CN103741449B - A kind of anti-static fabric and weaving method - Google Patents
A kind of anti-static fabric and weaving method Download PDFInfo
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- CN103741449B CN103741449B CN201410016238.3A CN201410016238A CN103741449B CN 103741449 B CN103741449 B CN 103741449B CN 201410016238 A CN201410016238 A CN 201410016238A CN 103741449 B CN103741449 B CN 103741449B
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Abstract
The present invention discloses a kind of anti-static fabric and weaving method, relates to a kind of anti-static fabric knitting method of the nano zine oxide containing special shape, belongs to the field of weaving.This invention through alkali treatment by base cloth fabric, then in the solution containing zinc salt, the aqueous slkali containing amino, high molecular polymer, alcohols material, then after 35KHz frequency ultrasound 15min, is taken out to dry and is soaked; Finally fabric is placed on and dries 30min in 60 DEG C of baking ovens and obtain product.Its beneficial effect is: anti-static fabric of the present invention, and soft, comfortable ventilating is good, and antistatic performance excellent, weave without the need to Special Equipment, process easy, clothes fashion is not limit; Can dye arbitrarily, product itself is without environmental hazard.
Description
Technical field
The present invention relates to a kind of anti-static fabric knitting method of the nano zine oxide containing special shape, belong to the field of weaving, specifically a kind of anti-static fabric and weaving method.
Background technology
Along with the progress of technology and the development of society, the requirement of people to quality of life is more and more higher, especially more and more higher to the environmental requirement of daily life.Thus, the product of high-tech content constantly enters into textiles industry.The functional treatment processing of textiles constantly increases, and by giving these special functional added values improving textiles of textiles, thus improving the living environment of people, meeting the material requisite that people are growing.The various impacts of electrostatic on human society are well-known, can affect the precision of electronic product; Can cause producing electric discharge phenomena in petrochemical industry operation and setting off an explosion or burn; Human body static electrification also can cause easy dust suction, dress discomfort, have the harmful effects such as electric-shock feeling.In view of the foregoing, antistatic industry is all devoted to the research of anti-static product.
In polyamide textile processing and use procedure, polyamide fiber each other or all can generating strap electrical phenomena with the friction of other object contacts, if electric charge constantly accumulates and fails elimination, will cause various electrostatic phenomenon.Electrostatic makes polyamide textile processing difficulties, easy attract dust, the electric spark that electrostatic produces, and can set off an explosion and fire.The antistatic approach that polyamide fiber is conventional is: antistatic additive is added fibrous inside and surface, but the shortcomings such as its comprehensive comparison is poor, feel is poor, lack of homogeneity, fastness to washing are poor, poor air permeability; Utilize blended union mode to be mixed into conductive fiber in textiles, its antistatic property and durability are all more excellent, but its production cost is higher, and technics comparing is complicated, and feel is poor.
The durable antistatic textiles obtained in prior art, its main method is: 1. apply anion or CATION or both sexes or non-ionic surface active agent at fabric face; 2. the agent of surface-activity phase is mixed in fabric; 3. by RESIN FINISH, conductive resin is added in inside fabric; 4. by chemical graft, the macromolecule of electric conductivity is connected on fiber surface.As made on synthetic fiber band hygroscopicity group with antistatic performance; 5. component fibre structural molecule is improved; 6. the low component of reactive is added in the fibre.
Method is 1. easy to use, and current domestic and international application is relatively more extensive, but its defect is not durable, and process is soaped or dry-cleaning can be lost efficacy because coming off; 2. method is only applied on film; Method is 3. 4. 5. comparatively large on the physical property impact of fabric, and somewhat expensive; 6. method belongs to interior antistatic, can solve the electrostatic obstacle that fabric produces in manufacture process and use procedure, but after fabric itself is processed, then carry out processing weaving, in this process, its antistatic behaviour can be affected because of scattering and disappearing of its active ingredient again.Meanwhile, also also exist that manufacturing technique complexity, cost are high, feel is soft not, designs and varieties are few, conductive compound is on the impact of human body and the weak point such as serviceability is poor.
Summary of the invention
The object of the present invention is to provide a kind of anti-static fabric and weaving method.
For achieving the above object, the manufacture method of a kind of antistatic textile of the present invention, comprises the steps:
1. base cloth fabric fabric is put into 20 ~ 30g/L aqueous slkali to process, the part by weight of base cloth fabric fabric and aqueous slkali is made to be 1:50, at 60 ~ 100 DEG C of process 75 ~ 105min, room temperature is cooled to after process, be in the acetum of 2 ~ 5% again by concentration and pH to 7 ~ 10, the rear 60 DEG C of dry for standby of water cleaning;
2. obtain solution, gets in the solution of the zinc salt of 50ml0.04 ~ 0.12mol/L the aqueous slkali containing amino adding 50ml0.08 ~ 0.15mol/L, carries out vigorous stirring 2h with the speed of 400 ~ 1000rpm, keep obtain solution temperature to be 60 ~ 95 DEG C;
3. in the container that step 2. obtained solution is housed, the base cloth fabric fabric for subsequent use 1. prepared through step is added, the high molecular polymer and the concentration that add 0.4g are wherein 95% alcohols material 50ml simultaneously, then be placed in 35KHz frequency ultrasound process 15min, take out after base cloth fabric fabric dries and base cloth fabric fabric is immersed again;
4. last base cloth fabric fabric is put in an oven 60 DEG C dry 30min.
Described base cloth fabric is several or a kind of in blending, cotton, woollen goods;
The alkali used in described Alkali reduction is inorganic base, and wherein the kind of inorganic base is several or a kind of in NaOH, ammoniacal liquor, urea, ammonium;
Described zinc salt is several or a kind of in zinc nitrate, zinc chloride, zinc acetate;
Described high molecular polymer is several or a kind of in polyvinylpyrrolidone (PVP), polyethylene glycol;
Described alcohols material is the combination of a kind of or its any amount in ethanol or methyl alcohol, and the concentration of alcohols material is 95%.
A kind of anti-static fabric of the present invention and weaving method, its beneficial effect is: anti-static fabric of the present invention, and soft, comfortable ventilating is good; And antistatic performance is excellent; The antistatic performance of the fabric that anti-static fabric of the present invention is made into meets the requirement of standard GB/T 12014-2009 " anti-static clothing "; This fabric is specially adapted to staff's dress of the inflammable and explosive environment such as oil, chemical industry, colliery, oil depot gas station, electric power, is widely used; The product of the method manufacture has excellent textile performance, and weaving is without the need to Special Equipment, and process easy, clothes fashion is not limit; Can dye arbitrarily, product itself is without environmental hazard.
Detailed description of the invention
Be clearly and completely described below in conjunction with the technical scheme in the embodiment of the present invention, obviously, described embodiment is only one of them embodiment of the present invention, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
1. blended yarn woven fabric fabric is put into 20g/L sodium hydroxide alkali groove, carry out alkali decrement treatment, the part by weight of blended yarn woven fabric fabric and aqueous slkali is made to be 1:50, at the condition process 75min of 60 DEG C, room temperature is cooled to after process, being neutralized to pH with the acetum that concentration is 2% is 7, the rear 60 DEG C of dry for standby of water cleaning;
2. obtain solution, gets in the solution of the zinc nitrate of 50ml0.04mol/L the aqueous slkali containing amino adding 50ml0.08mol/L, carries out vigorous stirring 2h with the speed of 400rpm, keep obtain solution temperature to be 60 ~ 95 DEG C;
3. in the container that step 2. obtained solution is housed, add the blended yarn woven fabric fabric for subsequent use 1. prepared through step, add the ethanol 50ml that the polyvinylpyrrolidone of 0.4g and concentration are 95% wherein simultaneously, then be placed in 35KHz frequency ultrasound process 15min, take out after blended yarn woven fabric fabric dries and blended yarn woven fabric fabric is immersed again;
4. finally blended yarn woven fabric fabric is put 60 DEG C of baking 30min in an oven.
Embodiment 2
1. cotton fabric fabric is put into 30g/L ammoniacal liquor alkali groove, make the part by weight of cotton fabric fabric and aqueous slkali be 1:50, under the condition of 100 DEG C, process 105min, be cooled to room temperature after process, being neutralized to pH with the acetum that concentration is 5% is 10, the rear 60 DEG C of dry for standby of water cleaning;
2. obtain solution, gets in the solution of the zinc chloride of 50ml0.12mol/L the aqueous slkali containing amino adding 50ml0.15mol/L, carries out vigorous stirring 2h with the speed of 1000rpm, keep obtain solution temperature to be 95 DEG C;
3. in the container that step 2 obtained solution is housed, add the cotton fabric fabric for subsequent use prepared through step 1, add the methyl alcohol 50ml that the polyethylene glycol of 0.4g and concentration are 95% wherein simultaneously, then be placed in 35KHz frequency ultrasound process 15min, take out after cotton fabric fabric dries and cotton fabric fabric is immersed again;
4. finally base cloth fabric fabric is put 60 DEG C of baking 30min in an oven.
Embodiment 3
1. woolen fabric fabric is put into 25g/L urea alkali groove to process, make the part by weight of woolen fabric fabric and aqueous slkali be 1:50, at 80 DEG C of process 90min, after process, be cooled to room temperature, be in the acetum of 3% by concentration and pH to 9, the rear 60 DEG C of dry for standby of water cleaning;
2. obtain solution, gets in the zinc acetate solution of 50ml0.08mol/L the aqueous slkali containing amino adding 50ml0.12mol/L, carries out vigorous stirring 2h with the speed of 600rpm, keep obtain solution temperature to be 80 DEG C;
3. in the container that step 2. obtained solution is housed, add the woolen fabric fabric for subsequent use 1. prepared through step, add the ethanol 50ml that the polyethylene glycol of 0.4g and concentration are 95% wherein simultaneously, then be placed in 35KHz frequency ultrasound process 15min, take out after woolen fabric fabric dries and woolen fabric fabric is immersed again;
4. finally woolen fabric fabric is put 60 DEG C of baking 30min in an oven.
The antistatic performance standard of country:
This anti-static product and existing product performance comparison:
Experimental result: by alkali-treated fabric after these techniques, surface resistivity reaches minimum 10
4.
Claims (4)
1. a manufacture method for antistatic textile, is characterized in that: comprise the steps:
1. base cloth fabric fabric is put into 20 ~ 30g/L aqueous slkali to process, the part by weight of base cloth fabric fabric and aqueous slkali is made to be 1:50, at 60 ~ 100 DEG C of process 75 ~ 105min, room temperature is cooled to after process, be in the acetum of 2 ~ 5% again by concentration and pH to 7 ~ 10, the rear 60 DEG C of dry for standby of water cleaning;
2. obtain solution, gets in the solution of the zinc salt of 50ml0.04 ~ 0.12mol/L the aqueous slkali containing amino adding 50ml0.08 ~ 0.15mol/L, carries out vigorous stirring 2h with the speed of 400 ~ 1000rpm, keep obtain solution temperature to be 60 ~ 95 DEG C;
3. in the container that step 2. obtained solution is housed, the base cloth fabric fabric for subsequent use 1. prepared through step is added, add the alcohols material 50ml that the high molecular polymer of 0.4g and concentration are 95% wherein simultaneously, then be placed in 35KHz frequency ultrasound process 15min, take out after base cloth fabric fabric dries and base cloth fabric fabric is immersed again;
4. last base cloth fabric fabric is put in an oven 60 DEG C dry 30min;
Wherein step 2. described in containing amino aqueous slkali be ammoniacal liquor and urea one or more; Wherein step 3. described in high molecular polymer be several or a kind of in polyvinylpyrrolidone (PVP), polyethylene glycol.
2. the manufacture method of a kind of antistatic textile as claimed in claim 1, is characterized in that: described base cloth fabric is several or a kind of in blending, cotton, woollen goods.
3. the manufacture method of a kind of antistatic textile as claimed in claim 1, is characterized in that: described zinc salt is several or a kind of in zinc nitrate, zinc chloride.
4. the manufacture method of a kind of antistatic textile as claimed in claim 1, is characterized in that: described alcohols material is the combination of a kind of or its any amount in ethanol or methyl alcohol.
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| CN201410016238.3A CN103741449B (en) | 2014-01-14 | 2014-01-14 | A kind of anti-static fabric and weaving method |
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| CN201410016238.3A CN103741449B (en) | 2014-01-14 | 2014-01-14 | A kind of anti-static fabric and weaving method |
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| CN103741449B true CN103741449B (en) | 2015-12-30 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104088167B (en) * | 2014-07-04 | 2016-08-17 | 常州大学 | A kind of improve the natural dye dying fabric color degree of depth and the method for light fastness |
| CN106149352B (en) * | 2016-08-09 | 2018-05-18 | 东华大学 | A kind of preparation method of nano zinc oxide modified cotton fabric |
| CN107476043A (en) * | 2017-08-31 | 2017-12-15 | 王露 | A kind of underwear antistatic process method |
| CN107956116A (en) * | 2017-11-30 | 2018-04-24 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method of embroidery antistatic finishing agent |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102242475A (en) * | 2011-06-04 | 2011-11-16 | 淮北维科印染有限公司 | Production process for artificial silk bleached cloth |
| CN102493175A (en) * | 2011-11-24 | 2012-06-13 | 东华大学 | Method for preparing photoelectric functional compound fabric through fractional in-situ deposition |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102242475A (en) * | 2011-06-04 | 2011-11-16 | 淮北维科印染有限公司 | Production process for artificial silk bleached cloth |
| CN102493175A (en) * | 2011-11-24 | 2012-06-13 | 东华大学 | Method for preparing photoelectric functional compound fabric through fractional in-situ deposition |
Non-Patent Citations (1)
| Title |
|---|
| 涤纶织物表面纳米ZnO微晶的制备;周兆懿;《印染》;20091101(第21期);第1页-第5页 * |
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