid projection (36) is positioned at bung (3) middle part, in lid projection (36), be provided with flabellum bar (42), lid projection (36) is provided with peep hole (35).
9. extraction equipment according to claim 8, is characterized in that: described staving (2) periphery is provided with water level peep hole (21).
CN201310741123.6A 2013-12-27 2013-12-27 Extraction equipment Active CN103752035B (en)

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CN103752035B CN103752035B (en) 2015-11-18

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106745443A (en) * 2017-01-18 2017-05-31 赵俊博 A kind of extracting process of low concentration of water sample extraction device to phenol in water quality
CN107201455A (en) * 2017-07-19 2017-09-26 赣州清亦华科科技有限公司 A kind of horizontal extraction equipment for rare earth feed liquid
CN110652954A (en) * 2019-09-19 2020-01-07 贾影丽 Cosmetics cauldron formula reaction unit
CN111100659A (en) * 2019-12-23 2020-05-05 江西理工大学 Coupling type pulverized coal gas pyrolysis reactor and use process thereof
CN111995568A (en) * 2020-09-15 2020-11-27 北京六合宁远科技有限公司 Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2340326Y (en) * 1998-07-14 1999-09-29 名晶兴业股份有限公司 Structure of clasping cooker cover with cooker body
JP2007175693A (en) * 2005-12-02 2007-07-12 Tokyo Univ Of Agriculture & Technology Separation method using amide compound
US20070158266A1 (en) * 2003-02-07 2007-07-12 Ferro Corporation Method And Apparatus For Producing Particles Via Supercritical Fluid Processing
CN201558569U (en) * 2009-08-17 2010-08-25 东莞市同道科技服务有限公司 Traditional Chinese medicinal material active ingredient extraction equipment
CN202078768U (en) * 2011-05-25 2011-12-21 姚明勤 Efficient, fast, super-strong and energy-collecting extraction device for traditional Chinese medicine
CN202654753U (en) * 2012-06-29 2013-01-09 广东顺大食品调料有限公司 Ultrasonic extraction tank

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2340326Y (en) * 1998-07-14 1999-09-29 名晶兴业股份有限公司 Structure of clasping cooker cover with cooker body
US20070158266A1 (en) * 2003-02-07 2007-07-12 Ferro Corporation Method And Apparatus For Producing Particles Via Supercritical Fluid Processing
JP2007175693A (en) * 2005-12-02 2007-07-12 Tokyo Univ Of Agriculture & Technology Separation method using amide compound
CN201558569U (en) * 2009-08-17 2010-08-25 东莞市同道科技服务有限公司 Traditional Chinese medicinal material active ingredient extraction equipment
CN202078768U (en) * 2011-05-25 2011-12-21 姚明勤 Efficient, fast, super-strong and energy-collecting extraction device for traditional Chinese medicine
CN202654753U (en) * 2012-06-29 2013-01-09 广东顺大食品调料有限公司 Ultrasonic extraction tank

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106745443A (en) * 2017-01-18 2017-05-31 赵俊博 A kind of extracting process of low concentration of water sample extraction device to phenol in water quality
CN106745443B (en) * 2017-01-18 2018-02-06 赵俊博 A kind of extracting process of low concentration of water sample extraction device to phenol in water quality
CN107201455A (en) * 2017-07-19 2017-09-26 赣州清亦华科科技有限公司 A kind of horizontal extraction equipment for rare earth feed liquid
CN110652954A (en) * 2019-09-19 2020-01-07 贾影丽 Cosmetics cauldron formula reaction unit
CN111100659A (en) * 2019-12-23 2020-05-05 江西理工大学 Coupling type pulverized coal gas pyrolysis reactor and use process thereof
CN111995568A (en) * 2020-09-15 2020-11-27 北京六合宁远科技有限公司 Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups
CN111995568B (en) * 2020-09-15 2022-04-05 北京六合宁远科技有限公司 Preparation method of poly-substituted fluorine-containing hexa-heterocyclic methylamine with protection groups

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