CN103705630A - Compound donkey-hide gelatin pulp with functions of nourishing yin and supplementing blood and preparation process thereof - Google Patents
Compound donkey-hide gelatin pulp with functions of nourishing yin and supplementing blood and preparation process thereof Download PDFInfo
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- CN103705630A CN103705630A CN201410019999.4A CN201410019999A CN103705630A CN 103705630 A CN103705630 A CN 103705630A CN 201410019999 A CN201410019999 A CN 201410019999A CN 103705630 A CN103705630 A CN 103705630A
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Abstract
The invention relates to a compound donkey-hide gelatin pulp with functions of nourishing yin and supplementing blood and a preparation process thereof. No compound donkey-hide gelatin pulp which has the functions of nourishing yin and supplementing blood and can be used for treating nosebleed exists in the prior art. The compound donkey-hide gelatin pulp with functions of nourishing yin and supplementing blood is prepared from the following raw materials of 125-130 parts by weight of donkey-hide gelatin, 30-50 parts by weight of momordica grosvenori, 380-390 parts by weight of prepared rehmannia root, 430-450 parts by weight of scaphium scaphigerum, 160-165 parts by weight of hawthorn, 130-150 parts by weight of saccharose and 125-130 parts by weight of platycodon grandiflorum. The compound donkey-hide gelatin pulp with functions of nourishing yin and supplementing blood, provided by the invention, contains precious Chinese medicinal herbs such as the donkey-hide gelatin and the momordica grosvenori, has the functions of nourishing yin and supplementing blood, can be used for treating nosebleed, and is suitable for being taken by multiple kinds of crowds.
Description
Technical field
The present invention relates to a kind of nourishing YIN and supplementing blood FUFANG EJIAO JIANG and preparation technology thereof.
Background technology
Colla Corii Asini is a kind of famous and precious blood tonic, and always well-known doctor has the greatest esteem, but takes the first molten of front needs, then takes, very inconvenient.FUFANG EJIAO JIANG is a kind of bottled oral liquid of Donga Colla Corii Asini company limited exploitation, taking convenience, and the successful of enriching blood, does not also have YIN nourishing, enriches blood in prior art, and can be used to treat the ass glue oral liquid of blood nosebleed.
Summary of the invention
The technical problem to be solved in the present invention is the above-mentioned defect that how to overcome prior art, a kind of YIN nourishing is provided, enriches blood, and can be used to treat nourishing YIN and supplementing blood FUFANG EJIAO JIANG and the preparation technology thereof of blood nosebleed.
For solving the problems of the technologies described above, its raw material of this nourishing YIN and supplementing blood FUFANG EJIAO JIANG comprise the Colla Corii Asini of 125-130 weight portion, the Fructus Momordicae of the Radix Ginseng of 55-65 weight portion, 30-50 weight portion, the Radix Rehmanniae Preparata of the Semen Sterculiae Lychnophorae of 430-450 weight portion, 380-390 weight portion, the sucrose of the Fructus Crataegi of 160-165 weight portion and 130-150 weight portion.
The preparation technology of this nourishing YIN and supplementing blood FUFANG EJIAO JIANG, comprises the steps:
1.. take the Radix Ginseng of 55-65 weight portion, after section, immerse 45% ethanol of 60~80 weight portions, then add in high pressure alcohol extraction tank, then by air pump to inflating pressure 8~10kgf/cm in high pressure alcohol extraction tank
2, soak 2 hours; Its mesohigh alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforementioned weight ratio, take the Fructus Momordicae of 30-50 weight portion, the Semen Sterculiae Lychnophorae of 430-450 weight portion, the Radix Rehmanniae Preparata of 410-430 weight portion, the Radix Codonopsis of 410-430 weight portion, the Fructus Crataegi of 170-190 weight portion, add in the tank body of new medicine extractor, then add 5000 kilograms, water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high pressure alcohol extraction tank is put into fast to the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, emit medicine juice for the first time, stand-by,
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high pressure alcohol extraction pot bottom communicates with tank body by baiting valve;
3.. then add for the second time 3000 kilograms, water, heated and boiled, is greater than at 1.01 o'clock to medicine juice proportion, emits medicine juice for the second time, stand-by;
4.. then add for the third time 1800 kilograms, water, heated and boiled, after reaching more than 1.005, emits medicine juice for the third time to medicine juice proportion;
5.. three medicine juice are squeezed into seperator together with pump and carry out separation, obtain hybrid separation liquid, separated front medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid is sucked in triple effect evaporator and evaporated by vacuum, after being evaporated to medicine juice proportion and reaching between 1.05-1.06, emit stand-byly, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 weight portion and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirred, make it to dissolve into after uniform glue, with foam, turn glue foam and impurity defecation, then add the sucrose of 110-130 weight portion to dissolve completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. by, 6. walk gained medicine juice and and 7. walk gained gum sugar liquid, with pump, squeeze in the settling box with heating function, slowly add sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, standing more than 16 hours, then the mixed liquor after precipitation is carried out to separation with seperator, every 30 minutes deslagginves are once, after mixed liquor separation, enter turnover barrel, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 ℃ are boiled 15 minutes; Finally medicine juice is squeezed in the finished product liquid receiver with 100 mesh sieves with pump, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
So design, people participates in ethanol and puts into together after high pressure alcohol extraction tank, under High Pressure, ethanol fully infiltrates in each cell of Radix Ginseng, after adding fast in the tank body of new medicine extractor, pressure reduces suddenly, meets again the medicine juice of high temperature, ethanol in ginseng-cell breaks through ginseng-cell wall, and effective ingredient in Radix Ginseng, Radix Scrophulariae is brought in medicine juice.
As optimization, the when 9. step is concentrated, by vacuum, by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
As optimization, the when 9. step is concentrated, adopts film condensing device, concentrates, by the clear water of film condensing device, give over to 2., 3., 4. step adds water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product FUFANG EJIAO JIANG.
As optimization, the 1. step: 45% ethanol of 60~80 weight portions is immersed in Radix Ginseng section, pulls out after 2 hours, puts into screw extruder extruding, then juice is put back to together with residue in ethanol, finally adds together in high pressure alcohol extraction tank again.
Nourishing YIN and supplementing blood FUFANG EJIAO JIANG of the present invention contains the rare Chinese medicines such as Colla Corii Asini, Fructus Momordicae, has YIN nourishing, enriches blood, and can be used to treat blood nosebleed, is applicable to multiple crowd and takes.
Accompanying drawing explanation
The equipment of the present invention being used below in conjunction with accompanying drawing is described further:
Fig. 1 is the structural representation of high pressure alcohol extraction tank and new medicine extractor.
Fig. 2 is the schematic diagram that utilizes film condensing device concentrated medicament.
In figure: 1 be high pressure alcohol extraction tank, 2 for visor, 3 for closed charging aperture, 4 for Pressure gauge, 5 for intake valve, 6 for tank body, 7 for condenser, 8 for vapour jacket, 9 for slag notch, 10 for baiting valve, 11 for film condensing device, 12 for medicine juice feed pipe, 13 for medicine juice discharge nozzle after concentrated, 14 for outlet pipe, 15 be piston pump.
The specific embodiment
Embodiment one: 1.. take the Radix Ginseng of 55kg, after section, immerse 45% ethanol (being that volumetric concentration is 45% ethanol water) of 60kg, then add in high pressure alcohol extraction tank, then by air pump to inflating pressure 8~10kgf/cm in high pressure alcohol extraction tank
2, soak 2 hours; Its mesohigh alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforementioned weight ratio, take the Fructus Momordicae of 30kg, the Radix Rehmanniae Preparata of the Semen Sterculiae Lychnophorae of 440kg, 410kg, the Fructus Crataegi of the Radix Codonopsis of 420kg, 190kg, add in the tank body of new medicine extractor, then add 5000 kilograms, water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, then the material in high pressure alcohol extraction tank is put into fast to the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, emit medicine juice for the first time, stand-by;
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high pressure alcohol extraction pot bottom communicates with tank body by baiting valve;
3.. then add for the second time 3000 kilograms, water, heated and boiled, is greater than at 1.01 o'clock to medicine juice proportion, emits medicine juice for the second time, stand-by;
4.. then add for the third time 1800 kilograms, water, heated and boiled, after reaching more than 1.005, emits medicine juice for the third time to medicine juice proportion;
5.. three medicine juice are squeezed into seperator together with pump and carry out separation, obtain hybrid separation liquid, separated front medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid is sucked in triple effect evaporator and evaporated by vacuum, after being evaporated to medicine juice proportion and reaching between 1.05-1.06, emit stand-byly, obtain medicine juice;
7.. get the Colla Corii Asini of 125kg and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirred, make it to dissolve into after uniform glue, with foam, turn glue foam and impurity defecation, then add the sucrose of 120kg to dissolve completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. by, 6. walk gained medicine juice and and 7. walk gained gum sugar liquid, with pump, squeeze in the settling box with heating function, slowly add sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, standing more than 16 hours, then the mixed liquor after precipitation is carried out to separation with seperator, every 30 minutes deslagginves are once, after mixed liquor separation, enter turnover barrel, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 ℃ are boiled 15 minutes; Finally medicine juice is squeezed in the finished product liquid receiver with 100 mesh sieves with pump, covered and enclosed, is no more than 6 hours standing time, fill, and sterilizing obtains nourishing YIN and supplementing blood FUFANG EJIAO JIANG A.
Embodiment 2: raw material is changed into: 45% ethanol of the Colla Corii Asini of 127.5kg, 70kg, the Radix Ginseng of 60kg, the Semen Sterculiae Lychnophorae of the Fructus Momordicae of 40kg, 450kg, the Radix Codonopsis of the Radix Rehmanniae Preparata of 420kg, 430kg, the sucrose of the Fructus Crataegi of 170kg and 130kg, the when 9. step is concentrated, adopt film condensing device, concentrate, as shown in Figure 2, by the clear water of film condensing device 11, give over to 2., 3., 4. to walk and add water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product nourishing YIN and supplementing blood FUFANG EJIAO JIANG B, all the other techniques as described in Example 1, are omited.
Embodiment 3: raw material is changed into: 45% ethanol of the Colla Corii Asini of 130kg, 80kg, the Radix Ginseng of 65kg, the Semen Sterculiae Lychnophorae of the Fructus Momordicae of 50kg, 430kg,, the Radix Rehmanniae Preparata of 430kg is, the Fructus Crataegi of the Radix Codonopsis of 410kg, 180kg and the sucrose of 110kg, the the 1. step: 45% ethanol that 60~80 amounts parts are immersed in Radix Ginseng section was pulled out after 2 hours, put into the extruding of screw extruder (not shown), then juice is put back in ethanol together with residue, finally add together again in high pressure alcohol extraction tank 1, all the other techniques as described in Example 1, make nourishing YIN and supplementing blood FUFANG EJIAO JIANG C.
Contrast experiment 1: choose same batch of ginseng raw material, be divided into four groups, press respectively technique and the conventional preparation technology's production of FUFANG EJIAO JIANG FUFANG EJIAO JIANG described in embodiment 1,2,3, produce respectively Radix Ginseng residue A, Radix Ginseng residue B, Radix Ginseng residue C, Radix Ginseng residue D.Detect respectively ginsenoside (Ginsenoside) total content in above-mentioned four kinds of Radix Ginseng residues, obtain following table
Certain man, 39 years old, shortness of breath and palpitation, dizziness and blurred vision, the mental status were poor, all can go out weekly the more than situation of epistaxis one to twice, pale complexion, morning, noon and afternoon every day are half an hour after meal, takes respectively this nourishing YIN and supplementing blood of 10ml FUFANG EJIAO JIANG C, after three months, epistaxis phenomenon disappears, and after half a year, complexion is day by day ruddy, breathe day by day smooth and easyly, simultaneously sleep quality is good.
Certain female, 23 years old, have an old and weathered face, the few tongue of red tongue, cough ant phlegm, morning, noon and afternoon every day are half an hour after meal, takes respectively this nourishing YIN and supplementing blood of 10ml FUFANG EJIAO JIANG A, after half a year color gradually ruddy, phlegm syndrome disappear.
Certain man, 34 years old, dry mouth and throat, urine yellowish urine, defecates dry and astringent, has constipation symptom, and morning, noon and afternoon every day are half an hour after meal, takes respectively this nourishing YIN and supplementing blood of 10ml FUFANG EJIAO JIANG A, and dispute is salubrious, and urine is clear, and stool is smooth, and constipation disappears.
Claims (5)
1. a nourishing YIN and supplementing blood FUFANG EJIAO JIANG, is characterized in that: its raw material comprise the Colla Corii Asini of 125-130 weight portion, the Fructus Momordicae of the Radix Ginseng of 55-65 weight portion, 30-50 weight portion, the Radix Rehmanniae Preparata of the Semen Sterculiae Lychnophorae of 430-450 weight portion, 380-390 weight portion, the sucrose of the Fructus Crataegi of 160-165 weight portion and 130-150 weight portion.
2. the preparation technology of nourishing YIN and supplementing blood FUFANG EJIAO JIANG described in claim 1, comprises the steps:
1.. take the Radix Ginseng of 55-65 weight portion, after section, immerse 45% ethanol of 60~80 weight portions, then add in high pressure alcohol extraction tank, then by air pump to inflating pressure 8~10kgf/cm in high pressure alcohol extraction tank
2, soak 2 hours; Its mesohigh alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforementioned weight ratio, take the Fructus Momordicae of 30-50 weight portion, the Semen Sterculiae Lychnophorae of 430-450 weight portion, the Radix Rehmanniae Preparata of 410-430 weight portion, the Radix Codonopsis of 410-430 weight portion, the Fructus Crataegi of 170-190 weight portion, add in the tank body of new medicine extractor, then add 5000 kilograms, water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high pressure alcohol extraction tank is put into fast to the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, emit medicine juice for the first time, stand-by,
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high pressure alcohol extraction pot bottom communicates with tank body by baiting valve;
3.. then add for the second time 3000 kilograms, water, heated and boiled, is greater than at 1.01 o'clock to medicine juice proportion, emits medicine juice for the second time, stand-by;
4.. then add for the third time 1800 kilograms, water, heated and boiled, after reaching more than 1.005, emits medicine juice for the third time to medicine juice proportion;
5.. three medicine juice are squeezed into seperator together with pump and carry out separation, obtain hybrid separation liquid, separated front medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid is sucked in triple effect evaporator and evaporated by vacuum, after being evaporated to medicine juice proportion and reaching between 1.05-1.06, emit stand-byly, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 weight portion and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirred, make it to dissolve into after uniform glue, with foam, turn glue foam and impurity defecation, then add the sucrose of 110-130 weight portion to dissolve completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. by, 6. walk gained medicine juice and and 7. walk gained gum sugar liquid, with pump, squeeze in the settling box with heating function, slowly add sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, standing more than 16 hours, then the mixed liquor after precipitation is carried out to separation with seperator, every 30 minutes deslagginves are once, after mixed liquor separation, enter turnover barrel, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 ℃ are boiled 15 minutes; Finally medicine juice is squeezed in the finished product liquid receiver with 100 mesh sieves with pump, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
3. the preparation technology of nourishing YIN and supplementing blood FUFANG EJIAO JIANG according to claim 2, is characterized in that: the when 9. step is concentrated, by vacuum, by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
4. the preparation technology of nourishing YIN and supplementing blood FUFANG EJIAO JIANG according to claim 2, it is characterized in that: the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step adds water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product FUFANG EJIAO JIANG.
5. according to the preparation technology of nourishing YIN and supplementing blood FUFANG EJIAO JIANG described in claim 2 or 3 or 4, it is characterized in that: the 1. step: 45% ethanol of 60~80 weight portions is immersed in Radix Ginseng section, after 2 hours, pull out, put into screw extruder extruding, then juice is put back to together with residue in ethanol, finally added together again in high pressure alcohol extraction tank.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1112807A (en) * | 1994-11-28 | 1995-12-06 | 蒋松林 | Medicinal diet health-care tea |
CN1446488A (en) * | 2003-03-21 | 2003-10-08 | 付舟山 | Muyu stone beverage and its preparation method |
CN1919036A (en) * | 2005-05-23 | 2007-02-28 | 吴跃飞 | Green health care animal foodstuff produced by living animal bioreactor and producing method thereof |
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1112807A (en) * | 1994-11-28 | 1995-12-06 | 蒋松林 | Medicinal diet health-care tea |
CN1446488A (en) * | 2003-03-21 | 2003-10-08 | 付舟山 | Muyu stone beverage and its preparation method |
CN1919036A (en) * | 2005-05-23 | 2007-02-28 | 吴跃飞 | Green health care animal foodstuff produced by living animal bioreactor and producing method thereof |
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