CN103610609B - A kind of Chinese herbal medicine floral water and preparation method thereof - Google Patents
A kind of Chinese herbal medicine floral water and preparation method thereof Download PDFInfo
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- CN103610609B CN103610609B CN201310612387.1A CN201310612387A CN103610609B CN 103610609 B CN103610609 B CN 103610609B CN 201310612387 A CN201310612387 A CN 201310612387A CN 103610609 B CN103610609 B CN 103610609B
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 49
- 241000411851 herbal medicine Species 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title abstract description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 42
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- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims abstract description 29
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- 230000000694 effects Effects 0.000 abstract description 16
- 239000003205 fragrance Substances 0.000 abstract description 10
- 239000000077 insect repellent Substances 0.000 abstract description 9
- NIQCNGHVCWTJSM-UHFFFAOYSA-N Dimethyl phthalate Chemical compound COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 abstract description 8
- 230000001139 anti-pruritic effect Effects 0.000 abstract description 7
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- 206010020751 Hypersensitivity Diseases 0.000 abstract description 6
- MMOXZBCLCQITDF-UHFFFAOYSA-N N,N-diethyl-m-toluamide Chemical compound CCN(CC)C(=O)C1=CC=CC(C)=C1 MMOXZBCLCQITDF-UHFFFAOYSA-N 0.000 abstract description 5
- 229960001673 diethyltoluamide Drugs 0.000 abstract description 5
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- 230000002940 repellent Effects 0.000 abstract description 5
- FBSAITBEAPNWJG-UHFFFAOYSA-N dimethyl phthalate Natural products CC(=O)OC1=CC=CC=C1OC(C)=O FBSAITBEAPNWJG-UHFFFAOYSA-N 0.000 abstract description 4
- 229960001826 dimethylphthalate Drugs 0.000 abstract description 4
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- OKIJSNGRQAOIGZ-UHFFFAOYSA-N Butopyronoxyl Chemical compound CCCCOC(=O)C1=CC(=O)CC(C)(C)O1 OKIJSNGRQAOIGZ-UHFFFAOYSA-N 0.000 description 1
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Abstract
The present invention relates to chemistry daily necessities field, specifically a kind of Chinese herbal medicine floral water and preparation method thereof.A kind of Chinese herbal medicine floral water, raw material including following weight portion: Fructus Litseae essential oil 1～10 parts, Flos Magnoliae quintessence oil 1～10 parts, P-Cymene 1～10 parts, Borneolum Syntheticum 1.5～3.0 parts, propylene glycol 1.0～2.0 parts and polyoxyethylene sorbitan monoleate, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of polyoxyethylene sorbitan monoleate are 1:5～6.5.The present invention use there is driving away mosquito, to keep away the natural herbal quintessence oil of dirty effect be active component for repellent antipruritic, fragrance, solve current mosquito-repellent perfume and use the problem of the household pesticides compositions such as being irritating to the skin property and hypersensitive diethyltoluamide, dimethyl phthalate, add safety in utilization.
Description
Technical field
The present invention relates to chemistry daily necessities field, specifically a kind of Chinese herbal medicine floral water and preparation method thereof.
Background technology
Summer, mosquito bite can not only make skin produce red and swollen pruritus etc., additionally it is possible to causes the infectious disease that some are serious, affects health and the life of people, the infant that particularly skin is tender.Therefore, floral water (particularly having the floral water of mosquito-repelling function) becomes people's product in the indispensability in summer.
But, tradition has the floral water of mosquito-repelling function, and its main anophelifuge activity composition mostly is the household pesticides compositions such as diethyltoluamide, dimethyl phthalate, anophelifuge fat or dihydropyrone, belongs to micro-poison product, the irritant and anaphylaxis to the skin of contact.Additionally, tradition floral water usually contains the ethanol (about 70%) of higher concentration for the reason of the aspects such as preparation stabilization, thus side effect served by band, as accelerated skin water loss, causing xerosis cutis, the most aging, generation wrinkle, the stimulation of skin tender to infant is the most prominent；The floral water that the concentration containing high concentration ethanol is high is sprayed on air, produces strong, unpleasant pungent taste, and improper use also can the harm such as breaking out of fire.Child's particularly infant of less than 6 years old is in the growth promoter vigorous stage, and skin absorption ability is relatively strong, and respiratory tract resistivity is more weak, should avoid using chemistry mosquito repellent product；And after mosquito bite, small wound can be left on skin, if at this moment using tradition floral water, the chemical substances such as ethanol therein, chemistry anophelifuge directly can enter deep skin by these small wounds, thus produce stimulation pain, add hyperphlogosis, cause skin injury, particularly diethyltoluamide, such as long-term or a large amount of uses it is also possible that neurological symptom and induction leukemia etc..Therefore, exploitation safety non-toxic and the mosquito-repellent perfume without ethanol have important social meaning.
Natural herbal has driving away mosquito, repellent antipruritic, fragrance keep away dirty effect, safe to the human body nontoxic, non-stimulated, without allergy, and degradable, free from environmental pollution etc., these features are all that chemosynthesis anophelifuge does not has.Therefore, the natural herbal floral water without ethanol is important development direction and the trend in following floral water market.
Summary of the invention
It is desirable to provide a kind of, there is driving away mosquito, repellent antipruritic, the fragrance a kind of Chinese herbal medicine floral water keeping away dirty effect and preparation method thereof, solve current mosquito-repellent perfume and use household pesticides the being irritating to the skin property of composition such as diethyltoluamide, dimethyl phthalate and hypersensitive problem；Also solve ethanol that traditional floral water contains higher concentration and cause skin water loss, aging, produce wrinkle and the problem that some potential safety hazards can be caused.
The present invention is achieved by the following technical solutions:
A kind of Chinese herbal medicine floral water, including the raw material of following weight portion:
Fructus Litseae essential oil 1～10 parts, Flos Magnoliae quintessence oil 1～10 parts, P-Cymene 1～10 parts, Borneolum Syntheticum 1.5～3.0 parts, propylene glycol 1.0～2.0 parts and Tween-80, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of Tween-80 are 1:5～6.5.
Fructus Litseae essential oil of the present invention, Flos Magnoliae quintessence oil and P-Cymene can use steam distillation, co_2 supercritical fluid extraction method, solvent method, milling process or other pharmaceutics extracting method well known in the art by extracting acquisition in medical material.Or, directly it is commercially available by market.
The Fructus Litseae essential oil of present invention employing, Flos Magnoliae quintessence oil, P-Cymene, Borneolum Syntheticum.Wherein Fructus Litseae: fragrant odour, main active is Fructus Litseae essential oil, there is warming middle-JIAO to relieve pain, promoting flow of QI and blood, the effect of diuresis of relievining asthma, " Guangxi Chinese medicinal herbal " is recorded: " parasite killing; disappear legendary venomous insect; diuresis ", and modern study shows that Fructus Litseae has antiplatelet aggregation, antiinflammatory, antibacterial, antiallergic and mosquito dispersing effect.Flos Magnoliae: fragrance light weight, there is effect of dispersing wind and cold, clearing the nasal passage, " Japan hanako materia medica " record: " control headache; the loathing of cold, body are kept silent, pruritus ", modern study shows that Flos Magnoliae has local convergence and anesthesia, antimicrobial, antiallergic, antiinflammatory and mosquito dispersing effect, and main active is Flos Magnoliae quintessence oil.Folium Artemisiae Argyi: gas fragrance is pungent, main have effect of dispersing cold for relieving pain, warming the meridian for stopping bleeding, removing damp to relieve itching containing P-Cymene, and modern study shows that Folium Artemisiae Argyi has hemostasis, antiinflammatory, antibacterial, antiallergic and mosquito dispersing effect.Borneolum Syntheticum: fragrant odour, has effect of heat-clearing and toxic substances removing, reducing swelling and alleviating pain, and Compendium of Material Medica is recorded: " logical all keys, dissipate stagnated fire ", and " Bencao Jingshu " is recorded: " gas of fragrance can ward off all evil；Hot property, can dissipate all rheumatism ", modern study shows that Borneolum Syntheticum has anti-inflammation, antipruritic, analgesic effect.The floral water using the proportioning of each raw material of the present invention to prepare has repellent antipruritic, driving away mosquito, fragrance keep away dirty effect, have definite anophelifuge, antipruritic, subside a swelling and the effect removing abnormal flavour.
In the present invention, Tween-80 is a nonionic surfactant being widely used in food, cosmetics and medicine field, can form organized assembles-micelle that lipophilic group is inside, hydrophilic group is outside when reaching finite concentration in aqueous；Formed after micelle, be insoluble in that the derived essential oil of water just can enter into the kernel of micelle and dissolubility in aqueous dramatically increases, and the stability of quintessence oil can be improved.
Propylene glycol is a skin nourishment wetting agent, can prevent the moisture on skin from quickly volatilizing and being dried, skin plays nourishing moisture-keeping function.
During use, adding purified water in the present invention, as long as its addition can be by each material mix homogeneously, those skilled in the art easily realize.
The preparation method of said herbal medicine floral water is as follows:
1, Fructus Litseae essential oil is weighed, Flos Magnoliae quintessence oil, P-Cymene, mix homogeneously, it is thus achieved that mixed essential oil, standby；
2, weighing Borneolum Syntheticum, join in above-mentioned mixed essential oil, stirring is fully dissolved to Borneolum Syntheticum, obtains quintessence oil phase, standby；
3, weigh Tween-80, mix homogeneously with quintessence oil phase, add the propylene glycol of 1.0～2.0 weight portions, mix homogeneously, obtain mixture, standby；
4, mixture adds purified water, be uniformly mixed, under the conditions of 4 DEG C, stand 1～4 week, be then passed through membrane filtration, obtain filtrate；
5, filtrate is qualified through quality inspection, embedding, packaging, it is thus achieved that Chinese herbal medicine floral water.
Chinese herbal medicine floral water of the present invention, except using preparation method of the present invention, also can use preparation method known to other, such as by each raw material mix homogeneously, and membrane filtration, embedding, packaging.And this preparation method have employed the pharmaceutic adjuvant good with skin-friendliness, floral water does not contains ethanol, comfortable, safe and nontoxic, infant, women and all can use ethanol allergy sufferers safely.
Chinese herbal medicine floral water of the present invention have the advantages that the present invention use there is driving away mosquito, to keep away the natural herbal quintessence oil of dirty effect be active component for repellent antipruritic, fragrance, solve current mosquito-repellent perfume and use the problem of the household pesticides compositions such as being irritating to the skin property and hypersensitive diethyltoluamide, dimethyl phthalate, add safety in utilization；Chinese herbal medicine floral water of the present invention, avoiding tradition floral water and contain the drawback of the ethanol (about 70%) of higher concentration to improve the reason of the aspects such as preparation stability, the ethanol solving high concentration is prone to cause skin water loss, aging, generation wrinkle and some safety issues；It is suitable for infant, women and ethanol allergy sufferers is used.
Beneficial effect produced by the present invention is further illustrated below from application result:
One, SD rat repellency test
1. aggressivity test: at 20cm × 20cm
Put into 100 Aedes albopictus in the mosquito cage of × 20cm, cut off the hair of SD rat abdomen 2cm × 2cm area so that it is epidermis exposes；SD rat is fixed on 5 min in mosquito cage, and the mosquito coming to stop falling is qualified for attack more than 20, and the mosquito that attack is qualified can be used for testing.
2. anophelifuge test: the SD rat of attack pass the test is fixed, cropping exposes the skin of abdominal part 2cm × 2cm, by product of the present invention (process group) and distilled water (reference substance) uniform application, remainder tightly hides, after coating, rat is put in the mosquito cage that attack is qualified, observe and stop falling on the epidermis exposed with or without mosquito, and record the time that first mosquito stops falling and biting.Test is repeated 3 times, the average effective mosquito repellent time of record sample and effective anophelifuge rate.Wherein, effective mosquito repellent time: start to calculate until the 1st mosquito bite duration (min) when coating；Effectively anophelifuge rate: effectively anophelifuge rate=(matched group averagely stop fall several process group averagely stop the number that falls) ÷ matched group averagely stops the number × 100% that falls.
3. result of the test: the average effective mosquito repellent time of product of the present invention is 40～70min, in 40min, effective anophelifuge rate is 100%, and after 50min, effective anophelifuge rate is 80.12%.
Two, field condition test
1, anophelifuge test: in mosquito activity peak season, floral water of the present invention is spread upon equably experimenter's (process group) two lower limb and knee joint, 28 experimenters enter mosquito density high field institute, it is separated by 2～3m, sit quietly in little stool, expose the position being coated with floral water of the present invention, observe and record mosquito thorn and sting situation；Separately setting 8 people as matched group (not smearing floral water of the present invention), the thorn measuring 15min stings index.
2, result of the test: product of the present invention thorn sting index be 32/15min time, its average effective mosquito repellent time is 45.5min.It addition, all experimenters reflect that product fragrance of the present invention is natural, fragrance is pleasant, it is comfortable to use, there are not any excitement and skin allergy symptom.
Detailed description of the invention
Below the detailed description of the invention of the present invention is described in detail.
Embodiment
1
A kind of Chinese herbal medicine floral water, including the raw material of following weight portion: (every part is 1kg)
Fructus Litseae essential oil 1 part, Flos Magnoliae quintessence oil 4 parts, P-Cymene 8 parts, Borneolum Syntheticum 3.0 parts, propylene glycol 1.3 parts and Tween-80, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of Tween-80 are 1:5.
Preparation method is as follows:
(1), Fructus Litseae essential oil 1kg is weighed, Flos Magnoliae quintessence oil 4kg, P-Cymene 8kg, mix homogeneously, it is thus achieved that mixed essential oil, standby；
(2), weighing Borneolum Syntheticum 3kg, join in above-mentioned mixed essential oil, stirring is fully dissolved to Borneolum Syntheticum, obtains quintessence oil phase, standby；
(3), weigh the Tween-80 of 80kg, mix homogeneously with quintessence oil phase, add propylene glycol 1.3kg, mix homogeneously, obtain mixture, standby；
(4), mixture adds purified water, be uniformly mixed, under the conditions of 4 DEG C, stand 1 week, then pass through membrane filtration, obtain filtrate；
(5), filtrate is through embedding after the assay was approved, packaging, it is thus achieved that Chinese herbal medicine floral water.
Embodiment
2
A kind of Chinese herbal medicine floral water, including the raw material of following weight portion: (every part is 2kg)
Fructus Litseae essential oil 8 parts, Flos Magnoliae quintessence oil 7 parts, P-Cymene 10 parts, Borneolum Syntheticum 2.5 parts, propylene glycol 1 part and Tween-80, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of Tween-80 are 1:6.
Preparation method is as follows:
(1), Fructus Litseae essential oil 16kg is weighed, Flos Magnoliae quintessence oil 14kg, P-Cymene 20kg, mix homogeneously, it is thus achieved that mixed essential oil, standby；
(2), weighing Borneolum Syntheticum 5kg, join in above-mentioned mixed essential oil, stirring is fully dissolved to Borneolum Syntheticum, obtains quintessence oil phase, standby；
(3), weigh the Tween-80 of 330kg, mix homogeneously with quintessence oil phase, add propylene glycol 1kg, mix homogeneously, obtain mixture, standby；
(4), mixture adds purified water, be uniformly mixed, under the conditions of 4 DEG C, stand 3 weeks, then pass through membrane filtration, obtain filtrate；
(5), filtrate is through embedding after the assay was approved, packaging, it is thus achieved that Chinese herbal medicine floral water.
Embodiment
3
A kind of Chinese herbal medicine floral water, including the raw material of following weight portion: (every part is 100g)
Fructus Litseae essential oil 5 parts, Flos Magnoliae quintessence oil 10 parts, P-Cymene 5 parts, Borneolum Syntheticum 2 parts, propylene glycol 1.5 parts and Tween-80, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of Tween-80 are 1:6.5.
Preparation method is as follows:
(1), Fructus Litseae essential oil 500g is weighed, Flos Magnoliae quintessence oil 1000g, P-Cymene 500g, mix homogeneously, it is thus achieved that mixed essential oil, standby；
(2), weighing Borneolum Syntheticum 200g, join in above-mentioned mixed essential oil, stirring is fully dissolved to Borneolum Syntheticum, obtains quintessence oil phase, standby；
(3), weigh the Tween-80 of 14.3kg, mix homogeneously with quintessence oil phase, add propylene glycol 150g, mix homogeneously, obtain mixture, standby；
(4), mixture adds purified water, be uniformly mixed, under the conditions of 4 DEG C, stand 4 weeks, then pass through membrane filtration, obtain filtrate；
(5), filtrate is through embedding after the assay was approved, packaging, it is thus achieved that Chinese herbal medicine floral water.
Embodiment
4
A kind of Chinese herbal medicine floral water, including the raw material of following weight portion: (every part is 500g)
Fructus Litseae essential oil 10 parts, Flos Magnoliae quintessence oil 1 part, P-Cymene 1 part, Borneolum Syntheticum 1.5 parts, propylene glycol 2 parts and Tween-80, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of Tween-80 are 1:5.5.
Preparation method is as follows:
(1), Fructus Litseae essential oil 5000g is weighed, Flos Magnoliae quintessence oil 500g, P-Cymene 500g, mix homogeneously, it is thus achieved that mixed essential oil, standby；
(2), weighing Borneolum Syntheticum 750g, join in above-mentioned mixed essential oil, stirring is fully dissolved to Borneolum Syntheticum, obtains quintessence oil phase, standby；
(3), weigh the Tween-80 of 37.125kg, mix homogeneously with quintessence oil phase, add propylene glycol 1000g, mix homogeneously, obtain mixture, standby；
(4), mixture adds purified water, be uniformly mixed, under the conditions of 4 DEG C, stand 2 weeks, then pass through membrane filtration, obtain filtrate；
(5), filtrate is through embedding after the assay was approved, packaging, it is thus achieved that Chinese herbal medicine floral water.
Claims (1)
1. a Chinese herbal medicine floral water, it is characterised in that be made up of the raw material of following weight portion:
Fructus Litseae essential oil 8 parts, Flos Magnoliae quintessence oil 7 parts, P-Cymene 10 parts, Borneolum Syntheticum 2.5 parts, propylene glycol 1 part and Tween-80, the gross weight of described Fructus Litseae essential oil, Flos Magnoliae quintessence oil, P-Cymene and Borneolum Syntheticum and the weight ratio of Tween-80 are 1:6；
Prepared by employing following steps:
(1), Fructus Litseae essential oil is weighed, Flos Magnoliae quintessence oil, P-Cymene, mix homogeneously, it is thus achieved that mixed essential oil, standby；
(2), weighing Borneolum Syntheticum, join in above-mentioned mixed essential oil, stirring is fully dissolved to Borneolum Syntheticum, obtains quintessence oil phase, standby；
(3), weigh Tween-80, mix homogeneously with quintessence oil phase, add propylene glycol, mix homogeneously, obtain mixture, standby；
(4), mixture adds purified water, be uniformly mixed, under the conditions of 4 DEG C, stand 1～4 week, then pass through membrane filtration, obtain filtrate；
(5), filtrate is through embedding, packaging, it is thus achieved that Chinese herbal medicine floral water.
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| CN201310612387.1A CN103610609B (en) | 2013-11-28 | 2013-11-28 | A kind of Chinese herbal medicine floral water and preparation method thereof |
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| CN201310612387.1A CN103610609B (en) | 2013-11-28 | 2013-11-28 | A kind of Chinese herbal medicine floral water and preparation method thereof |
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| CN103610609A CN103610609A (en) | 2014-03-05 |
| CN103610609B true CN103610609B (en) | 2016-08-17 |
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