CN103015179A - Method for producing waterproof cotton and nylon blended fabric - Google Patents
Method for producing waterproof cotton and nylon blended fabric Download PDFInfo
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- CN103015179A CN103015179A CN2012104983510A CN201210498351A CN103015179A CN 103015179 A CN103015179 A CN 103015179A CN 2012104983510 A CN2012104983510 A CN 2012104983510A CN 201210498351 A CN201210498351 A CN 201210498351A CN 103015179 A CN103015179 A CN 103015179A
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Abstract
The invention discloses a method for producing a waterproof cotton and nylon blended fabric. The method comprises the steps of adding perfluorooctyl ethyl acrylate, octodecyl methacrylate ester, polyoxyethylene fatty acid ester and a solvent into a reaction kettle in sequence, stirring, gradually raising the temperature to be between 80 and 90 DEG C, dripping a tert-butyl peroxypivalate initiating agent into the reaction kettle to continue to react, and cooling to obtain a mixed emulsion; and mixing the mixed emulsion with water and a crosslinking agent to obtain a finishing solution, performing two-soaking and two-rolling finishing on the cotton and nylon blended fabric, and drying and baking to obtain the waterproof cotton and nylon blended fabric. Therefore, the cotton and nylon blended fabric prepared by the method for producing the waterproof cotton and nylon blended fabric has a good waterproof function, can keep the original color after finishing, has a soft hand feeling, and is refreshing and comfortable to wear; less waste gases and waste materials are generated in the whole production process, so that the pollution to the environment is effectively reduced; and a finishing agent is good in quality, and can improve the quality of the cotton and nylon blended fabric after being used.
Description
Technical field
The present invention relates to the weaving face fabric field, particularly relate to a kind of production method of Waterproof cotton brocade BLENDED FABRIC.
Background technology
Fabric finishing agent refers to before finished product fabric be carried out the reagent that certain specific function of textiles is given in processing and sorting after textiles leaves loom again.According to dividing on the function antiflaming finishing agent is arranged usually, antistatic finishing agent.Sanitary finish agent, the antifouling and classifications such as soil-releasing finishing agent, water-refusing oil-refusing finishing agent.Apply a kind of finishing agent with special chemical molecular structure at fabric, change the composition of fiber surface, and be attached to firmly fiber or be combined with fibre chemistry, make fabric no longer wetting by water and edible oil institute commonly used, such finishing agent is water-refusing oil-refusing finishing agent.
Behind traditional water-refusing oil-refusing finishing agent finish fabric fabric feeling is hardened, process durability inadequate, water and oil repellant DeGrain after use a period of time, it is poor that the people wears gas permeability, comfort is not strong, can not well increase the added value of fabric, and the quality of fabric is reduced.
Summary of the invention
The technical problem that the present invention mainly solves provides a kind of production method of Waterproof cotton brocade BLENDED FABRIC, the water resistance of the cotton bright and beautiful BLENDED FABRIC of energy Effective Raise.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is: a kind of production method of Waterproof cotton brocade BLENDED FABRIC is provided, comprises that step is:
(1) add successively perfluoro capryl ethyl propylene acid esters, octadecyl methyl acrylate, fatty acid polyglycol sun vinyl acetate and solvent in the reactor, stir and be warming up to gradually 80-90 ℃, drip the t-butylperoxy pivarate initator in reactor, continue reaction, cooling obtains mixed emulsion;
(2) mixed emulsion, water and crosslinking agent are mixed to get dressing liquid, the bright and beautiful BLENDED FABRIC of cotton are carried out two soak two and roll arrangement, dry again and cure, obtain the cotton bright and beautiful BLENDED FABRIC of waterproof.
In a preferred embodiment of the present invention, solvent is the dipropylene glycol monomethyl ether described in the step (1).
In a preferred embodiment of the present invention, crosslinking agent is isocyanates described in the step (2).
In a preferred embodiment of the present invention, two to soak two pick-ups that roll be 70-80% described in the step (2).
The invention has the beneficial effects as follows: the production method of Waterproof cotton brocade BLENDED FABRIC of the present invention, the cotton bright and beautiful BLENDED FABRIC that makes has good water-proof function, can keep the original color and luster of cotton bright and beautiful BLENDED FABRIC after the arrangement, soft, wear clearly comfortablely, it is few that whole production process produces waste gas and wastes, effectively reduces the pollution to environment, the finishing agent quality is good, can increase the quality of cotton bright and beautiful BLENDED FABRIC after the use.
The specific embodiment
The below is described in detail preferred embodiment of the present invention, thereby so that advantages and features of the invention can be easier to be it will be appreciated by those skilled in the art that protection scope of the present invention is made more explicit defining.
Embodiment one:
(1) add successively perfluoro capryl ethyl propylene acid esters, octadecyl methyl acrylate, fatty acid polyglycol sun vinyl acetate and dipropylene glycol monomethyl ether in the reactor, stir and be warming up to gradually 80 ℃, in reactor, drip the t-butylperoxy pivarate initator, continue reaction 3 hours, cooling obtains mixed emulsion;
(2) mixed emulsion, water and isocyanates are mixed to get dressing liquid, the bright and beautiful BLENDED FABRIC of cotton are carried out two soak two and roll arrangement, pick-up is 70%, dries and cures, and obtains the cotton bright and beautiful BLENDED FABRIC of waterproof.
Embodiment two:
(1) add successively perfluoro capryl ethyl propylene acid esters, octadecyl methyl acrylate, fatty acid polyglycol sun vinyl acetate and dipropylene glycol monomethyl ether in the reactor, stir and be warming up to gradually 90 ℃, in reactor, drip the t-butylperoxy pivarate initator, continue reaction 3.5 hours, cooling obtains mixed emulsion;
(2) mixed emulsion, water and isocyanates are mixed to get dressing liquid, the bright and beautiful BLENDED FABRIC of cotton are carried out two soak two and roll arrangement, pick-up is 75%, dries and cures, and obtains the cotton bright and beautiful BLENDED FABRIC of waterproof.
Embodiment three:
(1) add successively perfluoro capryl ethyl propylene acid esters, octadecyl methyl acrylate, fatty acid polyglycol sun vinyl acetate and dipropylene glycol monomethyl ether in the reactor, stir and be warming up to gradually 85 ℃, in reactor, drip the t-butylperoxy pivarate initator, continue reaction 4 hours, cooling obtains mixed emulsion;
(2) mixed emulsion, water and isocyanates are mixed to get dressing liquid, the bright and beautiful BLENDED FABRIC of cotton are carried out two soak two and roll arrangement, pick-up is 80%, dries and cures, and obtains the cotton bright and beautiful BLENDED FABRIC of waterproof.
The production method of the Waterproof cotton brocade BLENDED FABRIC that the present invention discloses, the cotton bright and beautiful BLENDED FABRIC that makes has good water-proof function, can keep the original color and luster of cotton bright and beautiful BLENDED FABRIC after the arrangement, soft, wear clearly comfortablely, it is few that whole production process produces waste gas and wastes, effectively reduces the pollution to environment, the finishing agent quality is good, can increase the quality of cotton bright and beautiful BLENDED FABRIC after the use.
The above only is embodiments of the invention; be not so limit claim of the present invention; every equivalent structure or equivalent flow process conversion that utilizes description of the present invention to do; or directly or indirectly be used in other relevant technical fields, all in like manner be included in the scope of patent protection of the present invention.
Claims (4)
1. the production method of a Waterproof cotton brocade BLENDED FABRIC is characterized in that, comprises that step is:
(1) add successively perfluoro capryl ethyl propylene acid esters, octadecyl methyl acrylate, fatty acid polyglycol sun vinyl acetate and solvent in the reactor, stir and be warming up to gradually 80-90 ℃, drip the t-butylperoxy pivarate initator in reactor, continue reaction, cooling obtains mixed emulsion;
(2) mixed emulsion, water and crosslinking agent are mixed to get dressing liquid, the bright and beautiful BLENDED FABRIC of cotton are carried out two soak two and roll arrangement, dry again and cure, obtain the cotton bright and beautiful BLENDED FABRIC of waterproof.
2. the production method of Waterproof cotton brocade BLENDED FABRIC according to claim 1 is characterized in that, solvent is the dipropylene glycol monomethyl ether described in the step (1).
3. the production method of Waterproof cotton brocade BLENDED FABRIC according to claim 1 is characterized in that, crosslinking agent is isocyanates described in the step (2).
4. the production method of Waterproof cotton according to claim 1 brocade BLENDED FABRIC is characterized in that, two to soak two pick-ups that roll be 70-80% described in the step (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104983510A CN103015179A (en) | 2012-11-29 | 2012-11-29 | Method for producing waterproof cotton and nylon blended fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104983510A CN103015179A (en) | 2012-11-29 | 2012-11-29 | Method for producing waterproof cotton and nylon blended fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103015179A true CN103015179A (en) | 2013-04-03 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012104983510A Pending CN103015179A (en) | 2012-11-29 | 2012-11-29 | Method for producing waterproof cotton and nylon blended fabric |
Country Status (1)
| Country | Link |
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| CN (1) | CN103015179A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105085793A (en) * | 2014-05-20 | 2015-11-25 | 东莞市长安东阳光铝业研发有限公司 | Fluorinated textile finishing agent composition and preparation method therefor |
| CN107326674A (en) * | 2017-07-21 | 2017-11-07 | 安徽华锦柏亚纤纺科技有限公司 | A kind of waterproof oil-proof finishing method of polyester-cotton blend woven |
| CN113152087A (en) * | 2021-04-07 | 2021-07-23 | 伊科纳米科技(苏州)有限公司 | Waterproof flame-retardant finishing agent and finishing process of polyester fabric by using same |
| US11326303B2 (en) | 2015-06-05 | 2022-05-10 | Cornell University | Modified cellulosic compositions having increased hydrophobicity and processes for their production |
Citations (5)
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| US3896251A (en) * | 1972-03-06 | 1975-07-22 | Minnesota Mining & Mfg | Outerwear fabric treatment |
| JPH09118877A (en) * | 1995-10-24 | 1997-05-06 | Asahi Glass Co Ltd | Water-dispersing water-and oil-repellent composition having excellent stability against impurity |
| CN1374363A (en) * | 2001-03-05 | 2002-10-16 | 旭硝子株式会社 | Water-dispersible water-proof & oil-proof agent composition and finishing agent |
| CN1882622A (en) * | 2003-11-18 | 2006-12-20 | 纳幕尔杜邦公司 | Fluorine efficient finishes for textiles |
| CN101016696A (en) * | 2007-02-15 | 2007-08-15 | 浙江工业大学 | Method of preparing fluorine-containing hydrophobic and oil repellent fabric finishing agent |
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2012
- 2012-11-29 CN CN2012104983510A patent/CN103015179A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3896251A (en) * | 1972-03-06 | 1975-07-22 | Minnesota Mining & Mfg | Outerwear fabric treatment |
| JPH09118877A (en) * | 1995-10-24 | 1997-05-06 | Asahi Glass Co Ltd | Water-dispersing water-and oil-repellent composition having excellent stability against impurity |
| CN1374363A (en) * | 2001-03-05 | 2002-10-16 | 旭硝子株式会社 | Water-dispersible water-proof & oil-proof agent composition and finishing agent |
| CN1882622A (en) * | 2003-11-18 | 2006-12-20 | 纳幕尔杜邦公司 | Fluorine efficient finishes for textiles |
| CN101016696A (en) * | 2007-02-15 | 2007-08-15 | 浙江工业大学 | Method of preparing fluorine-containing hydrophobic and oil repellent fabric finishing agent |
Non-Patent Citations (3)
| Title |
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| MASAMICHI MORITA等: "Surface Properties of Perfluoroalkylethyl Acrylate/n-Alkyl Acrylate Copolymers", 《JOURNAL OF APPLIED POLYMER SCIENCE》 * |
| 王薇等: "含氟整理剂WR-1在锦纶织物上的应用", 《印染》 * |
| 陈荣圻: "纺织品全氟防水拒油易去污整理剂及其安全性", 《针织工业》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105085793A (en) * | 2014-05-20 | 2015-11-25 | 东莞市长安东阳光铝业研发有限公司 | Fluorinated textile finishing agent composition and preparation method therefor |
| CN105085793B (en) * | 2014-05-20 | 2019-06-25 | 东莞东阳光科研发有限公司 | A kind of fluorine-containing textile finishing agent composition and preparation method thereof |
| US11326303B2 (en) | 2015-06-05 | 2022-05-10 | Cornell University | Modified cellulosic compositions having increased hydrophobicity and processes for their production |
| US11913164B2 (en) | 2015-06-05 | 2024-02-27 | Cornell University | Modified cellulosic compositions having increased hydrophobicity and processes for their production |
| CN107326674A (en) * | 2017-07-21 | 2017-11-07 | 安徽华锦柏亚纤纺科技有限公司 | A kind of waterproof oil-proof finishing method of polyester-cotton blend woven |
| CN113152087A (en) * | 2021-04-07 | 2021-07-23 | 伊科纳米科技(苏州)有限公司 | Waterproof flame-retardant finishing agent and finishing process of polyester fabric by using same |
| CN113152087B (en) * | 2021-04-07 | 2023-08-04 | 伊科纳米科技(苏州)有限公司 | Waterproof flame-retardant finishing agent and finishing process for polyester fabric by using same |
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Application publication date: 20130403 |