CN103668985A - Ultraviolet-resistant three-proofing finishing agent - Google Patents
Ultraviolet-resistant three-proofing finishing agent Download PDFInfo
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- CN103668985A CN103668985A CN201310610487.0A CN201310610487A CN103668985A CN 103668985 A CN103668985 A CN 103668985A CN 201310610487 A CN201310610487 A CN 201310610487A CN 103668985 A CN103668985 A CN 103668985A
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Abstract
The invention relates to an ultraviolet-resistant three-proofing finishing agent and belongs to the technical field of textile auxiliaries. The ultraviolet-resistant three-proofing finishing agent comprises the following components in parts by weight: 12-16 parts of fluorocarbon emulsion, 8-12 parts of trifluoropropylmethylcyclotrisiloxane, 2-5 parts of a coupling agent, 1-3 parts of citric acid, 4-7 parts of 2-hydroxyl-4-methoxybenzophenone, 2-5 parts of bis-(2,2,6,6-tetramethyl-4-piperidyl)sebate, 3-5 parts of fat acid polyethenoxy ester and 120-150 parts of deionized water. The system of the ultraviolet-resistant three-proofing finishing agent provided by the invention is stable, and the ultraviolet-resistant three-proofing finishing agent not only has good water-proofing, oil-proofing and fouling-proofing functions, but also has a good ultraviolet-resisting function, and is easy to popularize and apply; a fabric finished by the ultraviolet-resistant three-proofing finishing agent touches better.
Description
Technical field
The invention belongs to textile auxiliary technical field, be specifically related to a kind of uvioresistant three-proof finishing agent.
Background technology
Three-proof finishing agent is a kind of fabric that is applicable to the fabrics such as cotton, hair, silk, chemical fibre and blend fibre, gives the spinning post-finishing agent that it has super water and oil repellant and anti-pollution function.So-called three prevent being waterproof, grease proofing and antifouling.Fabric feeling after traditional three-proof finishing agent arranges is stiff, and does not have anti-ultraviolet function.Therefore how overcoming the deficiencies in the prior art is problems that current textile auxiliary technical field is needed solution badly.
Summary of the invention
The object of the invention is, in order to solve the deficiencies in the prior art, provides a kind of uvioresistant three-proof finishing agent, and this finishing agent not only has good waterproof, grease proofing and anti-pollution function, also has uvioresistant effect.
The technical solution used in the present invention is as follows:
A kind of uvioresistant three-proof finishing agent, comprise the following component according to parts by weight meter: 4 ~ 7 parts of 12 ~ 16 parts of fluorine carbon emulsions, 8 ~ 12 parts of trifluoro propyl methyl cyclotrisiloxane, 2 ~ 5 parts of coupling agents, 1 ~ 3 part of citric acid, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) 2 ~ 5 parts of sebacates, 3 ~ 5 parts of polyoxyethylene carboxylates, 120 ~ 150 parts of deionized waters.
Further preferably described coupling agent is silane coupler.
Further preferably described silane coupler is γ-(2,3-epoxy the third oxygen) propyl trimethoxy silicane.
The preparation method of above-mentioned uvioresistant three-proof finishing agent is by deionized water, fluorine carbon emulsion, trifluoro propyl methyl cyclotrisiloxane, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) sebacate and coupling agent be placed in stirrer for mixing evenly after, add again polyoxyethylene carboxylate and citric acid, continue to be stirred to and mix, obtain uvioresistant three-proof finishing agent of the present invention.
compared with prior art, its beneficial effect is in the present invention:uvioresistant finishing agent stable system of the present invention, not only has good waterproof, grease proofing and anti-pollution function, also has good anti-ultraviolet function, and the fabric feeling after arrangement is better, is easy to apply.
Specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
A kind of uvioresistant three-proof finishing agent, comprise the following component according to parts by weight meter: 12 parts of fluorine carbon emulsions, 8 parts of trifluoro propyl methyl cyclotrisiloxane, γ-(2,3-epoxy the third oxygen) 4 parts of 2 parts of propyl trimethoxy silicanes, 1 part of citric acid, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) 2 parts of sebacates, 3 parts of polyoxyethylene carboxylates, 120 parts of deionized waters.
The preparation method of the uvioresistant three-proof finishing agent of the present embodiment is by deionized water, fluorine carbon emulsion, trifluoro propyl methyl cyclotrisiloxane, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) sebacate and γ-(2,3-epoxy the third oxygen) propyl trimethoxy silicane be placed in stirrer for mixing evenly after, add again polyoxyethylene carboxylate and citric acid, continue to be stirred to and mix, obtain the uvioresistant three-proof finishing agent of the present embodiment.
Embodiment 2
A kind of uvioresistant three-proof finishing agent, comprise the following component according to parts by weight meter: 16 parts of fluorine carbon emulsions, 12 parts of trifluoro propyl methyl cyclotrisiloxane, γ-(2,3-epoxy the third oxygen) 7 parts of 5 parts of propyl trimethoxy silicanes, 3 parts of citric acids, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) 5 parts of sebacates, 5 parts of polyoxyethylene carboxylates, 150 parts of deionized waters.
The preparation method of the uvioresistant three-proof finishing agent of the present embodiment is identical with the preparation method of the uvioresistant three-proof finishing agent of embodiment 1.
Embodiment 3
A kind of uvioresistant three-proof finishing agent, comprise the following component according to parts by weight meter: 14 parts of fluorine carbon emulsions, 10 parts of trifluoro propyl methyl cyclotrisiloxane, γ-(2,3-epoxy the third oxygen) 6 parts of 4 parts of propyl trimethoxy silicanes, 2 parts of citric acids, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) 3 parts of sebacates, 4 parts of polyoxyethylene carboxylates, 130 parts of deionized waters.
The preparation method of the uvioresistant three-proof finishing agent of the present embodiment is identical with the preparation method of the uvioresistant three-proof finishing agent of embodiment 1.
Adopt the white gauze of cotton to test, by in the uvioresistant three-proof finishing agent of the embodiment of the present invention 1 ~ 3 of the white gauze immersion of cotton 20 ~ 30g/L, pick-up is 70%, dry at 120 ℃, then according to the method for AATCC-22 and AATCC-118, it is refused water and refuses oily performance test, according to the method for GB-T 18830-2002, carry out anti-ultraviolet performance test, its test result is shown in Table 1 simultaneously.
The performance detection data of the uvioresistant three-proof finishing agent of table 1 embodiment 1 ~ 3
? | Refuse water | Refuse oil | UPF | T(UVA)av |
Embodiment 1 | 95 | 6 | 62 | <5% |
Embodiment 2 | 100 | 4 | 60 | <5% |
Embodiment 3 | 100 | 5 | 61 | <5% |
Claims (3)
1. a uvioresistant three-proof finishing agent, it is characterized in that comprising the following component according to parts by weight meter: 4 ~ 7 parts of 12 ~ 16 parts of fluorine carbon emulsions, 8 ~ 12 parts of trifluoro propyl methyl cyclotrisiloxane, 2 ~ 5 parts of coupling agents, 1 ~ 3 part of citric acid, ESCALOL 567, two (2,2,6,6-tetramethyl-4-piperidyl) 2 ~ 5 parts of sebacates, 3 ~ 5 parts of polyoxyethylene carboxylates, 120 ~ 150 parts of deionized waters.
2. uvioresistant three-proof finishing agent according to claim 1, is characterized in that described coupling agent is silane coupler.
3. uvioresistant three-proof finishing agent according to claim 1, is characterized in that described silane coupler is γ-(2,3-epoxy the third oxygen) propyl trimethoxy silicane.
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CN201310610487.0A CN103668985B (en) | 2013-11-27 | 2013-11-27 | A kind of uvioresistant three-proof finishing agent |
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CN103668985B CN103668985B (en) | 2015-11-11 |
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Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104452291A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of wool fabric |
CN105603743A (en) * | 2016-02-26 | 2016-05-25 | 苏州三和开泰花线织造有限公司 | Lasting efficient anti-ultraviolet finishing agent and preparation method thereof |
CN105648776A (en) * | 2016-04-01 | 2016-06-08 | 吴江市林旺纺织厂 | Antibacterial and anti-ultraviolet finishing agent and method for preparing same |
CN107604510A (en) * | 2017-10-13 | 2018-01-19 | 江苏美恒纺织实业有限公司 | One kind is breathed freely and uvioresistant fabrics and its manufacture method |
CN107740217A (en) * | 2017-10-13 | 2018-02-27 | 江苏美恒纺织实业有限公司 | A kind of multifunctional fabric and its manufacture method |
CN108505347A (en) * | 2018-04-25 | 2018-09-07 | 肖玉杰 | Breathable fabric |
CN108589297A (en) * | 2018-04-25 | 2018-09-28 | 肖玉杰 | Ventilative comfortable women's dress and its processing technology |
CN108729216A (en) * | 2018-05-29 | 2018-11-02 | 安徽英士博纺织发展有限公司 | A kind of rapid-curing cutback clothing fabric anti-ultraviolet finishing liquid |
CN109056156A (en) * | 2018-10-17 | 2018-12-21 | 南通薇星纺织科技有限公司 | UV protection polyester cotton shell fabric and preparation method thereof |
CN111434490A (en) * | 2019-04-30 | 2020-07-21 | 浙江东进新材料有限公司 | Foaming breathable film composite multifunctional fabric |
CN112921444A (en) * | 2021-03-09 | 2021-06-08 | 许玉华 | Anti-ultraviolet functional fiber and preparation process thereof |
CN114771074A (en) * | 2022-05-23 | 2022-07-22 | 绍兴精绣布艺有限公司 | Curtain fabric and preparation process thereof |
CN115045106A (en) * | 2022-05-10 | 2022-09-13 | 嘉兴元祯化工有限公司 | Ultraviolet-proof three-proofing finishing agent for fabric, preparation method and use method |
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CN1763302A (en) * | 2005-08-09 | 2006-04-26 | 西安华捷科技发展有限责任公司 | Nano compound, multifunctional oil-resistant, waterproof ultraviolet-resistant textile finishing agent and preparation method thereof |
CN101696548A (en) * | 2009-10-15 | 2010-04-21 | 浙江理工大学 | Wideband, uvioresistant and highly lightfast finishing agent as well as preparation method and application thereof |
CN102585145A (en) * | 2012-02-21 | 2012-07-18 | 黑龙江泰纳科技发展有限责任公司 | Three-protection anti-microbial finishing agent and preparation method thereof |
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CN103102447A (en) * | 2012-12-14 | 2013-05-15 | 常熟市琴达针织印染有限公司 | Preparation method of water/alcohol/blood proof finishing agent for fabrics |
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CN1763302A (en) * | 2005-08-09 | 2006-04-26 | 西安华捷科技发展有限责任公司 | Nano compound, multifunctional oil-resistant, waterproof ultraviolet-resistant textile finishing agent and preparation method thereof |
CN101696548A (en) * | 2009-10-15 | 2010-04-21 | 浙江理工大学 | Wideband, uvioresistant and highly lightfast finishing agent as well as preparation method and application thereof |
JP2013036136A (en) * | 2011-08-08 | 2013-02-21 | Komatsu Seiren Co Ltd | Water and oil repellent fabric with stain release property |
CN102585145A (en) * | 2012-02-21 | 2012-07-18 | 黑龙江泰纳科技发展有限责任公司 | Three-protection anti-microbial finishing agent and preparation method thereof |
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Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104452291A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of wool fabric |
CN105603743A (en) * | 2016-02-26 | 2016-05-25 | 苏州三和开泰花线织造有限公司 | Lasting efficient anti-ultraviolet finishing agent and preparation method thereof |
CN105648776A (en) * | 2016-04-01 | 2016-06-08 | 吴江市林旺纺织厂 | Antibacterial and anti-ultraviolet finishing agent and method for preparing same |
CN107604510A (en) * | 2017-10-13 | 2018-01-19 | 江苏美恒纺织实业有限公司 | One kind is breathed freely and uvioresistant fabrics and its manufacture method |
CN107740217A (en) * | 2017-10-13 | 2018-02-27 | 江苏美恒纺织实业有限公司 | A kind of multifunctional fabric and its manufacture method |
CN108589297A (en) * | 2018-04-25 | 2018-09-28 | 肖玉杰 | Ventilative comfortable women's dress and its processing technology |
CN108505347A (en) * | 2018-04-25 | 2018-09-07 | 肖玉杰 | Breathable fabric |
CN108729216A (en) * | 2018-05-29 | 2018-11-02 | 安徽英士博纺织发展有限公司 | A kind of rapid-curing cutback clothing fabric anti-ultraviolet finishing liquid |
CN109056156A (en) * | 2018-10-17 | 2018-12-21 | 南通薇星纺织科技有限公司 | UV protection polyester cotton shell fabric and preparation method thereof |
CN111434490A (en) * | 2019-04-30 | 2020-07-21 | 浙江东进新材料有限公司 | Foaming breathable film composite multifunctional fabric |
CN111434490B (en) * | 2019-04-30 | 2021-10-01 | 浙江东进新材料有限公司 | Foaming breathable film composite multifunctional fabric |
CN112921444A (en) * | 2021-03-09 | 2021-06-08 | 许玉华 | Anti-ultraviolet functional fiber and preparation process thereof |
CN112921444B (en) * | 2021-03-09 | 2023-02-03 | 无锡市世纪风服饰有限公司 | Anti-ultraviolet functional fiber and preparation process thereof |
CN115045106A (en) * | 2022-05-10 | 2022-09-13 | 嘉兴元祯化工有限公司 | Ultraviolet-proof three-proofing finishing agent for fabric, preparation method and use method |
CN114771074A (en) * | 2022-05-23 | 2022-07-22 | 绍兴精绣布艺有限公司 | Curtain fabric and preparation process thereof |
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