CN101818452A - Curly hair dressing agent for hair products, preparation method and method for dressing hair products - Google Patents
Curly hair dressing agent for hair products, preparation method and method for dressing hair products Download PDFInfo
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- CN101818452A CN101818452A CN 201010125442 CN201010125442A CN101818452A CN 101818452 A CN101818452 A CN 101818452A CN 201010125442 CN201010125442 CN 201010125442 CN 201010125442 A CN201010125442 A CN 201010125442A CN 101818452 A CN101818452 A CN 101818452A
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Abstract
The invention relates to curly hair dressing agent for hair products, preparation method and method for dressing hair products. The curly hair dressing agent for hair products is compounded from the following raw materials by chemical reaction: 6wt% to 8wt% of bis(hydroxymethyl) vinylene vinylene carbamide, 6wt% to 9wt% of sodium carbonate, 0.3wt% to 0.9wt% of catalyst, 0.3wt% to 0.8wt% of additive, 0.8wt% to 1.2wt% of conditioner, 0.1wt% to 0.4wt% of dispersing agent and the balance of deionized water with the hardness not more than 0.3 milligram equivalent/L . The prepared dressing agent for hair products has the chemical structure of antibacterium, softening and changing shaggy coats, has the functions of anti-static electricity, antibacterium and UV resistance, and has the advantages of durable effect, no poison, no irritation and simple preparation technique.
Description
Technical field
The invention belongs to chemical technology, textile technology, the mutual interleaving techniques of biotechnology field, the method that is specifically related to a kind of hair products curly hair finishing agent and preparation technology thereof and hair products are put in order.
Background technology
The finishing agent of hair products is based on organic matter at present, and there are the most of organic matters of following defective (1) in it mainly is not obvious to its impact effect of hair fiber surface treatment, and deformation takes place easily.(2) be good between the organic matter that to carry out function composite for difficulty.(3) with traditional finishing agent to the hair fiber surface treatment after, look takes place when high temperature (〉=105 °) easily to be become.
Summary of the invention
The objective of the invention is to overcome above-mentioned the deficiencies in the prior art and a kind of antibiotic, anti-ultraviolet function is provided, effect is lasting, and nontoxic, non-stimulated, manufacture craft simple hair products curly hair finishing agent and preparation technology thereof and method that hair products are put in order.
The object of the present invention is achieved like this:
A kind of hair products curly hair finishing agent is characterized in that: formed according to the percentage by weight after chemical reaction is synthetic by following raw materials: two methylols time ethylene urea 6-8%, sodium carbonate 6-9%, catalyst 0.3-0.9%, additive 0.3-0.8%, activating agent 0.8-1.2%, conditioner 0.9-2%, dispersant 0.1-0.4%, surplus are the deionized water that hardness is not more than 0.03 equivalent parts per million;
Wherein catalyst is 0.2% FeSO with percentage by weight
4The aqueous solution, percentage by weight are that 0.01% watery hydrochloric acid mixes according to volume ratio at normal temperatures at 2: 1; Additive is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight; Activating agent is 0.25% MgSO with percentage by weight
4The aqueous solution, percentage by weight are that 1.0% the hydroxylamine hydrochloride aqueous solution mixes according to volume ratio at normal temperatures at 2: 1; Conditioner is that 3% the Sodium Tvlose aqueous solution, percentage by weight are that 1.6% the stearic acid aqueous solution mixes according to volume ratio at normal temperatures at 2: 1 with percentage by weight; Dispersant be according to percentage by weight with auxiliary material composition 25%, fatty alcohol-polyoxyethylene ether 12.5% and distilled water 62.5% through the synthetic mixture that forms of emulsion reaction, wherein the auxiliary material composition is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight.
A kind of preparation technology of above-mentioned hair products curly hair finishing agent is characterized in that: carry out according to following steps:
1), the choosing of reagent material: with as above two methylols time ethylene ureas and sodium carbonate as Main Ingredients and Appearance, the FeSO with 0.2%
4The mixture of the aqueous solution, 0.01% watery hydrochloric acid is as catalyst, and the mixture of the hexadecyltrimethylammonium chloride aqueous solution with 3%, 2.5% octadecyl dimethyl bromize ammonium solution is as additive, the MgSO with 0.25%
4The mixture of the aqueous solution, 1.0% the hydroxylamine hydrochloride aqueous solution is as activating agent, the mixture of the Sodium Tvlose aqueous solution with 3%, 1.6% the stearic acid aqueous solution is as conditioner, is dispersant with auxiliary material composition 25%, fatty alcohol-polyoxyethylene ether 12.5% and distilled water 62.5% through the synthetic mixture that forms of emulsion reaction, chooses the deionized water that hardness is not more than 0.03 equivalent parts per million;
2), the configuration of reagent solution: described additive joined 1/4 deionized water for stirring and form A solution, the described activating agent with 1/3 slowly joins in the described conditioner, forms B solution;
3) described catalyst is added in two methylol time ethylene ureas, stir and formed C solution in 10 minutes;
4), in 3/4 deionized water, slowly add the C solution stirring 30 minutes, slowly add sodium carbonate liquor limit edged and stir, add A solution after 20 minutes earlier, add B solution then, add remaining 2/3 described activating agent and described dispersant limit edged at last and stir, stir, after 30 minutes, obtain hair products curly hair finish solution, hair products curly hair finish solution is kept in Dark Place, and with blue thick PVC plastic cement barreled, preserve in the darkroom.
A kind of method of utilizing above-mentioned hair products curly hair finishing agent that hair products are put in order is characterized in that:
1), washing: with shampoo or washing powder washing hair products;
2), removal floating color: add in the 1000ml water with 30ml chlorine, put into above-mentioned hair products, soaked 3 minutes, clean, remove the loose colour on above-mentioned hair products surface;
3), softening: add the hair products curly hair finish solution of 20-30g in 1000ml water, solution temperature is controlled at 75 ℃, above-mentioned hair products is placed on soaked in this solution 20-30 minute again;
4), washing: above-mentioned hair products are cleaned up with shampoo or washing powder;
5), bubble oil: above-mentioned hair products are placed in the oil of 45-60 ℃ of temperature, steeped 20-25 minute, upper plate oven dry then.
The present invention has following advantage: prepared hair product finishing agent has antibiotic; softening; change the chemical constitution (soften cuticle on hair top layer; the reorganization disulfide bond); anlistatig function; in preparation process, do not use the elasticity of strong acid such as sulfuric acid to hair; toughness; the mechanical performance influence is less; the technology that the present invention adopts is fairly simple; make minuscule investment; the material therefor buying easily; be fit to large-scale production; the hair products of being put in order can reach 91.6% to the rate of ultraviolet shield of UVA section; rate of ultraviolet shield to the UVB section crosses 99.85%; its UPF value is 89.70; behind the hair products that this finishing agent of this external application was handled; steep oil processing again; feel behind the bubble oil is very good; good and the longer duration of curly hair effect; certain antibiotic through still having after the washing repeatedly; uvioresistant; antistatic; deformation does not take place, and handle effect is good.
The specific embodiment
Embodiment 1: a kind of hair products curly hair finishing agent is that the sodium carbonate with two methylols time ethylene ureas of 6 grams and 6 grams are the major ingredient composition, is the deionized water that 85.6 hardness that restrain are not more than 0.03 equivalent parts per million with catalyst 0.3 gram, additive 0.3 gram, activating agent 0.8 gram, conditioner 0.9 gram, dispersant 0.1 gram, surplus.The solution total amount of participating in reaction is 100g.
Wherein the catalyst of 0.3 gram is 0.2% FeSO with percentage by weight
4The aqueous solution, percentage by weight are that 0.01% watery hydrochloric acid mixes according to volume ratio at normal temperatures at 2: 1; 0.3 the additive of gram is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight; 0.8 the activating agent of gram is 0.25% MgSO with percentage by weight
4The aqueous solution, percentage by weight are that 1.0% the hydroxylamine hydrochloride aqueous solution mixes according to volume ratio at normal temperatures at 2: 1; 0.9 the conditioner of gram is that 3% the Sodium Tvlose aqueous solution, percentage by weight are that 1.6% the stearic acid aqueous solution mixes according to volume ratio at normal temperatures at 2: 1 with percentage by weight; 0.1 the dispersant of gram be according to percentage by weight with auxiliary material composition 0.025 gram, fatty alcohol-polyoxyethylene ether 0.0125 gram and distilled water 0.0625 gram through the synthetic mixture that forms of emulsion reaction, wherein the auxiliary material composition is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight.
Its manufacture craft is as follows:
1), deionized water for stirring that the additive of described 0.3 gram is joined 21.4 grams form the A solution, described activating agent 0.27 gram with 1/3 slowly joins in the described conditioner, forms B solution;
2), described catalyst 0.3 gram is joined in two methylols time ethylene ureas of 6 grams, stir 10 minutes formation C solution;
3), in the deionized water of 64.2 grams, slowly add the C solution stirring 30 minutes, slowly add sodium carbonate limit edged and stir, add A solution after 20 minutes earlier, add B solution then, add remaining 2/3 described activating agent 0.53 gram and the 0.1 gram limit edged stirring of described dispersant at last, stir, after 30 minutes, obtain hair products curly hair finish solution D, hair products curly hair finish solution is kept in Dark Place, and with blue thick PVC plastic cement barreled, preserve in the darkroom.
Using above-mentioned hair product finishing agent is the technology that hair products are put in order to the hair fabric:
Clean hair products with shampoo or washing powder---add in the 1000ml water and embathe hair products with 30ml solutions of chlorine (effective chlorine is 7.5 grams), the flush away loose colour, clean hair products---D solution (hair product finishing agent) with 2.5%, solution temperature is 75 ℃, soaked---cleaning hair products---bubble oil 20-25 minute with shampoo or washing powder, 45 ℃-60 ℃ of solution temperatures soak 20-25 minute---upper plate---oven dry (temperature is 70 ℃/1.5 hours).Deionized water: hardness≤0.03 milligram. equivalent/liter soft water.The deionized water total amount is the amount that final solution total amount 100 grams deduct other raw material.
Embodiment 2: a kind of hair products curly hair finishing agent is that the sodium carbonate with two methylols time ethylene ureas of 8 grams and 8 grams are the major ingredient composition, is the deionized water that 78.7 hardness that restrain are not more than 0.03 equivalent parts per million with catalyst 0.9 gram, additive 0.8 gram, activating agent 1.2 grams, conditioner 2 grams, dispersant 0.4 gram, surplus; The solution total amount of participating in reaction is 100g.
Wherein the catalyst of 0.9 gram is 0.2% FeSO with percentage by weight
4The aqueous solution, percentage by weight are that 0.01% watery hydrochloric acid mixes according to volume ratio at normal temperatures at 2: 1; 0.8 the additive of gram is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight; 1.2 the activating agent of gram is 0.25% MgSO with percentage by weight
4The aqueous solution, percentage by weight are that 1.0% the hydroxylamine hydrochloride aqueous solution mixes according to volume ratio at normal temperatures at 2: 1; The conditioners of 2 grams are that 3% the Sodium Tvlose aqueous solution, percentage by weight are that 1.6% the stearic acid aqueous solution mixes according to volume ratio at normal temperatures at 2: 1 with percentage by weight; 0.4 the dispersant of gram be according to percentage by weight with auxiliary material composition 0.1 gram, fatty alcohol-polyoxyethylene ether 0.05 gram and distilled water 0.25 gram through the synthetic mixture that forms of emulsion reaction, wherein the auxiliary material composition is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight.
Its manufacture craft is as follows:
1), deionized water for stirring that the additive of described 0.8 gram is joined 19.7 grams form the A solution, described activating agent 0.4 gram with 1/3 slowly joins in the described conditioner, forms B solution;
2) described catalyst 0.9 gram is joined in two methylols time ethylene urea of 8 grams, stir and formed C solution in 10 minutes;
4), in the deionized water of 59.0 grams, slowly add the C solution stirring 30 minutes, slowly add sodium carbonate limit edged and stir, add A solution after 20 minutes earlier, add B solution then, add remaining 2/3 described activating agent 0.8 gram and the stirring of described dispersant 0.4 Ke Kebian edged at last, stir, after 30 minutes, obtain hair products curly hair finish solution D, hair products curly hair finish solution is kept in Dark Place, and with blue thick PVC plastic cement barreled, preserve in the darkroom.
Using above-mentioned hair product finishing agent is the technology that hair products are put in order to the hair fabric:
Clean with shampoo or washing powder that hair products---the inferior chlorine water solution with 3% embathes hair products, the flush away loose colour cleans hair products---add 20 gram D solution (hair product finishing agent) with 1000ml water, solution temperature is 75 ℃, soaked---cleaning hair products---bubble oil 20-25 minute with shampoo or washing powder, 45 ℃-60 ℃ of solution temperatures soak 20-25 minute---upper plate---oven dry (temperature is 70 ℃/1.5 hours).
Embodiment 3: with two methylols time ethylene urea be sodium carbonate major ingredient composition, be catalyst with (1) activator, (2) additive is the auxiliary material composition, (3) activating agent, (4) conditioner, (5) dispersant.Its segmentation and consumption are: two methylols inferior ethylene urea: 7.5g, sodium carbonate: 6g, activator: 0.35g, additive: 0.3g, activating agent: 1g, conditioner: 1.1g, dispersant: 0.2g, all the other are deionized waters.The final solution total amount is 100g altogether.
Its manufacture craft is as follows:
1), with the 0.3g additive, the 20.89g deionized water and stirring forms A solution and the 1/3g activating agent is slowly joined forms B solution in the 1.1g conditioner.
2), the 0.35g activator joined in the two methylols of the 7.5g time ethylene ureas stirred 10 minutes, form C solution.
3), in remaining 62.66g deionized water, slowly add C solution, stirred 30 minutes, slowly add 6g sodium carbonate, the limit edged stirs, and adds A solution after 20 minutes earlier, adds B solution then, adding remaining 2/3g activating agent and 0.2g dispersant limit edged at last stirs, stir, obtain D solution (being hair product finishing agent) after 30 minutes, D solution is kept in Dark Place, as with blue thick PVC plastic cement barreled, preserve in the darkroom.
Use the finishing technique of above-mentioned hair product finishing agent to the hair fabric:
Clean hair products with shampoo or washing powder---with adding in the 1000ml water and embathe hair products with 30ml solutions of chlorine (effective chlorine is 7.5 grams), the flush away loose colour, clean hair products---D solution (hair product finishing agent) with 2.5%, solution temperature is 75 ℃, soaked---cleaning hair products---bubble oil 20-25 minute with shampoo or washing powder, 45 ℃-60 ℃ of solution temperatures soak 20-25 minute---upper plate---oven dry (temperature is 70 ℃/1.5 hours)
Embodiment 4: with two methylols time ethylene urea be that the sodium carbonate master expects composition, with (1) activator is catalyst, (2) additive and be the auxiliary material composition, (3) activating agent, (4) conditioner, (5) dispersant, its segmentation and consumption are: two methylols time ethylene urea: 7g, sodium carbonate: 6.5g, activator: 0.3g, additive: 0.4g, activating agent: 1.2g, conditioner: 1.45g, dispersant: 0.3g, all the other are deionized waters, the common 100g of final solution total amount.
Its manufacture craft is as follows:
1), with the 0.4g additive, the 20.7g deionized water and stirring forms A solution and the 0.4g activating agent is slowly joined forms B solution in the 1.45g conditioner.
2), the 0.3g activator joined in the two methylols of the 7g time ethylene ureas stirred 10 minutes, form C solution.
3), in remaining 62.15g ionized water, slowly add C solution, stirred 30 minutes, slowly add 6.5g sodium carbonate, the limit edged stirs, and adds A solution after 20 minutes earlier, add B solution then, add remaining 0.8g activating agent and 0.3g dispersant limit edged at last and stir, stir, after 30 minutes, obtain D solution (being hair product finishing agent), D solution is kept in Dark Place, and with blue thick PVC plastic cement barreled, preserve in the darkroom.
Use the finishing technique of above-mentioned hair product finishing agent to the hair fabric:
Clean with shampoo or washing powder that hair products---the inferior chlorine water solution with 3% embathes hair products, the flush away loose colour cleans hair products---add 2.0%D solution (hair product finishing agent) with 1000ml water, solution temperature is 75 ℃, soaked---cleaning hair products---bubble oil 20-25 minute with shampoo or washing powder, 45 ℃-60 ℃ of solution temperatures soak 20-25 minute---upper plate---oven dry (temperature is 70 ℃/1.5 hours).
Claims (3)
1. hair products curly hair finishing agent is characterized in that: formed according to the percentage by weight after chemical reaction is synthetic by following raw materials: two methylols time ethylene urea 6-8%, sodium carbonate 6-9%, catalyst 0.3-0.9%, additive 0.3-0.8%, activating agent 0.8-1.2%, conditioner 0.9-2%, dispersant 0.1-0.4%, surplus are the deionized water that hardness is not more than 0.03 equivalent parts per million;
Wherein catalyst is 0.2% FeSO with percentage by weight
4The aqueous solution, percentage by weight are that 0.01% watery hydrochloric acid mixes according to volume ratio at normal temperatures at 2: 1; Additive is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight; Activating agent is 0.25% MgSO with percentage by weight
4The aqueous solution, percentage by weight are that 1.0% the hydroxylamine hydrochloride aqueous solution mixes according to volume ratio at normal temperatures at 2: 1; Conditioner is that 3% the Sodium Tvlose aqueous solution, percentage by weight are that 1.6% the stearic acid aqueous solution mixes according to volume ratio at normal temperatures at 2: 1 with percentage by weight; Dispersant be according to percentage by weight with auxiliary material composition 25%, fatty alcohol-polyoxyethylene ether 12.5% and distilled water 62.5% through the synthetic mixture that forms of emulsion reaction, wherein the auxiliary material composition is that 3% the hexadecyltrimethylammonium chloride aqueous solution, percentage by weight are that 2.5% octadecyl dimethyl bromize ammonium solution mixes according to volume ratio at normal temperatures at 1: 1 with percentage by weight.
2. the preparation technology of a hair products curly hair finishing agent as claimed in claim 1 is characterized in that: carry out according to following steps:
1), the choosing of reagent material: with as above two methylols time ethylene ureas and sodium carbonate as Main Ingredients and Appearance, the FeSO with 0.2%
4The mixture of the aqueous solution, 0.01% watery hydrochloric acid is as catalyst, and the mixture of the hexadecyltrimethylammonium chloride aqueous solution with 3%, 2.5% octadecyl dimethyl bromize ammonium solution is as additive, the MgSO with 0.25%
4The mixture of the aqueous solution, 1.0% the hydroxylamine hydrochloride aqueous solution is as activating agent, the mixture of the Sodium Tvlose aqueous solution with 3%, 1.6% the stearic acid aqueous solution is as conditioner, is dispersant with auxiliary material composition 25%, fatty alcohol-polyoxyethylene ether 12.5% and distilled water 62.5% through the synthetic mixture that forms of emulsion reaction, chooses the deionized water that hardness is not more than 0.03 equivalent parts per million;
2), the configuration of reagent solution: described additive joined 1/4 deionized water for stirring and form A solution, the described activating agent with 1/3 slowly joins in the described conditioner, forms B solution;
3) described catalyst is added in two methylol time ethylene ureas, stir and formed C solution in 10 minutes;
4), in 3/4 deionized water, slowly add the C solution stirring 30 minutes, slowly add sodium carbonate limit edged and stir, add A solution after 20 minutes earlier, add B solution then, add remaining 2/3 described activating agent and described dispersant limit edged at last and stir, stir, after 30 minutes, obtain hair products curly hair finish solution, hair products curly hair finish solution is kept in Dark Place, and with blue thick PVC plastic cement barreled, preserve in the darkroom.
3. method of utilizing above-mentioned hair products curly hair finishing agent that hair products are put in order is characterized in that:
1), washing: with shampoo or washing powder washing hair products;
2), removal floating color: add in the 1000ml water with 30ml chlorine, put into above-mentioned hair products, soaked 3 minutes, clean, remove the loose colour on above-mentioned hair products surface;
3), softening: add the hair products curly hair finish solution of 20-30g in 1000ml water, solution temperature is controlled at 75 ℃, above-mentioned hair products is placed on soaked in this solution 20-30 minute again;
4), washing: above-mentioned hair products are cleaned up with shampoo or washing powder;
5), bubble oil: above-mentioned hair products are placed in the oil of 45-60 ℃ of temperature, steeped 20-25 minute, upper plate oven dry then.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101254420A CN101818452B (en) | 2010-03-17 | 2010-03-17 | Curly hair dressing agent for hair products, preparation method and method for dressing hair products |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2010101254420A CN101818452B (en) | 2010-03-17 | 2010-03-17 | Curly hair dressing agent for hair products, preparation method and method for dressing hair products |
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| CN101818452A true CN101818452A (en) | 2010-09-01 |
| CN101818452B CN101818452B (en) | 2012-05-23 |
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| Application Number | Title | Priority Date | Filing Date |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102268815A (en) * | 2011-05-25 | 2011-12-07 | 许昌恒源发制品股份有限公司 | Wig softener and preparation process thereof and method for arranging wig product |
| CN103726337A (en) * | 2013-11-18 | 2014-04-16 | 河南瑞贝卡发制品股份有限公司 | Fibrous curly hair fixing adhesion agent, preparation method and periwig prepared with adhesion agent |
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|---|---|---|---|---|
| CN1411366A (en) * | 1999-12-17 | 2003-04-16 | 荷兰联合利华有限公司 | Hair treatment composition comprising cationic surfactants |
| US20030211064A1 (en) * | 2002-04-22 | 2003-11-13 | The Procter & Gamble Company | Fiber treatment blend |
| EP1894603A1 (en) * | 2006-09-04 | 2008-03-05 | Takasago International Corporation | Encapsulation of bulky fragrance molecules |
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2010
- 2010-03-17 CN CN2010101254420A patent/CN101818452B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1411366A (en) * | 1999-12-17 | 2003-04-16 | 荷兰联合利华有限公司 | Hair treatment composition comprising cationic surfactants |
| US20030211064A1 (en) * | 2002-04-22 | 2003-11-13 | The Procter & Gamble Company | Fiber treatment blend |
| CN1646082A (en) * | 2002-04-22 | 2005-07-27 | 宝洁公司 | Fiber treatment blend |
| EP1894603A1 (en) * | 2006-09-04 | 2008-03-05 | Takasago International Corporation | Encapsulation of bulky fragrance molecules |
Non-Patent Citations (2)
| Title |
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| 《中国洗涤用品工业》 20081231 张华涛 头发护理聚合物的发展趋势 第62－64页 1－3 , 第2期 2 * |
| 《日用化学品科学》 20081031 李世忠等 香波配方技术与头发护理 第26－29页 1－3 第31卷, 第10期 2 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102268815A (en) * | 2011-05-25 | 2011-12-07 | 许昌恒源发制品股份有限公司 | Wig softener and preparation process thereof and method for arranging wig product |
| CN102268815B (en) * | 2011-05-25 | 2012-12-05 | 许昌恒源发制品股份有限公司 | Wig softener and preparation process thereof and method for arranging wig product |
| CN103726337A (en) * | 2013-11-18 | 2014-04-16 | 河南瑞贝卡发制品股份有限公司 | Fibrous curly hair fixing adhesion agent, preparation method and periwig prepared with adhesion agent |
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| CN101818452B (en) | 2012-05-23 |
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