CN103698190A - Dip dyeing method for preparation of concrete microanalysis sample under normal temperature and pressure - Google Patents
Dip dyeing method for preparation of concrete microanalysis sample under normal temperature and pressure Download PDFInfo
- Publication number
- CN103698190A CN103698190A CN201210470819.5A CN201210470819A CN103698190A CN 103698190 A CN103698190 A CN 103698190A CN 201210470819 A CN201210470819 A CN 201210470819A CN 103698190 A CN103698190 A CN 103698190A
- Authority
- CN
- China
- Prior art keywords
- concrete
- dip dyeing
- sample
- fluorescence
- micro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Landscapes
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
The invention discloses a dip dyeing method for preparation of a concrete microanalysis sample under normal temperature and pressure, and the method can perform dip dyeing on a concrete microstructure (microcracks and air holes) under ordinary laboratory conditions. The method includes: firstly soaking a concrete slice sample in a fluorescence liquid solution, then daubing another fluorescence liquid material that can harden and consolidate in microcracks and air holes on the sample surface uniformly, thus finishing dip dyeing. The method disclosed by the invention is simple to operate, and has no need for heating, vacuum pumping or high pressure applying and other relevant devices or equipment. While strengthening the contrast of the microstructure and the matrix in a concrete fluorescence microscopic image, the method maximumly avoids interference to the original microstructure of concrete during dip dyeing, and improves the reliability of microanalysis results.
Description
Technical field
The present invention relates to prepare under a kind of normal temperature and pressure the dip dyeing method of concrete micro-analysis sample, can under the condition of conventional test chamber, to concrete microstructure (micro-crack and pore), carry out dip dyeing, in strengthening concrete fluorescence microscope images in micromechanism and matrix contrast, avoided to greatest extent the interference to the original micromechanism of concrete in dip dyeing process, improve micro-analysis reliability of structure, be specially adapted to the automatic measuring fractional analysis that utilizes digital image-processing methods to carry out concrete micro-image.
Background technology
Concrete physico mechanical characteristic and the permanance microstructure characteristic (micro-crack and pore) inner with it is inseparable, so concrete micro-analysis technology is research emphasis and the difficult point of concrete field.Because the contrast of micro-crack, pore and the matrix of inside concrete is not high, so in micro-analysis, need concrete to carry out dip dyeing, to strengthen the contrast of micro-crack in micro-image, pore and matrix, be convenient to identification and the quantitative analysis of micromechanism.Vacuum fluorescence epoxy impregnation method is current comparatively conventional dip dyeing method, but utilize the method in sample making course, to need concrete sample to carry out heat drying, vacuumize or apply HIGH PRESSURE TREATMENT, therefore testing laboratory's relevant device is had relatively high expectations, also easily cause the generation of inside concrete secondary micro-crack, the observation and analysis of impact to original flaw shape state in sample simultaneously.How simplifying dip dyeing process and reducing dip dyeing process is the study hotspot of researcher to the interference of inner microstructure always.
Summary of the invention
For solving the problems of the technologies described above, the present invention proposes to prepare under a kind of normal temperature and pressure the dip dyeing method of concrete micro-analysis sample, can simplify dip dyeing process and reduce the interference of dip dyeing process to inner microstructure.
The present invention is simple to operate, does not need concrete to carry out heat drying, vacuumize or apply HIGH PRESSURE TREATMENT, has reduced to greatest extent the artificial interference to sample in dip dyeing process, has improved the reliability of Micro-Structure Analysis result.
Accompanying drawing explanation
Fig. 1 is by the inventive method gained concrete section micro-image one.
Fig. 2 is by the inventive method gained concrete section micro-image two.
Wherein:
1 micro-crack, 2,3 bubbles.
Embodiment
The dip dyeing method of preparing concrete micro-analysis sample under a kind of normal temperature and pressure of the present invention, comprises two steps below:
The first step, concrete section sample is placed in a kind of fluorescence liquid solution and soaks;
Second step, takes out this concrete section sample, and the concrete section sample surfaces after immersion is evenly smeared the fluorescence fluent material that one deck can harden fixed in micro-crack and pore.
The first step is soaked concrete section sample fluorescence liquid solution used and is configured and form according to a certain percentage by fluorescent dye and water-soluble liquid, due to the mutual solubility with water, in immersion process, fluorescence liquid solution cements out the free water in concrete substrate be filled in pore and micro-crack.The described fluorescence liquid solution that is used for soaking concrete sample can be also the solution being formed by fluorescent dye and alcohol configuration
In second step, smear fluorescence fluent material and also inner fluorescent dye material is played to the effect of sealing up for safekeeping when filling surface pores.This fluorescence fluent material is fluorescent polymer.Preferably, this fluorescence fluent material is the fluorescence epoxy resin being comprised of epoxy resin, rigidizer and fluorescent dye.
In the dip dyeing process of above-mentioned whole concrete section sample, all under the condition of conventional test chamber, carry out, do not need concrete section sample to carry out heat drying, vacuumize or apply high pressure.
A specific embodiment of the inventive method is:
Cut out the thick square of 20mm section (length of side 10cm) living through deteriorated concrete (concrete test block in this example had born the compressive load that is subject to that is equivalent to its compressive strength 70%) inside, after polishing, cleaning, be soaked in the closed container that fills fluorescence liquid solution (fluorescent dye and alcohol are formed for 1:99～1:9 mixed preparing by volume) 3～7 days; Taking out section dries at room temperature until alcohol volatilizees completely; On the sightingpiston of sample, coat the fluorescence epoxy resin of skim 0.1% concentration (quality of fluorescent dye and epoxy resin is 1:1000); After epoxy cure, the slice surface of polishing is gently removed unnecessary epoxy.Section after polishing is placed under fluorescent microscope and is observed, and the fluorescence microscopy picture of gained is shown in Fig. 1 and Fig. 2 (being 40 times of enlargement factors), by Fig. 1 and Fig. 2, can clearly see micro-crack 1 and the pore 2,3 in concrete.In Fig. 1, white stria is micro-crack 1, containing two white stripes of different in width.In Fig. 2, white stria is micro-crack 1, and white circular spot is bubble 2,3.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of making within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (9)
1. a dip dyeing method of preparing concrete micro-analysis sample under normal temperature and pressure, is characterized in that comprising two steps below:
The first step, is placed in the concrete sample of cutting into slices a kind of fluorescence liquid solution and soaks;
Second step, takes out this concrete section sample, and this concrete section sample surfaces after immersion is evenly smeared the fluorescence fluent material that one deck can harden fixed in micro-crack and pore.
2. under normal temperature and pressure as claimed in claim 1, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that it is the solution being formed by fluorescent dye and water-soluble liquid configuration that the fluorescence liquid solution of concrete sample is soaked in described being used for.
3. under normal temperature and pressure as claimed in claim 1, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that it is the solution being formed by fluorescent dye and alcohol configuration that the fluorescence liquid solution of concrete sample is soaked in described being used for.
4. under normal temperature and pressure as claimed in claim 3, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that described fluorescence liquid solution forms fluorescent dye and alcohol by volume for 1:99 to 1:9 mixed preparing.
5. under normal temperature and pressure as claimed in claim 1, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that the described fluorescence fluent material that can harden fixed is fluorescent polymer in micro-crack and pore.
6. under normal temperature and pressure as claimed in claim 1, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that the fluorescence epoxy resin of the described fluorescence fluent material that can harden fixed for being formed by epoxy resin, rigidizer and fluorescent dye in micro-crack and pore.
7. under normal temperature and pressure as claimed in claim 6, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that, in described fluorescence epoxy resin, the mass ratio of fluorescent dye and epoxy resin is 1:1000.
8. under normal temperature and pressure as claimed in claim 1, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that all under the condition of conventional test chamber, carrying out in the dip dyeing process of whole concrete section sample, do not need concrete section sample to carry out heat drying, vacuumize or apply high pressure.
9. under normal temperature and pressure as claimed in claim 1, prepare the dip dyeing method of concrete micro-analysis sample, it is characterized in that:
In the first step, the sample of concrete being cut into slices is placed in the closed container 3～7 days that fills described fluorescence liquid solution; Described fluorescence liquid solution forms fluorescent dye and alcohol by volume for 1:99～1:9 mixed preparing;
In second step, take out this concrete section sample, dry at room temperature until alcohol volatilizees completely, this concrete section sample surfaces after immersion is evenly smeared fluorescence fluent material described in one deck; Described fluorescence fluent material is the fluorescence epoxy resin being comprised of epoxy resin, rigidizer and fluorescent dye; In described fluorescence epoxy resin, the mass ratio of fluorescent dye and epoxy resin is 1:1000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210470819.5A CN103698190A (en) | 2012-11-20 | 2012-11-20 | Dip dyeing method for preparation of concrete microanalysis sample under normal temperature and pressure |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210470819.5A CN103698190A (en) | 2012-11-20 | 2012-11-20 | Dip dyeing method for preparation of concrete microanalysis sample under normal temperature and pressure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103698190A true CN103698190A (en) | 2014-04-02 |
Family
ID=50359794
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210470819.5A Pending CN103698190A (en) | 2012-11-20 | 2012-11-20 | Dip dyeing method for preparation of concrete microanalysis sample under normal temperature and pressure |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103698190A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108254294A (en) * | 2018-03-26 | 2018-07-06 | 杭州培聚教育科技有限公司 | The visualization of cement-based material crack water absorption course and water absorption rate measuring device and method |
| CN111751188A (en) * | 2020-07-08 | 2020-10-09 | 郑州大学 | Macroscopic fracture mechanical analysis method for large-mixing-amount rubber concrete |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0196541A (en) * | 1987-10-08 | 1989-04-14 | Toagosei Chem Ind Co Ltd | Crack detecting agent |
| US20020187274A1 (en) * | 2001-06-11 | 2002-12-12 | Parviz Soroushian | Preparation of concrete samples for microscopic analysis |
| JP2004264233A (en) * | 2003-03-04 | 2004-09-24 | Mitsubishi Paper Mills Ltd | Method for visualizing crack in concrete member |
-
2012
- 2012-11-20 CN CN201210470819.5A patent/CN103698190A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0196541A (en) * | 1987-10-08 | 1989-04-14 | Toagosei Chem Ind Co Ltd | Crack detecting agent |
| JP2551033B2 (en) * | 1987-10-08 | 1996-11-06 | 東亞合成株式会社 | Crack detection agent |
| US20020187274A1 (en) * | 2001-06-11 | 2002-12-12 | Parviz Soroushian | Preparation of concrete samples for microscopic analysis |
| JP2004264233A (en) * | 2003-03-04 | 2004-09-24 | Mitsubishi Paper Mills Ltd | Method for visualizing crack in concrete member |
Non-Patent Citations (1)
| Title |
|---|
| H. HORNAIN等: "《MICROSCOPIC OBSERVATION OF CRACKS IN CONCRETE - A NEW SAMPLE PREPARATION TECHNIQUE USING DYE IMPREGNATION》", 《CEMENT AND CONCRETE RESEARCH》, vol. 26, no. 4, 31 December 1996 (1996-12-31), pages 576 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108254294A (en) * | 2018-03-26 | 2018-07-06 | 杭州培聚教育科技有限公司 | The visualization of cement-based material crack water absorption course and water absorption rate measuring device and method |
| CN108254294B (en) * | 2018-03-26 | 2024-05-10 | 杭州科以才成科技有限公司 | Device and method for visualization and water absorption rate measurement of crack water absorption process of cement-based material |
| CN111751188A (en) * | 2020-07-08 | 2020-10-09 | 郑州大学 | Macroscopic fracture mechanical analysis method for large-mixing-amount rubber concrete |
| CN111751188B (en) * | 2020-07-08 | 2023-01-10 | 郑州大学 | Macroscopic fracture mechanical analysis method for large-mixing-amount rubber concrete |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103063498B (en) | Prepare the two benches vacuum impregnation colouring method of concrete micro-analysis sample | |
| CN103940648B (en) | The preparation method of fish gill tissue paraffin section | |
| CN103822922B (en) | The quick method for determining mortar/aggregate area fraction in concrete section | |
| CN104977202A (en) | Preparation method of transmission electron microscope sample of paraffin-embedded section tissue | |
| CN103698190A (en) | Dip dyeing method for preparation of concrete microanalysis sample under normal temperature and pressure | |
| CN109187118A (en) | Hard tissue pathological section unfolding method and device | |
| CN104502619A (en) | Preparation method and using method of hydrophilic adhesive glass slide | |
| CN103698507B (en) | Detachable and sealed space glass slide incubator | |
| CN103743612B (en) | Detachably, the microslide couveuse of volume adjustable and airtight space | |
| CN110926907A (en) | Method suitable for making equine animal ovary paraffin section | |
| CN108844796A (en) | A kind of blade paraffin section method | |
| RU2499242C2 (en) | Method for preparing biological tissue samples for histopathological examinations | |
| CN104698163B (en) | The using method of the detachable also microslide couveuse of volume adjustable | |
| WO2017047617A1 (en) | Cell-holding substrate holder for preparing observation specimen, kit including same, and observation specimen preparation method | |
| CN106813962B (en) | A kind of production method that zooplankter liquid-based seals sample processed | |
| CN112945657B (en) | Pretreatment device and method for preparing plant material paraffin section | |
| CN104048868A (en) | Zooplankton microscopic slide specimen preparation method | |
| CN108844822A (en) | A method of for detecting chopped strand alkaline resistance properties | |
| CN101949805A (en) | Method for testing physical and mechanical properties of acid contaminated soil | |
| CN104374618A (en) | Plant chromosome tablet observation method | |
| CN107621483A (en) | A kind of method of testing of micro concrete hole solution pH value | |
| CN104833562A (en) | Rapid manufacturing method for rock casting body slice | |
| CN208297220U (en) | A kind of chopped bundle accelerated ageing sample producing device | |
| JP4797167B2 (en) | Embedding cassette | |
| CN106989973B (en) | A method of preparing histotomy |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140402 |