CN108505347A - Breathable fabric - Google Patents
Breathable fabric Download PDFInfo
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- CN108505347A CN108505347A CN201810378224.4A CN201810378224A CN108505347A CN 108505347 A CN108505347 A CN 108505347A CN 201810378224 A CN201810378224 A CN 201810378224A CN 108505347 A CN108505347 A CN 108505347A
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- China
- Prior art keywords
- parts
- weight
- fabric
- breathable fabric
- titanate esters
- Prior art date
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- 239000004744 fabric Substances 0.000 title claims abstract description 88
- -1 glycol dimercaptosuccinates Chemical class 0.000 claims abstract description 57
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 51
- 239000007788 liquid Substances 0.000 claims abstract description 31
- 238000007598 dipping method Methods 0.000 claims abstract description 20
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000003921 oil Substances 0.000 claims abstract description 13
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 13
- 239000010703 silicon Substances 0.000 claims abstract description 13
- PRPAGESBURMWTI-UHFFFAOYSA-N [C].[F] Chemical compound [C].[F] PRPAGESBURMWTI-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000839 emulsion Substances 0.000 claims abstract description 12
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims abstract description 12
- XYZZKVRWGOWVGO-UHFFFAOYSA-N Glycerol-phosphate Chemical class OP(O)(O)=O.OCC(O)CO XYZZKVRWGOWVGO-UHFFFAOYSA-N 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000007822 coupling agent Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 9
- 239000002253 acid Substances 0.000 claims description 41
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 40
- 125000004423 acyloxy group Chemical group 0.000 claims description 38
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical class CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 claims description 21
- 229920002818 (Hydroxyethyl)methacrylate Polymers 0.000 claims description 20
- NWVVVBRKAWDGAB-UHFFFAOYSA-N p-methoxyphenol Chemical compound COC1=CC=C(O)C=C1 NWVVVBRKAWDGAB-UHFFFAOYSA-N 0.000 claims description 10
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical class CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 6
- 229940070748 dimercaptosuccinate Drugs 0.000 claims description 4
- 150000002148 esters Chemical class 0.000 claims description 4
- ACTRVOBWPAIOHC-UHFFFAOYSA-N succimer Chemical compound OC(=O)C(S)C(S)C(O)=O ACTRVOBWPAIOHC-UHFFFAOYSA-N 0.000 claims description 4
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical group [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 claims description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 230000035699 permeability Effects 0.000 abstract description 9
- 238000001035 drying Methods 0.000 abstract description 5
- BIFQHCGLXZWNLN-UHFFFAOYSA-N 2,2,6-trifluoro-4-methyl-4-propyl-1,3,5,2,4,6-trioxatrisilinane Chemical compound CCC[Si]1(C)O[SiH](F)O[Si](F)(F)O1 BIFQHCGLXZWNLN-UHFFFAOYSA-N 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- 238000002360 preparation method Methods 0.000 description 15
- GNSFRPWPOGYVLO-UHFFFAOYSA-N 3-hydroxypropyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCCCO GNSFRPWPOGYVLO-UHFFFAOYSA-N 0.000 description 13
- 238000010792 warming Methods 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 239000000377 silicon dioxide Substances 0.000 description 7
- 238000003756 stirring Methods 0.000 description 7
- 239000008367 deionised water Substances 0.000 description 6
- 229910021641 deionized water Inorganic materials 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- QZPSOSOOLFHYRR-UHFFFAOYSA-N 3-hydroxypropyl prop-2-enoate Chemical compound OCCCOC(=O)C=C QZPSOSOOLFHYRR-UHFFFAOYSA-N 0.000 description 5
- PYBNTRWJKQJDRE-UHFFFAOYSA-L dodecanoate;tin(2+) Chemical class [Sn+2].CCCCCCCCCCCC([O-])=O.CCCCCCCCCCCC([O-])=O PYBNTRWJKQJDRE-UHFFFAOYSA-L 0.000 description 5
- 125000005395 methacrylic acid group Chemical class 0.000 description 5
- 235000008708 Morus alba Nutrition 0.000 description 3
- 240000000249 Morus alba Species 0.000 description 3
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical group CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 3
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 2
- 241000222122 Candida albicans Species 0.000 description 2
- 229920002334 Spandex Polymers 0.000 description 2
- 229920004933 Terylene® Polymers 0.000 description 2
- AWUCVROLDVIAJX-UHFFFAOYSA-N alpha-glycerophosphate Natural products OCC(O)COP(O)(O)=O AWUCVROLDVIAJX-UHFFFAOYSA-N 0.000 description 2
- 239000000022 bacteriostatic agent Substances 0.000 description 2
- 229940095731 candida albicans Drugs 0.000 description 2
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000004759 spandex Substances 0.000 description 2
- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- OOCCDEMITAIZTP-UHFFFAOYSA-N allylic benzylic alcohol Natural products OCC=CC1=CC=CC=C1 OOCCDEMITAIZTP-UHFFFAOYSA-N 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000005204 hydroxybenzenes Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- AWUCVROLDVIAJX-GSVOUGTGSA-N sn-glycerol 3-phosphate Chemical compound OC[C@@H](O)COP(O)(O)=O AWUCVROLDVIAJX-GSVOUGTGSA-N 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/244—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons
- D06M15/256—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons containing fluorine
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/45—Oxides or hydroxides of elements of Groups 3 or 13 of the Periodic Table; Aluminates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/252—Mercaptans, thiophenols, sulfides or polysulfides, e.g. mercapto acetic acid; Sulfonium compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- Engineering & Computer Science (AREA)
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of breathable fabrics, are prepared using following methods：5 15 parts by weight fluorine carbon emulsions, 0.5 1.5 parts by weight of glycerin phosphates, 13 parts by weight trifluoro propyl methyl cyclotrisiloxane, 24 parts by weight titanate coupling agents, 10 20 parts by weight glycol dimercaptosuccinates, 10 20 parts by weight ethoxylated dodecyl alcohols, 0.3 0.9 parts by weight amido silicon oils are added to be uniformly mixed in 100 120 parts by weight water and obtain dressing liquid；Fabric is impregnated to 10 30min in dressing liquid, the fabric after dipping is subjected to mangle, pick-up is 60 80%, and drying obtains the breathable fabric.The breathable fabric of the present invention has good permeability, comfortable and easy to wear, and the surface modeling of the smooth smoothness of fabric, and can be properly bonded with human body, and good comfort effect is visually generated to people.
Description
Technical field
The present invention relates to a kind of fabrics, and in particular to a kind of breathable fabric.
Background technology
China is that maximum fabric clothing producing country, exported country and country of consumption, export amount account for world export trade in the world
It is more than easy a quarter.Textile fabric is related to the every aspect of people's life, and existing fabric cannot be satisfied the people increasingly
The material and cultural needs of growth.In particular, fabric permeability and bad in the prior art.Therefore, in terms of fabric, need into
The research and discovery of one step.
Invention content
For deficiencies of the prior art, the present invention adopts the following technical scheme that：
A kind of breathable fabric, is prepared using following methods：
S1, by 5-15 parts by weight fluorine carbon emulsion, 0.5-1.5 parts by weight of glycerin phosphate, 1-3 parts by weight trifluoro propyl methyl
Cyclotrisiloxane, 2-4 parts by weight titanate coupling agent, 10-20 parts by weight glycol dimercaptosuccinate, the 10-20 parts by weight moons
Cinnamic alcohol polyoxyethylene ether, 0.3-0.9 parts by weight amido silicon oils, which are added to be uniformly mixed in 100-120 parts by weight water, obtains dressing liquid；
S2, fabric in dressing liquid is impregnated into 10-30min, the fabric after dipping is subjected to mangle, pick-up 60-
80%, drying obtains breathable fabric.
The temperature of the dipping is 30-50 DEG C, and the mass ratio of the fabric and dressing liquid is 1：(5-15).
The temperature of the drying is 65-85 DEG C, time 3-9h.
The fabric is weaved by one or more in terylene, mulberry silk, spandex.The fabric grammes per square metre is 20-
120g/m2。
The titanate coupling agent is isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters.
Further, the titanate coupling agent is three (dioctylphyrophosphoric acid acyloxy) titanate esters of modified isopropyl.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 120-130g isopropyls
Base three (dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 55-75 DEG C, and 0.05-0.2g p-hydroxyanisole, 0.003- is added
0.009g dibutyl tin laurates, it is 55-75 DEG C to keep temperature, and 5-15g methyl is added dropwise in the case where rotating speed is 200-500r/min
Temperature after being added dropwise, is risen to 95-105 DEG C, is with rotating speed by hydroxy-ethyl acrylate and 20-30g hydroxy propyl methacrylates
2-5h is reacted under 100-300r/min to get modified three (dioctylphyrophosphoric acid acyloxy) titanate esters of isopropyl.
Further, the preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：It will
120-130g isopropyls three (dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 55-75 DEG C, and 0.05-0.2g para hydroxybenzenes are added
Methyl ether, 0.003-0.009g dibutyl tin laurates, it is 55-75 DEG C to keep temperature, is dripped in the case where rotating speed is 200-500r/min
Add 5-15g hydroxyethyl methacrylates and 20-30g hydroxy propyl methacrylates, after being added dropwise, 5-15g cerias be added,
Temperature is risen to 95-105 DEG C, is to react 2-5h under 100-300r/min to get modified three (dioctyl coke phosphorus of isopropyl with rotating speed
Sour acyloxy) titanate esters.
The rate of addition of the hydroxyethyl methacrylate is 0.01-0.05g/s.
The rate of addition of the hydroxy propyl methacrylate is 0.01-0.05g/s.
Still further preferably, to improve the anti-microbial property of fabric, the present invention also provides following technical proposals：
A kind of breathable fabric, is prepared using following methods：
S1, by 5-15 parts by weight fluorine carbon emulsion, 0.5-1.5 parts by weight of glycerin phosphate, 1-3 parts by weight trifluoro propyl methyl
Cyclotrisiloxane, 2-4 parts by weight titanate coupling agent, 10-20 parts by weight glycol dimercaptosuccinate, 1-3 parts by weight are antibacterial
Agent, 10-20 parts by weight ethoxylated dodecyl alcohol, 0.3-0.9 parts by weight amido silicon oils are added in 100-120 parts by weight water and mix
Uniformly obtain dressing liquid；
S2, fabric in dressing liquid is impregnated into 10-30min, the fabric after dipping is subjected to mangle, pick-up 60-
80%, drying obtains breathable fabric.
The temperature of the dipping is 30-50 DEG C, and the mass ratio of the fabric and dressing liquid is 1：(5-15).
The temperature of the drying is 65-85 DEG C, time 3-9h.
The bacteriostatic agent is oleic imidazolinone quaternary ammonium salt and/or 1- benzyl -1- aminoethyl -2- alkyl imidazoline in heptan quaternary ammoniums
Salt.Preferably, the bacteriostatic agent is by 60-70wt% oleic imidazolinones quaternary ammonium salt and 30-40wt%1- benzyl -1- aminoethyls -
2- alkyl imidazoline quaternary ammonium salts in heptan form.
The fabric is weaved by one or more in terylene, mulberry silk, spandex.The fabric grammes per square metre is 20-
120g/m2。
The titanate coupling agent is isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters.
Further, the titanate coupling agent is three (dioctylphyrophosphoric acid acyloxy) titanate esters of modified isopropyl.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 120-130g isopropyls
Base three (dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 55-75 DEG C, and 0.05-0.2g p-hydroxyanisole, 0.003- is added
0.009g dibutyl tin laurates, it is 55-75 DEG C to keep temperature, and 5-15g methyl is added dropwise in the case where rotating speed is 200-500r/min
Hydroxy-ethyl acrylate and 20-30g hydroxy propyl methacrylates after being added dropwise, are added 5-15g cerias, temperature are risen to
95-105 DEG C, be that 2-5h is reacted under 100-300r/min to get modified isopropyl three (dioctylphyrophosphoric acid acyloxy) with rotating speed
Titanate esters.
The rate of addition of the hydroxyethyl methacrylate is 0.01-0.05g/s.
The rate of addition of the hydroxy propyl methacrylate is 0.01-0.05g/s.
The breathable fabric of the present invention has good permeability, comfortable and easy to wear, and the curved surface of the smooth smoothness of fabric is made
Type, and can be properly bonded with human body, good comfort effect is visually generated to people.
Specific implementation mode
Drapability is tested：It is carried out with reference to FZ/T 01045-1996, test equipment is carried using measuring appratus Co., Ltd of Wuhan state
The fabric Drape analyzer of the model YG811E of confession；Experiment before by antibacterial moisture-permeable shell fabric temperature be 20 DEG C, it is relatively wet
Damping 24 hours under conditions of degree is 65%.The drapability of fabric is an important indicator of wearability of fabric, is had good
The clothes of drapability can form the surface modeling of smooth smoothness, and can be properly bonded with human body, visual comfortable to people
Property.
Permeability detects：By standard GB/T/T5453-1997《The measurement of textile fabric gas permeability》It carries out,
Under the conditions of 1.3kPa in the analytical unit time (second) the penetrated air of every square metre of area amount (L/m2·s)。
Bacteriostasis property is tested：Reference《National Standard of the People's Republic of China GB15979-1995, disposable health are used
Product sanitary standard》, detect bacteriostasis property of the breathable fabric obtained to following microorganisms.The microorganism tested：Candida albicans
Bacterium (ATCC10231), Friedlander's bacillus (ATCC4352).By breathable fabric obtained, (every area is 70cm2) respectively
It is 253.7nm through wavelength, exposure intensity is 200 μ W/cm2After ultraviolet light 1.5min sterilizations, on every breathable fabric
Even coating Candida albicans 1.0 × 105CFU/ pieces, Friedlander's bacillus 1.0 × 105CFU/ pieces, effect are tested every after 30 minutes
Piece breathable fabric bacterial content.
Raw material introduction in embodiment：
Fluorine carbon emulsion is according to application No. is method systems shown in embodiment 1 in the Chinese patent of application number 201410771906.3
It is standby.
Glycerophosphate, No. CAS：57-03-4.
Trifluoro propyl methyl cyclotrisiloxane, No. CAS：2374-14-3.
Glycol dimercaptosuccinate, No. CAS：123-81-9.
The paper that oleic imidazolinone quaternary ammonium salt is delivered according to Wu Xiaonan《The synthesis of oleic imidazolinone quaternary ammonium salt and corrosion inhibition
Research》It is prepared by determining optimum process condition and method.
1- benzyl -1- aminoethyl -2- alkyl imidazoline quaternary ammonium salts in heptan are according to application No. is 200910305443.0 China
In patent prepared by method shown in specific implementation mode two.
Ethoxylated dodecyl alcohol is provided by Jiangsu Hai'an Petrochemical Plant, product specification L-3.
Isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, No. CAS：67691-13-8.
P-hydroxyanisole, No. CAS：150-76-5.
Dibutyl tin laurate, No. CAS：77-58-7.
Hydroxyethyl methacrylate, No. CAS：868-77-9.
Hydroxy propyl methacrylate, No. CAS：27813-02-1.
Ceria, No. CAS：1306-38-3, grain size 200nm.
The fabric is provided by Huzhou Yong Rui Textile Co., Ltd., and color is white, and ingredient is 100% mulberry silk, grammes per square metre
For 34g/m2。
Amido silicon oil is the amido silicon oil for the model JF-8060 that Jiashan Jiangnan textile material Co., Ltd provides.
Embodiment 1
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 parts by weight isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates, 2 weight
Part oleic imidazolinone quaternary ammonium salt, 12 parts by weight ethoxylated dodecyl alcohols, 0.5 parts by weight amido silicon oil are added 110 parts by weight and go
It is uniformly mixed for 300r/min stirrings 20min with rotating speed in ionized water and obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
Embodiment 2
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 part by weight modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates, 2
110 weight are added in parts by weight oleic imidazolinone quaternary ammonium salt, 12 parts by weight ethoxylated dodecyl alcohols, 0.5 parts by weight amido silicon oil
It is uniformly mixed for 300r/min stirrings 20min with rotating speed in part deionized water and obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 125g isopropyls three
(dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 65 DEG C, and 0.1g p-hydroxyanisole, two fourth of 0.005g tin dilaurates is added
Ji Xi, it is 65 DEG C to keep temperature, and 10g hydroxyethyl methacrylates and 25g methacrylic acids is added dropwise in the case where rotating speed is 300r/min
The rate of addition of hydroxypropyl acrylate, the hydroxyethyl methacrylate is 0.02g/s, the rate of addition of the hydroxy propyl methacrylate
10g cerias are added after hydroxyethyl methacrylate and hydroxy propyl methacrylate are all added dropwise for 0.02g/s, it will
Temperature rises to 95 DEG C, is that 4h is reacted under 150r/min to get modified three (dioctylphyrophosphoric acid acyloxy) titanium of isopropyl with rotating speed
Acid esters.
Embodiment 3
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 part by weight modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates, 2
110 weight are added in parts by weight oleic imidazolinone quaternary ammonium salt, 12 parts by weight ethoxylated dodecyl alcohols, 0.5 parts by weight amido silicon oil
It is uniformly mixed for 300r/min stirrings 20min with rotating speed in part deionized water and obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 125g isopropyls three
(dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 65 DEG C, and 0.1g p-hydroxyanisole, two fourth of 0.005g tin dilaurates is added
Ji Xi, it is 65 DEG C to keep temperature, and 10g hydroxyethyl methacrylates and 25g methacrylic acids is added dropwise in the case where rotating speed is 300r/min
The rate of addition of hydroxypropyl acrylate, the hydroxyethyl methacrylate is 0.02g/s, the rate of addition of the hydroxy propyl methacrylate
Temperature is risen to 95 DEG C after hydroxyethyl methacrylate and hydroxy propyl methacrylate are all added dropwise for 0.02g/s, with
Rotating speed is that 4h is reacted under 150r/min to get modified three (dioctylphyrophosphoric acid acyloxy) titanate esters of isopropyl.
Embodiment 4
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 part by weight modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates, 2
Parts by weight 1- benzyl -1- aminoethyl -2- alkyl imidazoline quaternary ammonium salts in heptan, 12 parts by weight ethoxylated dodecyl alcohols, 0.5 parts by weight
Amido silicon oil, which is added in 110 parts by weight of deionized water to be uniformly mixed for 300r/min stirrings 20min with rotating speed, obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 125g isopropyls three
(dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 65 DEG C, and 0.1g p-hydroxyanisole, two fourth of 0.005g tin dilaurates is added
Ji Xi, it is 65 DEG C to keep temperature, and 10g hydroxyethyl methacrylates and 25g methacrylic acids is added dropwise in the case where rotating speed is 300r/min
The rate of addition of hydroxypropyl acrylate, the hydroxyethyl methacrylate is 0.02g/s, the rate of addition of the hydroxy propyl methacrylate
10g cerias are added after hydroxyethyl methacrylate and hydroxy propyl methacrylate are all added dropwise for 0.02g/s, it will
Temperature rises to 95 DEG C, is that 4h is reacted under 150r/min to get modified three (dioctylphyrophosphoric acid acyloxy) titanium of isopropyl with rotating speed
Acid esters.
Embodiment 5
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 parts by weight isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates, 12 weights
It is 300r/min that amount part ethoxylated dodecyl alcohol, 0.5 parts by weight amido silicon oil, which are added in 110 parts by weight of deionized water with rotating speed,
Stirring 20min, which is uniformly mixed, obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
Embodiment 6
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 part by weight modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates,
12 parts by weight ethoxylated dodecyl alcohols, 0.5 parts by weight amido silicon oil are added in 110 parts by weight of deionized water is with rotating speed
300r/min stirrings 20min, which is uniformly mixed, obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 125g isopropyls three
(dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 65 DEG C, and 0.1g p-hydroxyanisole, two fourth of 0.005g tin dilaurates is added
Ji Xi, it is 65 DEG C to keep temperature, and 10g hydroxyethyl methacrylates and 25g methacrylic acids is added dropwise in the case where rotating speed is 300r/min
The rate of addition of hydroxypropyl acrylate, the hydroxyethyl methacrylate is 0.02g/s, the rate of addition of the hydroxy propyl methacrylate
Temperature is risen to 95 DEG C after hydroxyethyl methacrylate and hydroxy propyl methacrylate are all added dropwise for 0.02g/s, with
Rotating speed is that 4h is reacted under 150r/min to get modified three (dioctylphyrophosphoric acid acyloxy) titanate esters of isopropyl.
Embodiment 7
A kind of preparation method of breathable fabric, includes the following steps：
S1, by 10 parts by weight fluorine carbon emulsions, 1 parts by weight of glycerin phosphate, 1.5 parts by weight trifluoro propyl methyl ring, three silica
Alkane, 3 part by weight modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters, 12 parts by weight glycol dimercaptosuccinates,
12 parts by weight ethoxylated dodecyl alcohols, 0.5 parts by weight amido silicon oil are added in 110 parts by weight of deionized water is with rotating speed
300r/min stirrings 20min, which is uniformly mixed, obtains dressing liquid；
S2, fabric impregnates to 20min in dressing liquid, the temperature of the dipping is 40 DEG C, the fabric and dressing liquid
Mass ratio is 1：10, the fabric after dipping is subjected to mangle, pick-up 70wt% is dried 7h at being 70 DEG C in temperature, obtained
Breathable fabric.
The preparation method of the modified isopropyl three (dioctylphyrophosphoric acid acyloxy) titanate esters is：By 125g isopropyls three
(dioctylphyrophosphoric acid acyloxy) titanate esters are warming up to 65 DEG C, and 0.1g p-hydroxyanisole, two fourth of 0.005g tin dilaurates is added
Ji Xi, it is 65 DEG C to keep temperature, and 10g hydroxyethyl methacrylates and 25g methacrylic acids is added dropwise in the case where rotating speed is 300r/min
The rate of addition of hydroxypropyl acrylate, the hydroxyethyl methacrylate is 0.02g/s, the rate of addition of the hydroxy propyl methacrylate
10g cerias are added after hydroxyethyl methacrylate and hydroxy propyl methacrylate are all added dropwise for 0.02g/s, it will
Temperature rises to 95 DEG C, is that 4h is reacted under 150r/min to get modified three (dioctylphyrophosphoric acid acyloxy) titanium of isopropyl with rotating speed
Acid esters.
Test case 1
Breathable fabric bacteriostasis property prepared by embodiment 1-4, permeability, draping property are tested.Specific test
It the results are shown in Table 1.
Table 1：Test result table
Breathable fabric permeability prepared by embodiment 5-7, draping property are tested.Specific test result is shown in Table 2.
Table 2：Test result table
| Permeability (L/m2·s) | Suspended coefficient (%) | |
| Embodiment 5 | 348 | 7.08 |
| Embodiment 6 | 374 | 6.71 |
| Embodiment 7 | 391 | 6.52 |
The breathable fabric of the present invention has good permeability, comfortable and easy to wear, and the curved surface of the smooth smoothness of fabric is made
Type, and can be properly bonded with human body, good comfort effect is visually generated to people.
Claims (4)
1. a kind of breathable fabric, is prepared using following methods：
S1, by 5-15 parts by weight fluorine carbon emulsion, 0.5-1.5 parts by weight of glycerin phosphate, 1-3 parts by weight trifluoro propyl methyl ring three
Siloxanes, 2-4 parts by weight titanate coupling agent, 10-20 parts by weight glycol dimercaptosuccinate, 10-20 parts by weight laruyl alcohols
Polyoxyethylene ether, 0.3-0.9 parts by weight amido silicon oils, which are added to be uniformly mixed in 100-120 parts by weight water, obtains dressing liquid；
S2, fabric in dressing liquid is impregnated into 10-30min, the fabric after dipping is subjected to mangle, pick-up 60-80% dries
It is dry, obtain the breathable fabric.
2. breathable fabric as described in claim 1, which is characterized in that the titanate coupling agent is three (dioctyl of isopropyl
Pyrophosphoric acid acyloxy) titanate esters.
3. breathable fabric as claimed in claim 2, which is characterized in that the titanate coupling agent is modified isopropyl three (two
Octyl pyrophosphoric acid acyloxy) titanate esters.
4. breathable fabric as claimed in claim 3, which is characterized in that three (dioctylphyrophosphoric acid acyl-oxygen of the modified isopropyl
Base) titanate esters are prepared using following methods：By 120-130g isopropyls three (dioctylphyrophosphoric acid acyloxy) titanate esters liter
0.05-0.2g p-hydroxyanisole, 0.003-0.009g dibutyl tin laurates is added to 55-75 DEG C in temperature, and holding temperature is
55-75 DEG C, 5-15g hydroxyethyl methacrylates and 20-30g methacrylic acid hydroxypropyls is added dropwise in the case where rotating speed is 200-500r/min
Temperature after being added dropwise, is risen to 95-105 DEG C by ester, is that 2-5h is reacted under 100-300r/min to get modified isopropyl with rotating speed
Base three (dioctylphyrophosphoric acid acyloxy) titanate esters.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810378224.4A CN108505347A (en) | 2018-04-25 | 2018-04-25 | Breathable fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810378224.4A CN108505347A (en) | 2018-04-25 | 2018-04-25 | Breathable fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108505347A true CN108505347A (en) | 2018-09-07 |
Family
ID=63383257
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810378224.4A Withdrawn CN108505347A (en) | 2018-04-25 | 2018-04-25 | Breathable fabric |
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| CN111235880A (en) * | 2020-03-24 | 2020-06-05 | 朱红英 | Protective cap with antibacterial function and preparation method thereof |
| CN113261716A (en) * | 2021-06-18 | 2021-08-17 | 安徽钟南人防工程防护设备有限公司 | Dampproofing ventilative protective clothing of regulation and control formula |
| CN113403851A (en) * | 2021-06-22 | 2021-09-17 | 安徽钟南人防工程防护设备有限公司 | High-breathability protective clothing and production method thereof |
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