CN202403942U - Sampling device for synthetic reaction kettle - Google Patents
Sampling device for synthetic reaction kettle Download PDFInfo
- Publication number
- CN202403942U CN202403942U CN2012200354214U CN201220035421U CN202403942U CN 202403942 U CN202403942 U CN 202403942U CN 2012200354214 U CN2012200354214 U CN 2012200354214U CN 201220035421 U CN201220035421 U CN 201220035421U CN 202403942 U CN202403942 U CN 202403942U
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- China
- Prior art keywords
- sampling
- utility
- reaction vessel
- model
- sampler
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 238000005070 sampling Methods 0.000 title claims abstract description 32
- 238000006243 chemical reaction Methods 0.000 title abstract description 26
- 238000003786 synthesis reaction Methods 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 13
- 238000001514 detection method Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000031709 bromination Effects 0.000 description 1
- 238000005893 bromination reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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Abstract
The utility model discloses a sampling device for a synthetic reaction kettle. The sampling device comprises the synthetic reaction kettle; the sampling device is arranged at the bottom of the synthetic reaction kettle; the sampling device comprises a sampling pipe communicated with the inner cavity of the synthetic reaction kettle, and a lofting valve and a sampling valve which are arranged on the sampling pipe from top to bottom; and a sampling bin is arranged between the lofting valve and the sampling valve. Compared with the prior art, the utility model has the advantages that the sampling device is safe and convenient to sample, a vacuum system is not required to be closed in vacuum reaction, the reaction conditions in the reaction kettle are not destroyed, and the reaction quality is ensured.
Description
Technical field
The utility model relates to sampler, relates in particular to a kind of sampler that is used for synthesis reaction vessel.
Background technology
In Chemical Manufacture, synthesis reaction vessel is the synthesis device of using always, often needs repeatedly in agitated reactor, take a sample in synthetic reaction process and after the reaction end, and detection reaction still internal reaction carries out situation or reaction finishes the product quality indicator situation.Traditional sampling detection mode is generally the manhole or the interior sampling of hand hole autoreaction still of opening the agitated reactor top, or is provided with sample valve in the bottom of agitated reactor, from the sample valve sampling, detects then.These two kinds sampling detection mode not only troublesome poeration, hysteresis, and destroyed the molecular balance of system in the agitated reactor, make the normal reaction process be interrupted, influence reaction process and product quality.Especially be corrosive, in the reaction that poisonous gas is participated in, cause easily during sampling that hazardous gas effluxes synthetic grade of bromination, cause environmental pollution or bring harm the operator is healthy; When needs vacuumize reaction, also need close vacuum system, destroyed the reaction conditions in the agitated reactor; And generally be to carry out at a certain temperature in synthetic reaction, above-mentioned dual mode all has certain danger to operating personnel when taking a sample.
The utility model content
The utility model technical matters to be solved is: the deficiency to prior art exists provides a kind of safe ready of taking a sample, can not destroy the sampler that is used for synthesis reaction vessel of molecular balance.
For solving the problems of the technologies described above, the technical scheme of the utility model is:
The sampler that is used for synthesis reaction vessel; Comprise synthesis reaction vessel; The bottom of said synthesis reaction vessel is provided with sampler; Said sampler comprises the stopple coupon that is communicated with the inner chamber of said synthesis reaction vessel and is arranged on setting-out valve and the sample cock on the said stopple coupon from top to bottom, is provided with the sampling feed bin between said setting-out valve and the sample cock.
As a kind of preferred, the bottom of said synthesis reaction vessel is provided with material outlet, and said sampler is arranged on said material outlet place.
As a kind of improvement, said sampling feed bin is provided with transparent form.
Owing to adopted technique scheme, the beneficial effect of the utility model is:
The sampler of the utility model comprises setting-out valve and the sample cock that is arranged on the said stopple coupon from top to bottom, is provided with the sampling feed bin between said setting-out valve and the sample cock, when sampling, opens the setting-out valve earlier; To expect that appearance is put into the sampling feed bin; Close the setting-out valve then, open sample cock again, access material appearance; Compare prior art sampling safety and convenient; And when vacuum reaction, need not close vacuum system, and can not destroy agitated reactor internal reaction condition, guaranteed reaction mass.
The utility model is provided with transparent form on the sampling feed bin, when opening the setting-out of setting-out valve, can how much come setting-out according to sampling amount, avoids the material waste.
Description of drawings
Accompanying drawing is the structural representation of the utility model embodiment.
Among the figure: 1. synthesis reaction vessel; 2. material outlet; 3. material inlet; 4. vacuum interface; 5. sampler; 51. stopple coupon; 52. setting-out valve; 53. sample cock; 54. sampling feed bin; 55. transparent window.
Embodiment
Further set forth the utility model below in conjunction with accompanying drawing.Should be understood that these embodiment only to be used to the utility model is described and be not used in the restriction the utility model scope.Should be understood that in addition those skilled in the art can do various changes or modification to the utility model after the content of having read the utility model instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Shown in accompanying drawing; The sampler that is used for synthesis reaction vessel comprises synthesis reaction vessel 1, and the bottom of said synthesis reaction vessel 1 is provided with material outlet 2; The top is provided with material inlet 3 and vacuum interface 4; Material outlet 2 places of the bottom of said synthesis reaction vessel 1 are provided with sampler 5, and said sampler 5 comprises the stopple coupon 51 that is communicated with the inner chamber of said synthesis reaction vessel 1 and is arranged on the setting-out valve 52 and sample cock 53 on the said stopple coupon 51 from top to bottom; Be provided with sampling feed bin 54 between said setting-out valve 52 and the sample cock 53, said sampling feed bin 54 is provided with transparent window 55.
During the utility model work, in synthetic reaction process, when needing the sampling detection reaction to carry out degree or final products purity; At first open the setting-out valve 52 at material outlet 2 places that are located at synthesis reaction vessel 1 bottom; To expect that appearance is put into sampling feed bin 54, observe what of lofting amounts, close setting-out valve 52 then through the transparent window that is provided with of sampling feed bin 54 55; Open sample cock 53 again, access material appearance.
More than show and described the advantage of ultimate principle, principal character and the utility model of the utility model.The technician of the industry should understand; The utility model is not restricted to the described embodiments; The principle of describing in the foregoing description and the instructions that the utility model just is described; Under the prerequisite that does not break away from the utility model spirit and scope, the utility model also has various changes and modifications, and these variations and improvement all fall in the utility model scope that requires protection.The utility model protection defined by the appended claims and their equivalents defined
.
All are from the design of the utility model, and the structure conversion of having done without creative work all drops within the protection domain of the utility model.
Claims (3)
1. the sampler that is used for synthesis reaction vessel; Comprise synthesis reaction vessel; The bottom of said synthesis reaction vessel is provided with sampler; It is characterized in that: said sampler comprises the stopple coupon that is communicated with the inner chamber of said synthesis reaction vessel and is arranged on setting-out valve and the sample cock on the said stopple coupon from top to bottom, is provided with the sampling feed bin between said setting-out valve and the sample cock.
2. the sampler that is used for synthesis reaction vessel as claimed in claim 1 is characterized in that: the bottom of said synthesis reaction vessel is provided with material outlet, and said sampler is arranged on said material outlet place.
3. the sampler that is used for synthesis reaction vessel as claimed in claim 1 is characterized in that: said sampling feed bin is provided with transparent form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012200354214U CN202403942U (en) | 2012-02-04 | 2012-02-04 | Sampling device for synthetic reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012200354214U CN202403942U (en) | 2012-02-04 | 2012-02-04 | Sampling device for synthetic reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202403942U true CN202403942U (en) | 2012-08-29 |
Family
ID=46701583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012200354214U Expired - Lifetime CN202403942U (en) | 2012-02-04 | 2012-02-04 | Sampling device for synthetic reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202403942U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108463706A (en) * | 2015-12-10 | 2018-08-28 | 阿克森斯公司 | Granular solids sampler |
-
2012
- 2012-02-04 CN CN2012200354214U patent/CN202403942U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108463706A (en) * | 2015-12-10 | 2018-08-28 | 阿克森斯公司 | Granular solids sampler |
| CN108463706B (en) * | 2015-12-10 | 2021-03-12 | 阿克森斯公司 | Granular solid sampling device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: SHANDONG HEYI BIOLOGY TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: WEIFANG XINGXIN TECHNOLOGY SERVICE CO., LTD. Effective date: 20130503 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 261061 WEIFANG, SHANDONG PROVINCE TO: 262737 WEIFANG, SHANDONG PROVINCE |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20130503 Address after: 262737, Shandong, Weifang Binhai Economic and Technological Development Zone, east of China Road, north of innovation Street Patentee after: SHANDONG HEYI CHEMICAL TECHNOLOGY CO.,LTD. Address before: 819 room 261061, Gaoxin street, Gaoxin street, Weifang hi tech Zone, Shandong Patentee before: Weifang Xingxin Technology Service Co.,Ltd. |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Sampling device for synthetic reaction kettle Effective date of registration: 20150831 Granted publication date: 20120829 Pledgee: China Co. truction Bank Corp of Weifang Haihua branch Pledgor: SHANDONG HEYI CHEMICAL TECHNOLOGY CO.,LTD. Registration number: 2015990000741 |
|
| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20180817 Granted publication date: 20120829 Pledgee: China Co. truction Bank Corp of Weifang Haihua branch Pledgor: SHANDONG HEYI CHEMICAL TECHNOLOGY CO.,LTD. Registration number: 2015990000741 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Sampling device for synthetic reaction kettle Effective date of registration: 20181010 Granted publication date: 20120829 Pledgee: China Co. truction Bank Corp of Weifang Haihua branch Pledgor: SHANDONG HEYI CHEMICAL TECHNOLOGY CO.,LTD. Registration number: 2018980000183 |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20120829 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220704 Granted publication date: 20120829 Pledgee: China Co. truction Bank Corp of Weifang Haihua branch Pledgor: SHANDONG HEYI CHEMICAL TECHNOLOGY CO.,LTD. Registration number: 2018980000183 |