CN103571010A - 一种低烟无卤阻燃电缆料 - Google Patents

一种低烟无卤阻燃电缆料 Download PDF

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CN103571010A
CN103571010A CN201310464745.9A CN201310464745A CN103571010A CN 103571010 A CN103571010 A CN 103571010A CN 201310464745 A CN201310464745 A CN 201310464745A CN 103571010 A CN103571010 A CN 103571010A
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何成龙
何源
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Abstract

本发明提供了一种低烟无卤阻燃电缆料，由下列重量份的原料制成：聚乙烯20-30、聚苯乙烯20-25、丁苯橡胶10-15、聚乙烯蜡3-6、稀土稳定剂5-8、氢氧化镁20-30、氢氧化锌20-30、聚磷酸铵10-20、甲基三甲氧基硅烷1-2、抗氧剂1010 1-4、氧化锌4-5、相容剂ST-32-4、纳米氮化铝0.1-0.3、聚乙烯醇1-2、改性填料10-12。本发明发明的电缆料，通过在配方中的偶联剂和相容剂、阻燃协效剂、改性填料的作用，使得本发明低烟无卤阻燃电缆料具有良好的加工性能和低烟阻燃性能。

Description

一种低烟无卤阻燃电缆料
技术领域
本发明涉及电缆料领域，具体涉及一种低烟无卤阻燃电缆料。
背景技术
随着全球经济的迅猛发展，及人类环保意识的增强，各领域对电线电缆的质量和性能的要求越来越高，因电线、电缆的老化而引发的火灾也越来越多，如何降低火灾的发生率及发生火灾的时的死亡率，低烟、无卤、阻燃、环保也成为电线电缆行业的发展方向。其中无卤低烟阻燃电缆料的需求量越来越大，目前无卤低烟阻燃电缆料的生产大多是在聚烯烃基材中加入大量的氢氧化镁或氢氧化镁来达到阻燃效果，然而，大量无机材料的加入，影响了电缆料的物理机械性能和加工工艺性能，其在常温下柔软性能、耐气候性差、耐油性、耐低温性能都不是很好。
发明内容
本发明提供了一种低烟无卤阻燃电缆料。
本发明采用的技术方案为：
一种低烟无卤阻燃电缆料，其特征在于：由下列重量份的原料制成：聚乙烯20-30、聚苯乙烯20-25、丁苯橡胶10-15、聚乙烯蜡3-6、稀土稳定剂5-8、氢氧化镁20-30、氢氧化锌20-30、聚磷酸铵10-20、甲基三甲氧基硅烷1-2、抗氧剂10101-4、氧化锌4-5、相容剂ST-32-4、纳米氮化铝0.1-0.3、聚乙烯醇1-2、改性填料10-12。
所述的低烟无卤阻燃电缆料，其特征在于，由包含以下重量份的组分制成：聚乙烯25、聚苯乙烯22、丁苯橡胶14、聚乙烯蜡4、稀土稳定剂7、氢氧化镁25、氢氧化锌25、聚磷酸铵15、甲基三甲氧基硅烷1、抗氧剂10102、氧化锌4、相容剂ST-33、纳米氮化铝0.2、聚乙烯醇1、改性填料11。
所述的一种低烟无卤阻燃电缆料，其特征在于，所述的改性填料是通过下列方法制备而得：
将沸石在500-550℃下煅烧3-4小时，取出后，加入3-4%的氢氧化钠溶液中研磨1-2小时，然后，加入12-15%的盐酸溶液，调节PH值为4-5，陈化10-15小时，再加氢氧化钠溶液调节研磨液pH为中性，过滤，烘干得到填料粉末，然后，向所得粉末中加入相当于粉末重量1-2%的檀香精油、4-5%纳米玉石粉、1-2%的棕榈酸锌、1-2%的硬脂酸钙、共同研磨1-2小时后，再加入相当于粉末重量2-3%的甲基三乙氧基硅烷、2-3%聚乙二醇6000、2-3%的吗啉，10000-13000转/分的高速分散均匀，即得。
本发明的电缆料的制备方法：
按配方比例称取各组分原料，将称取的组分原料，在高速混合机中搅拌均匀，再在130-160℃的温度区间下经密炼机密炼，双螺杆挤出，磨面热切造粒，旋风分离机送料，振动筛筛分然后包装，即得到电缆料成品。
有益效果
本发明发明的电缆料，通过在配方中的偶联剂和相容剂、阻燃协效剂、改性填料的作用，使得本发明低烟无卤阻燃电缆料具有良好的加工性能和低烟阻燃性能。
具体实施方式
一种低烟无卤阻燃电缆料，由下列重量（kg）的原料制成：
聚乙烯25、聚苯乙烯22、丁苯橡胶14、聚乙烯蜡4、稀土稳定剂7、氢氧化镁25、氢氧化锌25、聚磷酸铵15、甲基三甲氧基硅烷1、抗氧剂10102、氧化锌4、相容剂ST-33、纳米氮化铝0.2、聚乙烯醇1、改性填料11。
本发明的电缆料的制备方法：
按配方比例称取各组分原料，将称取的组分原料，在高速混合机中搅拌均匀，再在130-160℃的温度区间下经密炼机密炼，双螺杆挤出，磨面热切造粒，旋风分离机送料，振动筛筛分然后包装，即得到电缆料成品。
其中，改性填料是通过下列方法制备而得：
将沸石在520℃下煅烧4小时，取出后，加入4%的氢氧化钠溶液中研磨1.5小时，然后，加入15%的盐酸溶液，调节PH值为4，陈化12小时，再加氢氧化钠溶液调节研磨液pH为中性，过滤，烘干得到填料粉末，然后，向所得粉末中加入相当于粉末重量1%的檀香精油、4.5%纳米玉石粉、2%的棕榈酸锌、1%的硬脂酸钙、共同研磨2小时后，再加入相当于粉末重量3%的甲基三乙氧基硅烷、2%聚乙二醇6000、2%的吗啉，10000-13000转/分的高速分散均匀，即得。
本实施例制得的电缆料的性能测试结果如下表：
Figure BDA0000391291730000031

Claims (3)

1.一种低烟无卤阻燃电缆料，其特征在于：由下列重量份的原料制成：聚乙烯 20-30、聚苯乙烯20-25、丁苯橡胶10-15、聚乙烯蜡3-6、稀土稳定剂5-8、氢氧化镁20-30、氢氧化锌20-30、聚磷酸铵10-20、甲基三甲氧基硅烷1-2、抗氧剂1010  1-4、氧化锌4-5、相容剂ST-3 2-4、纳米氮化铝0.1-0.3、 聚乙烯醇1-2、改性填料10-12。
2.根据权利要求1所述的低烟无卤阻燃电缆料，其特征在于，由包含以下重量份的组分制成：聚乙烯 25、聚苯乙烯22、丁苯橡胶14、聚乙烯蜡4、稀土稳定剂7、氢氧化镁25、 氢氧化锌25、聚磷酸铵15、甲基三甲氧基硅烷1、抗氧剂1010 2、氧化锌4、相容剂ST-3 3、纳米氮化铝 0.2、聚乙烯醇1、改性填料11。
3.   根据权利要求1或2所述的低烟无卤阻燃电缆料，其特征在于，所述的改性填料是通过下列方法制备而得： 
将沸石在500-550℃下煅烧3-4小时，取出后，加入3-4%的氢氧化钠溶液中研磨1-2小时，然后，加入12-15%的盐酸溶液，调节PH值为4-5，陈化10-15小时，再加氢氧化钠溶液调节研磨液pH为中性，过滤，烘干得到填料粉末，然后，向所得粉末中加入相当于粉末重量1-2%的檀香精油 、4-5%纳米玉石粉、1-2%的棕榈酸锌、1-2%的硬脂酸钙、共同研磨1-2小时后，再加入相当于粉末重量2-3%的甲基三乙氧基硅烷、2-3%聚乙二醇6000、2-3%的吗啉，10000-13000转/分的高速分散均匀，即得。
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Cited By (9)

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CN105086025A (zh) * 2014-05-14 2015-11-25 中国石油天然气股份有限公司 低烟阻燃粉末丁苯橡胶及其制备方法
CN105504434A (zh) * 2015-12-15 2016-04-20 中冠电缆有限公司 一种高韧性耐火复合丁苯橡胶电缆料及其制备方法
CN105524302A (zh) * 2016-01-21 2016-04-27 安徽远征电缆科技有限公司 一种耐火防火电缆配方
CN106633453A (zh) * 2016-11-16 2017-05-10 成都市创斯德机电设备有限公司 一种交联无烟阻燃电缆料及其制备方法
CN106750797A (zh) * 2016-12-20 2017-05-31 安徽新立电缆材料有限公司 一种防水且具有优异力学性能聚乙烯电缆材料
CN107266925A (zh) * 2017-08-03 2017-10-20 安徽华能电缆集团有限公司 一种pvc电缆阻燃层电缆料
CN109369994A (zh) * 2018-11-15 2019-02-22 赛轮集团股份有限公司 一种低锌橡胶组合物
CN109608746A (zh) * 2018-12-29 2019-04-12 安徽天康(集团)股份有限公司 一种橡套电缆
CN116656033A (zh) * 2023-04-17 2023-08-29 双登电缆股份有限公司 一种含有石墨烯的抗拉伸聚乙烯电缆材料及其制备工艺

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CN106566167A (zh) * 2016-11-14 2017-04-19 安徽建筑大学 一种二茂铁改性低烟无卤阻燃电缆料

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CN101570618A (zh) * 2008-04-30 2009-11-04 北京诚联恺达科技有限公司 一种耐温型高弹性无卤阻燃热塑性弹性体的制备方法
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105086025A (zh) * 2014-05-14 2015-11-25 中国石油天然气股份有限公司 低烟阻燃粉末丁苯橡胶及其制备方法
CN105504434A (zh) * 2015-12-15 2016-04-20 中冠电缆有限公司 一种高韧性耐火复合丁苯橡胶电缆料及其制备方法
CN105524302A (zh) * 2016-01-21 2016-04-27 安徽远征电缆科技有限公司 一种耐火防火电缆配方
CN106633453A (zh) * 2016-11-16 2017-05-10 成都市创斯德机电设备有限公司 一种交联无烟阻燃电缆料及其制备方法
CN106750797A (zh) * 2016-12-20 2017-05-31 安徽新立电缆材料有限公司 一种防水且具有优异力学性能聚乙烯电缆材料
CN107266925A (zh) * 2017-08-03 2017-10-20 安徽华能电缆集团有限公司 一种pvc电缆阻燃层电缆料
CN109369994A (zh) * 2018-11-15 2019-02-22 赛轮集团股份有限公司 一种低锌橡胶组合物
CN109608746A (zh) * 2018-12-29 2019-04-12 安徽天康(集团)股份有限公司 一种橡套电缆
CN116656033A (zh) * 2023-04-17 2023-08-29 双登电缆股份有限公司 一种含有石墨烯的抗拉伸聚乙烯电缆材料及其制备工艺
CN116656033B (zh) * 2023-04-17 2024-03-01 双登电缆股份有限公司 一种含有石墨烯的抗拉伸聚乙烯电缆材料及其制备工艺

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