CN103666218A - Alkyd resin high-temperature-resisting antirust paint and preparation method thereof - Google Patents
Alkyd resin high-temperature-resisting antirust paint and preparation method thereof Download PDFInfo
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- CN103666218A CN103666218A CN201310410008.0A CN201310410008A CN103666218A CN 103666218 A CN103666218 A CN 103666218A CN 201310410008 A CN201310410008 A CN 201310410008A CN 103666218 A CN103666218 A CN 103666218A
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Abstract
The invention provides alkyd resin high-temperature-resisting antirust paint. The alkyd resin high-temperature-resisting antirust paint is prepared from the following raw material components in parts by weight: 60 to 65 parts of alkyd resin, 12 to 15 parts of potash feldspar powder, 10 to 12 parts of E-12 epoxy resin, 12 to 15 parts of phthalic anhydride, 12 to 14 parts of carbon black, 6 to 8 parts of crylic acid-2-propylparaben, 3 to 4 parts of titanate coupling agent TMC-TTS, 8 to 10 parts of dimethyl sulfoxide, 4 to 5 parts of isopropyl benzene, 12 to 14 parts of ethyl acetate, 8 to 10 parts of dipropylenetriamine and 5 to 6 parts of coalescing agent. The raw materials of the alkyd resin high-temperature-resisting antirust paint are non-toxic, so that the alkyd resin high-temperature-resisting antirust paint has little toxicity for the human body in the production and application process, and the environmental pollution is low; by adding the coalescing agent in the formula, the compatibility of all components can be improved, and the coalescing effect can be greatly improved. The prepared paint film is resisting to the water, excellent in anticorrosion property, firm in adhesion strength and excellent in alkali resistance, water resistance and high temperature resistance.
Description
Technical field
The present invention relates to metal rust preventing technical field, be specifically related to a kind of Synolac thermostable rustproof paint and preparation method thereof.
Background technology
Metallic corrosion is the very serious problem that people face.The metal that scrap because of metallic corrosion every year in the whole world reaches more than several hundred million tons, and financial loss accounts for 1.5%～2.5% of total value of production in national economy.Metal rusting is the most general, loss is maximum a kind of corrosion.Antirust work is always one of great scientific research task both domestic and external, and people work out the corrosion that many kinds of measures prevented and suppressed metal, and antirust with coating is a kind of effective means.
Summary of the invention
The object of this invention is to provide a kind of Synolac thermostable rustproof paint and preparation method thereof, various metals is had to antirust function.
Technical scheme of the present invention is as follows:
A Synolac thermostable rustproof paint, is characterized in that, its feed composition by following weight part is prepared from:
Synolac 60-65, feldspar in powder 12-15, E-12 epoxy resin 10-12, phthalic anhydride 12-15, carbon black 12-14,2-hydroxypropyl acrylate 6-8, titanate coupling agent TMC-TTS3-4, dimethyl sulfoxide (DMSO) 8-10, isopropyl benzene 4-5, ethyl acetate 12-14, two propylene triamine 8-10, film coalescence aid 5-6.
Described Synolac thermostable rustproof paint, is characterized in that: described film coalescence aid is prepared from by the raw material of following weight part:
Alcohol ester 12 10-12, nano-sized carbon 0.1-0.2, ricinolic acid 1-2, aluminum nitride powder 2-3,2-amino-2-methyl-1-propanol 2-3, silane resin acceptor kh-550 1-2, diatomite in powder 0.3-0.5, tributyl citrate 3-4, ethyl acetate 4-5, Oil of Eucalyptus 1-2, methylethyl ketone peroxide 1-2;
Preparation method: nano-sized carbon, ricinolic acid, aluminum nitride powder, 2-amino-2-methyl-1-propanol, tributyl citrate, ethyl acetate are mixed, dispersed with stirring, then, add again methylethyl ketone peroxide, stirring reaction 40-60 minute, then, is heated to 75-80 ℃, add Oil of Eucalyptus, alcohol ester 12, continue to stir 30-40 minute, be cooled to 60-65 ℃, add other remaining component, 1200-1400 rev/min of stirring reaction 1-2 hour, obtains.
The preparation method of described Synolac thermostable rustproof paint, is characterized in that, comprises the following steps:
(1) part ethyl acetate is put in reactor and then Synolac, E-12 epoxy resin, phthalic anhydride, 2-hydroxypropyl acrylate, two propylene triamines are added wherein, stir 20-30 minute; Again feldspar in powder, carbon black, dimethyl sulfoxide (DMSO), isopropyl benzene, titanate coupling agent TMC-TTS are joined in reactor, stir 30-40 minute, add wherein fully agitation grinding to particle diameter 20-40um, to obtain mixed slurry film coalescence aid and remaining ethyl acetate again;
(2) by 400 order filter-cloth filterings for mixed slurry, obtain finished product of the present invention.
Beneficial effect of the present invention:
Advantages of nontoxic raw materials of the present invention, therefore production and use procedure are little to human body murder by poisoning, and environmental pollution is low, adds film coalescence aid in formula, has improved the consistency of each composition, has greatly improved film-formation result.The paint film of gained is water-fast, antiseptic property is excellent, and resistance to elevated temperatures is good, and bonding strength is firm, alkaline-resisting, water tolerance is all good.
Embodiment:
Embodiment
A Synolac thermostable rustproof paint, its feed composition by following weight (kg) is prepared from:
Synolac 64, feldspar in powder 13, E-12 epoxy resin 11, phthalic anhydride 14, carbon black 13,2-hydroxypropyl acrylate 7, titanate coupling agent TMC-TTS3, dimethyl sulfoxide (DMSO) 9, isopropyl benzene 5, ethyl acetate 13, two propylene triamines 9, film coalescence aid 5;
Concrete preparation method, comprises the following steps:
1, the preparation of film coalescence aid:
(kg) takes alcohol ester 12 by weight, nano-sized carbon 0.1, ricinolic acid 1, aluminum nitride powder 2, 2-amino-2-methyl-1-propanol 3, silane resin acceptor kh-550 1, diatomite in powder 0.4, tributyl citrate 3, ethyl acetate 4, Oil of Eucalyptus 2, methylethyl ketone peroxide 2, by nano-sized carbon, ricinolic acid, aluminum nitride powder, 2-amino-2-methyl-1-propanol, tributyl citrate, ethyl acetate is mixed, dispersed with stirring, then, add again methylethyl ketone peroxide, stirring reaction 40-60 minute, then, be heated to 75-80 ℃, add Oil of Eucalyptus, alcohol ester 12, continue to stir 30-40 minute, be cooled to 60-65 ℃, add other remaining component, 1200-1400 rev/min stirring reaction 1-2 hour and get final product.
2, the preparation of Synolac thermostable rustproof paint, make according to the following steps:
(1) part ethyl acetate is put in reactor and then Synolac, E-12 epoxy resin, phthalic anhydride, 2-hydroxypropyl acrylate, two propylene triamines are added wherein, stir 20-30 minute; Again feldspar in powder, carbon black, dimethyl sulfoxide (DMSO), isopropyl benzene, titanate coupling agent TMC-TTS are joined in reactor, stir 30-40 minute, add wherein fully agitation grinding to particle diameter 20-40um, to obtain mixed slurry film coalescence aid and remaining ethyl acetate again;
(2) by 400 order filter-cloth filterings for mixed slurry, obtain finished product of the present invention.
Testing data
Rust-inhibiting paint prepared by above-described embodiment is according to standard: HG/T2244-1991 < < lathe priming paint > > tests, and result is as following table 1.
The detected result of table 1 rust-inhibiting paint
Claims (3)
1. a Synolac thermostable rustproof paint, is characterized in that, its feed composition by following weight part is prepared from:
Synolac 60-65, feldspar in powder 12-15, E-12 epoxy resin 10-12, phthalic anhydride 12-15, carbon black 12-14, vinylformic acid-2-hydroxy propyl ester 6-8, titanate coupling agent TMC-TTS 3-4, dimethyl sulfoxide (DMSO) 8-10, isopropyl benzene 4-5, ethyl acetate 12-14, two propylene triamine 8-10, film coalescence aid 5-6.
2. Synolac thermostable rustproof paint according to claim 1, is characterized in that: described film coalescence aid is prepared from by the raw material of following weight part:
Alcohol ester 12 10-12, nano-sized carbon 0.1-0.2, ricinolic acid 1-2, aluminum nitride powder 2-3,2-amino-2-methyl-1-propyl alcohol 2-3, silane resin acceptor kh-550 1-2, diatomite in powder 0.3-0.5, tributyl citrate 3-4, ethyl acetate 4-5, Oil of Eucalyptus 1-2, methylethyl ketone peroxide 1-2;
Preparation method: nano-sized carbon, ricinolic acid, aluminum nitride powder, 2-amino-2-methyl-1-propyl alcohol, tributyl citrate, ethyl acetate are mixed, dispersed with stirring, then, add again methylethyl ketone peroxide, stirring reaction 40-60 minute, then, is heated to 75-80 ℃, add Oil of Eucalyptus, alcohol ester 12, continue to stir 30-40 minute, be cooled to 60-65 ℃, add other remaining component, 1200-1400 rev/min of stirring reaction 1-2 hour, obtains.
3. the preparation method of Synolac thermostable rustproof paint according to claim 1, is characterized in that, comprises the following steps:
(1) part ethyl acetate is put in reactor and then Synolac, E-12 epoxy resin, phthalic anhydride, vinylformic acid-2-hydroxy propyl ester, two propylene triamines are added wherein, stir 20-30 minute; Again feldspar in powder, carbon black, dimethyl sulfoxide (DMSO), isopropyl benzene, titanate coupling agent TMC-TTS are joined in reactor, stir 30-40 minute, add wherein fully agitation grinding to particle diameter 20-40um, to obtain mixed slurry film coalescence aid and remaining ethyl acetate again;
(2) by 400 order filter-cloth filterings for mixed slurry, obtain finished product of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310410008.0A CN103666218B (en) | 2013-09-10 | 2013-09-10 | A kind of Alkyd resin high-temperature-resantirust antirust paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310410008.0A CN103666218B (en) | 2013-09-10 | 2013-09-10 | A kind of Alkyd resin high-temperature-resantirust antirust paint and preparation method thereof |
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| CN103666218A true CN103666218A (en) | 2014-03-26 |
| CN103666218B CN103666218B (en) | 2016-08-10 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104277644A (en) * | 2014-10-20 | 2015-01-14 | 苏州常熟荣大威尔科技有限公司 | Novel pressure reducer |
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| RU2252236C1 (en) * | 2003-09-01 | 2005-05-20 | Открытое акционерное общество "Западно-Сибирский металлургический комбинат" (ОАО "ЗСМК") | Undercoat composition for coatings |
| CN1625588A (en) * | 2002-04-30 | 2005-06-08 | 罗特麦克电子私人有限公司 | No under coat anticorrosion composite without chromate and preparation method thereof |
| CN101240137A (en) * | 2008-02-20 | 2008-08-13 | 江阴市天邦涂料化工有限公司 | Special-purpose protection dope for petroleum pipe/drill pipe and its preparation method and construction method |
| CN101270258A (en) * | 2008-03-14 | 2008-09-24 | 天津大田包装容器有限公司 | Steel drum paint special for baking type alcohol acid amido and method of preparing the same |
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2013
- 2013-09-10 CN CN201310410008.0A patent/CN103666218B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1625588A (en) * | 2002-04-30 | 2005-06-08 | 罗特麦克电子私人有限公司 | No under coat anticorrosion composite without chromate and preparation method thereof |
| RU2252236C1 (en) * | 2003-09-01 | 2005-05-20 | Открытое акционерное общество "Западно-Сибирский металлургический комбинат" (ОАО "ЗСМК") | Undercoat composition for coatings |
| CN101240137A (en) * | 2008-02-20 | 2008-08-13 | 江阴市天邦涂料化工有限公司 | Special-purpose protection dope for petroleum pipe/drill pipe and its preparation method and construction method |
| CN101270258A (en) * | 2008-03-14 | 2008-09-24 | 天津大田包装容器有限公司 | Steel drum paint special for baking type alcohol acid amido and method of preparing the same |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104277644A (en) * | 2014-10-20 | 2015-01-14 | 苏州常熟荣大威尔科技有限公司 | Novel pressure reducer |
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| CN103666218B (en) | 2016-08-10 |
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Address after: No. 3636 Qifeng Road, Shizishan Economic Development Zone, Tongling City, Anhui Province, 244031 Patentee after: Tongling Side Technology Co.,Ltd. Address before: No. 3636 Qifeng Road, Shizishan Economic Development Zone, Tongling City, Anhui Province, 244031 Patentee before: TONGLING SIDE TECHNOLOGY Co.,Ltd. |