CN103726337A - Fibrous curly hair fixing adhesion agent, preparation method and periwig prepared with adhesion agent - Google Patents
Fibrous curly hair fixing adhesion agent, preparation method and periwig prepared with adhesion agent Download PDFInfo
- Publication number
- CN103726337A CN103726337A CN201310580979.XA CN201310580979A CN103726337A CN 103726337 A CN103726337 A CN 103726337A CN 201310580979 A CN201310580979 A CN 201310580979A CN 103726337 A CN103726337 A CN 103726337A
- Authority
- CN
- China
- Prior art keywords
- weight portions
- deionized water
- silicone oil
- curly hair
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a fibrous curly hair fixing adhesion agent, a preparation method and a periwig prepared with the adhesion agent. The method comprises the steps as follows: deionized water is added in an emulsifying machine and heated to 60-70 DEG C; 10-20 parts by weight of polyether modified amino-silicone and 10-20 parts of positive ion amino silicon oil terpolymer are added and stirred to enable the components to sufficiently disperse into the deionized water; and the temperature is decreased to 30-40 DEG C, 5-15 parts of epoxy silicone oil and 5-10 parts of PVP (polyvinyl pyrrolidone) copolymer are added after deionized water is supplemented, stirring is continuously performed for 1-1.5 hours to obtain a uniform light and white emulsion suffused with blue light, and the PH value is regulated into faintly acid so as to obtain a finished product. The obtained adhesion agent can be used for preparing the periwig, a transparent and glossy continuous film is formed on the fiber surface, is flexible and is not sticky, and accordingly, a higher fixing capacity and durable curl retainability are further obtained with lower usage quantity.
Description
[technical field]
The present invention relates to fibre trimmer and method and technology field, the wig that is specifically related to fiber curly hair sizing adhesive and preparation method and prepares with it.
[background technology]
Hair product industry, conventionally has and a variety ofly with curling special type, sends out product, and this product, in post processing processing, need to add a certain amount of auxiliary agent that has sizing adhesive effect, keeps the sizing bonding effect of product curvature.And requirement is sticky and not stiff, soft and loose, the resistance to cleaning texts of wearing.Fiber after arranging with the post processing maceration extract that is added with this adhesive, can fiber surface form the high-elastic transparent mantle of one deck give curly hair send out thread between moulding lasting, flexible smooth, not crude not stiff, high-elastic gloss, the dynamic beautiful sensation of people's youth of giving, simultaneously resistance to wear resistance to cleaning good.Thereby improve the quality of products class and added value.
In wig product, a large amount of adhesives that use are generally the adhesive of polyacrylic resin class in recent years, and are anionic property, and generally want and be generally cationic feel auxiliary agent separately to use, in order to avoid zwitterion reacts neutralization and reduces drug effect.Although it is pretty good that the special type after immersion is sent out product sizing bonding effect, but feel is stiff and institute's film forming is disposable dura mater, after comb is loose, just can not stick together again, wear a period of time or clean after will a slice at random, need to arrive professional hairdressing mechanism again moulding arrange and just can continue to use, be very loaded down with trivial details.Wearing wig today as a kind of fashion, people, to the extraordinary pursuit of sending out product of wig, remove outward appearance personalization, superior, more its curvature cohesiveness, persistence and the resistance to property worn are had higher requirement.This invention has overcome the some shortcomings shortcoming of conventional adhesive, with the bonding performance such as washable of good resilient flexible, is extensively favored.
[summary of the invention]
Object of the present invention is exactly that a kind of sizing adhesive that can form on human hair or synthetic fiber surface a kind of transparent flexible elastic membrane will be provided, and gives fiber softening elasticity, moulding is lasting, smooth glossy, laundry-resistant characteristic.
A kind of fiber curly hair sizing adhesive, is comprised of the polyether modified silicon oil of 10～20 weight portions, the cation amino-silicone oil terpolymer of 10～20 parts, the epoxide modified silicone oil of 5～15 parts, the PVP based polymer of 5～10 parts and the deionized water of 35～70 weight portions.
Preferably by the polyether modified amino silicone oil of 15 weight portions, the cation amino silicon terpolymer of 15 weight portions, epoxide modified silicone oil, the PVP based copolymer of 10 weight portions and the deionized water of 50 weight portions of 10 weight portions, formed.
Preferably by the polyether modified amino silicone oil of 10 weight portions, the cation amino silicon terpolymer of 20 weight portions, epoxide modified silicone oil, the PVP based copolymer of 15 weight portions and the deionized water of 45 weight portions of 10 weight portions, formed.
The present invention also comprises a kind of preparation method of fiber curly hair sizing adhesive, and the method is comprised of following steps:
Deionized water is added in mulser, while being heated to 60～70 ℃;
Add the cation amino-silicone oil terpolymer of 10～20 weight portion polyether modified amino silicone oil and 10～20 parts, open to stir it is scattered in deionized water completely;
Be cooled to 30～40 ℃, after benefit deionized water, add again 5～15 parts of epoxy silicon oils and 5～10 parts of PVP based copolymers, continue to stir 1～1.5 hour, obtain uniform pale blueing light emulsion, after adjusting pH value is faintly acid, get product.
A kind of wig, is characterized in that being made by following steps:
Pending fiber is fully immersed by consumption 2～6% (o.w.f), bath raio 1:10～15 in the maceration extract that contains above-mentioned fiber curly hair sizing adhesive;
At 25～30 ℃, flood 15～20 minutes;
After dipping, take out, to fiber product curvature moulding post-drying.
Polyether modified amino silicone oil, under the prerequisite of excellent feel that keeps amido silicon oil, has greatly improved its hydrophily and has been difficult for xanthochromia and stability of emulsion.The emulsion of stable performance simultaneously can make siloxanes arrange better and be bonded to fiber surface, forms the continuous film of uniform thickness, reduces fibre-fibre friction coefficient, thereby has the smooth effect of significant softness and have good antistatic effect.Described polyether modified silicon oil can be one or more of similar silicone oil of different molecular.
Cation amino silicon terpolymer, for not containing unique high molecular (AB) n terpolymer of surfactant, its collection organic silicon hydrophobic section and polyethers hydrophilic section and one's share of expenses for a joint undertaking, unique molecular structure like this, there is low-down surface tension and excellent spreadability, than traditional amido silicon oil, more easily on impaired hair quality, deposit, nurse one's health submissively, moisturizing keeps curly headed memory.Not only liquid outward appearance stable homogeneous is good, and has good compatibility, and the soft moisturizing memory characteristic that it is good allows fiber curly hair product reach soft and not loose, the effect that moulding is lasting.
Epoxide modified silicone oil is as the stronger organosilicon functional polymer of a kind of activity compound, when the high-elastic feel of smooth, soft is provided, due to itself reactivity and the characteristic such as high adsorption, can with fiber in the functional group such as hydroxyl, amino or carboxyl form covalent bond, with fiber strong bonded, can be further crosslinked with other active group in curing process in the later stage, form finer and close network structure silicon fiml, bar has improved crock fastness and the soaping fastness of wig product greatly.Described epoxy silicon oil can be one or more of similar silicone oil of different molecular.
PVP based copolymer has effectively overcome the deficiency of PVP self, has better film forming and conditioning property, is widely used in fiber hair styling product.Use compatibility is fabulous, and fiber is had to good affinity interaction, can significantly reduce the resistance of wet comb, at fiber surface, form transparent glossiness continuous film, pliable and tough and tack-free, under lower consumption, also can reach higher sizing ability, and lasting crimp retention.
Curly hair provided by the invention sizing adhesive is a kind of organic silicone finishing agent, can be with water arbitrarily than dilution, flood easy to usely, and and natural hair and artificial fiber curly hair are all had to good sizing bonding effect, production equipment is simple, and effect is remarkable.
[specific embodiment]
Below by specific embodiment, the present invention will be further described, and following embodiment is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.
Embodiment 1
1, fiber curly hair sizing adhesive component formula (in parts by weight):
The polyether modified amino silicone oil of 15g, can select conventional polyether modified amino silicone oil, preferably the polyether-modified dimethicone of mass percent 20-35%, thickener and the 60%-80% deionized water of 1-5%, consists of.
The cation amino silicon terpolymer of 15g, can select conventional polyether modified amino silicone oil, preferably by amino silicon cation polyether (AB) n of mass percent 60-80% terpolymer, 20-40% deionized water.
The epoxide modified silicone oil of 10g, can select conventional epoxide modified silicone oil, preferably by the epoxide modified dimethicone of the epoxide number >0.03 of mass percent 30-40%, the isomerous tridecanol ether emulsifying agent of 5-10%, thickener and the 60%-70% deionized water of 1-5%, be formed.
The PVP based copolymer of 10g, can select conventional PVP based copolymer, preferably contains the aqueous solution of 10% VP/ dimethylamino-propyl methacrylamide copolymer.
The deionized water of 50g.
2, preparation method:
The deionized water of 50g is put into beaker, while being heated to 70 ℃ of temperature, the ternary polymerization organosilicon of 15g polyether modified amino silicone oil and 15g is added, stir until be scattered in completely in water with mixer, be cooled to 40 ℃, after moisturizing, add the epoxy silicon oil of 10g and the PVP based copolymer of 10g, continue to stir 60 minutes, obtain uniform pale blueing light emulsion, after adjusting pH value is faintly acid, get product.
3, dipping using method:
Get the hand feel finishing liquid of 1000 milliliters 30 ℃ preparing in advance, add 4 grams of above-mentioned products that make to stir, it is fully dissolved, obtain maceration extract; Get 100 grams of pending fiber curly hair products, put into maceration extract, soak 20 minutes; Fiber after dipping is pulled out, on special double-edged fine-toothed comb, curly hair product is carried out to curvature moulding post-drying.
Embodiment 2
1, fiber curly hair sizing adhesive component formula (in parts by weight): the polyether modified amino silicone oil of 10g, the cation amino silicon terpolymer of 20g, the epoxide modified silicone oil of 10g, the PVP based copolymer of 15g, the deionized water of 45g.
2, preparation method:
The deionized water of 45g is put into beaker, while being heated to 70 ℃ of temperature, the ternary polymerization organosilicon of 10g polyether modified amino silicone oil and 20g is added, stir until be scattered in completely in water with mixer, be cooled to 40 ℃, after moisturizing, add the epoxy silicon oil of 10g and the PVP based copolymer of 15g, continue to stir 60 minutes, obtain uniform pale blueing light emulsion, after adjusting pH value is faintly acid, get product.
3, dipping using method:
Get the hand feel finishing liquid of 1000 milliliters 30 ℃ preparing in advance, add 3 grams of above-mentioned products that make to stir, it is fully dissolved, obtain maceration extract; Get 100 grams of pending fiber curly hair products, put into maceration extract, soak 20 minutes; Fiber after dipping is pulled out, on special double-edged fine-toothed comb, curly hair product is carried out to curvature moulding post-drying.
Claims (8)
1. a fiber curly hair sizing adhesive, is characterized in that being comprised of the polyether modified silicon oil of 10～20 weight portions, the cation amino-silicone oil terpolymer of 10～20 parts, the epoxide modified silicone oil of 5～15 parts, the PVP based polymer of 5～10 parts and the deionized water of 35～70 weight portions.
2. fiber curly hair sizing adhesive as claimed in claim 1, is characterized in that being comprised of the polyether modified amino silicone oil of 15 weight portions, the cation amino silicon terpolymer of 15 weight portions, epoxide modified silicone oil, the PVP based copolymer of 10 weight portions and the deionized water of 50 weight portions of 10 weight portions.
3. fiber curly hair sizing adhesive as claimed in claim 1, is characterized in that the polyether modified amino silicone oil of 10 weight portions, the cation amino silicon terpolymer of 20 weight portions, epoxide modified silicone oil, the PVP based copolymer of 15 weight portions and the deionized water of the 45 weight portions composition of 10 weight portions.
4. the fiber curly hair sizing adhesive as described in as arbitrary in claim 1～3, is characterized in that the polyether-modified dimethicone that described polyether modified amino silicone oil is 20-35% by mass percent, thickener and the 60%-80% deionized water of 1-5% form.
5. the fiber curly hair sizing adhesive as described in as arbitrary in claim 1～3, is characterized in that described cation amino silicon terpolymer is comprised of amino silicon cation polyether (AB) n terpolymer and the 20-40% deionized water of mass percent 60-80%.
6. the fiber curly hair sizing adhesive as described in as arbitrary in claim 1～3, is characterized in that described PVP based copolymer is the aqueous solution of the VP/ dimethylamino-propyl methacrylamide copolymer that contains mass percent 10%.
7. a preparation method for fiber curly hair sizing adhesive, is characterized in that the method is comprised of following steps:
Deionized water is added in mulser, while being heated to 60～70 ℃;
Add the cation amino-silicone oil terpolymer of 10～20 weight portion polyether modified amino silicone oil and 10～20 parts, open to stir it is scattered in deionized water completely;
Be cooled to 30～40 ℃, after benefit deionized water, add again 5～15 parts of epoxy silicon oils and 5～10 parts of PVP based copolymers, continue to stir 1～1.5 hour, obtain uniform pale blueing light emulsion, after adjusting pH value is faintly acid, get product.
8. a wig, is characterized in that being made by following steps:
Pending fiber is fully immersed by consumption 2～6% (o.w.f), bath raio 1:10～15 in the maceration extract that contains fiber curly hair sizing adhesive described in claim 1;
At 25～30 ℃, flood 15～20 minutes;
After dipping, take out, to fiber product curvature moulding post-drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310580979.XA CN103726337B (en) | 2013-11-18 | 2013-11-18 | Fiber curly hair sizing adhesive and preparation method and the wig prepared with it |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310580979.XA CN103726337B (en) | 2013-11-18 | 2013-11-18 | Fiber curly hair sizing adhesive and preparation method and the wig prepared with it |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103726337A true CN103726337A (en) | 2014-04-16 |
| CN103726337B CN103726337B (en) | 2016-08-17 |
Family
ID=50450610
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310580979.XA Active CN103726337B (en) | 2013-11-18 | 2013-11-18 | Fiber curly hair sizing adhesive and preparation method and the wig prepared with it |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103726337B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107828364A (en) * | 2017-11-16 | 2018-03-23 | 许昌学院 | Special adhesive of curly hair and preparation method thereof in a kind of wig process |
| CN108236155A (en) * | 2018-01-19 | 2018-07-03 | 安徽富泰发饰文化股份有限公司 | A kind of heat-setting method of wig curly hair |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005187684A (en) * | 2003-12-26 | 2005-07-14 | Lion Corp | Modified silicone emulsion, its manufacturing method and soft finishing agent for clothing |
| CN101424041A (en) * | 2007-10-30 | 2009-05-06 | 河南瑞贝卡发制品股份有限公司 | Method for preparing isolated hair finishing auxiliaries after frizzy hair and use |
| CN101818452A (en) * | 2010-03-17 | 2010-09-01 | 许昌恒源发制品股份有限公司 | Curly hair dressing agent for hair products, preparation method and method for dressing hair products |
-
2013
- 2013-11-18 CN CN201310580979.XA patent/CN103726337B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005187684A (en) * | 2003-12-26 | 2005-07-14 | Lion Corp | Modified silicone emulsion, its manufacturing method and soft finishing agent for clothing |
| CN101424041A (en) * | 2007-10-30 | 2009-05-06 | 河南瑞贝卡发制品股份有限公司 | Method for preparing isolated hair finishing auxiliaries after frizzy hair and use |
| CN101818452A (en) * | 2010-03-17 | 2010-09-01 | 许昌恒源发制品股份有限公司 | Curly hair dressing agent for hair products, preparation method and method for dressing hair products |
Non-Patent Citations (1)
| Title |
|---|
| 刘术佳等: "功能性发制品用PVC纤维纺丝工艺探讨", 《合成技术及应用》, vol. 27, no. 1, 31 March 2012 (2012-03-31), pages 33 - 37 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107828364A (en) * | 2017-11-16 | 2018-03-23 | 许昌学院 | Special adhesive of curly hair and preparation method thereof in a kind of wig process |
| CN107828364B (en) * | 2017-11-16 | 2020-11-13 | 许昌学院 | Adhesive special for curling hair in wig processing process and preparation method thereof |
| CN108236155A (en) * | 2018-01-19 | 2018-07-03 | 安徽富泰发饰文化股份有限公司 | A kind of heat-setting method of wig curly hair |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103726337B (en) | 2016-08-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110172826B (en) | Moisturizing fabric containing hyaluronic acid | |
| CN109554919A (en) | A kind of skin care antibacterial microcapsule finishing agent and its preparation method and application | |
| CN102552088B (en) | Rapid-nourishing hair-care combination | |
| CN101884604B (en) | Method for the shaping of hair by means of a step of applying a reducing composition and a heating step | |
| CN108166157A (en) | Antibacterial spunlace non-woven cloth beauty mask base fabric of a kind of moisture absorption and preparation method thereof | |
| CN104822421B (en) | Including the composition of organic siliconresin and silicone rubber compounds, the personal care product containing the composition | |
| CN111671677A (en) | Softening and repairing plant hair care composition | |
| CN103800252A (en) | Hair-care composition capable of quickly and deeply repairing hair | |
| CN109475759A (en) | Cosmetic care system | |
| KR102640128B1 (en) | Hair care compositions and methods | |
| CN105380831A (en) | Mild nursing hair oil treatment and care composition containing no silicone oil and preparation method of mild nursing hair oil treatment and care composition | |
| CN103726337A (en) | Fibrous curly hair fixing adhesion agent, preparation method and periwig prepared with adhesion agent | |
| US20210022980A1 (en) | Hair-protecting composition comprising collagen and manufacturing method therefor | |
| CN111757684A (en) | Human hair fiber treating agent | |
| CN108677539A (en) | A kind of processing method of heat and moisture preserving cloth | |
| CN109431862A (en) | A kind of lasting eyeliner | |
| CN102525846B (en) | Hair care composition and preparation method thereof | |
| CN101644001A (en) | Preparation method and application of fiber pre-finishing auxiliary agent | |
| CN106061460B (en) | Hair nursing sensory agent | |
| CN109350554A (en) | A kind of Haircare composition and its application with deep layer repair | |
| CN101424041B (en) | Method for preparing isolated hair finishing auxiliaries after frizzy hair and use | |
| KR102620014B1 (en) | eyelash cosmetics | |
| CN102307560B (en) | Composition of temporary hair thickener | |
| CN105601844A (en) | Preparation method and application of novel modified organic silicon softening agent | |
| US3130127A (en) | Maleic anhydride and ethylene oxide copolymers in hair preparations |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |