CN103570445A - 磷酸化浒苔寡糖粉剂肥料的制备方法 - Google Patents
磷酸化浒苔寡糖粉剂肥料的制备方法 Download PDFInfo
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- CN103570445A CN103570445A CN201210277752.3A CN201210277752A CN103570445A CN 103570445 A CN103570445 A CN 103570445A CN 201210277752 A CN201210277752 A CN 201210277752A CN 103570445 A CN103570445 A CN 103570445A
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- enteromorpha
- phosphorylation
- oligosaccharides
- fertilizer
- preparation
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- 241000196252 Ulva Species 0.000 title claims abstract description 72
- 150000002482 oligosaccharides Chemical class 0.000 title claims abstract description 65
- 229920001542 oligosaccharide Polymers 0.000 title claims abstract description 64
- 238000006366 phosphorylation reaction Methods 0.000 title claims abstract description 58
- 230000026731 phosphorylation Effects 0.000 title claims abstract description 55
- 239000003337 fertilizer Substances 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title claims abstract description 30
- 239000000843 powder Substances 0.000 title claims abstract description 25
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 13
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000011591 potassium Substances 0.000 claims abstract description 11
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 6
- 239000010452 phosphate Substances 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 150000004676 glycans Chemical class 0.000 claims description 11
- 229910052698 phosphorus Inorganic materials 0.000 claims description 11
- 229920001282 polysaccharide Polymers 0.000 claims description 11
- 239000005017 polysaccharide Substances 0.000 claims description 11
- 239000011574 phosphorus Substances 0.000 claims description 9
- 230000008901 benefit Effects 0.000 claims description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- 239000013543 active substance Substances 0.000 claims description 6
- 238000006555 catalytic reaction Methods 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 229920002097 Lichenin Polymers 0.000 claims description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 2
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 2
- 239000005648 plant growth regulator Substances 0.000 claims description 2
- OQZCJRJRGMMSGK-UHFFFAOYSA-M potassium metaphosphate Chemical compound [K+].[O-]P(=O)=O OQZCJRJRGMMSGK-UHFFFAOYSA-M 0.000 claims description 2
- 229940099402 potassium metaphosphate Drugs 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 239000004576 sand Substances 0.000 claims description 2
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 2
- 239000011573 trace mineral Substances 0.000 claims description 2
- 235000013619 trace mineral Nutrition 0.000 claims description 2
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 12
- 230000004048 modification Effects 0.000 abstract description 8
- 238000012986 modification Methods 0.000 abstract description 8
- 238000011161 development Methods 0.000 abstract description 5
- RDXARWSSOJYNLI-UHFFFAOYSA-N [P].[K] Chemical compound [P].[K] RDXARWSSOJYNLI-UHFFFAOYSA-N 0.000 abstract description 3
- 230000033228 biological regulation Effects 0.000 abstract description 2
- 230000009977 dual effect Effects 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract 2
- 241001474374 Blennius Species 0.000 abstract 1
- 239000011149 active material Substances 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 230000007071 enzymatic hydrolysis Effects 0.000 abstract 1
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 abstract 1
- 231100001261 hazardous Toxicity 0.000 abstract 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 abstract 1
- 235000019796 monopotassium phosphate Nutrition 0.000 abstract 1
- 230000000361 pesticidal effect Effects 0.000 abstract 1
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 abstract 1
- 238000001694 spray drying Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 6
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- 238000000034 method Methods 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 4
- 102000004190 Enzymes Human genes 0.000 description 2
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- 241000544058 Halophila Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
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- 229940088597 hormone Drugs 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000029936 alkylation Effects 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
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- 210000004027 cell Anatomy 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
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- 230000000749 insecticidal effect Effects 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000002786 root growth Effects 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 235000014102 seafood Nutrition 0.000 description 1
- 239000002688 soil aggregate Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000019635 sulfation Effects 0.000 description 1
- 238000005670 sulfation reaction Methods 0.000 description 1
- 230000006103 sulfonylation Effects 0.000 description 1
- 238000005694 sulfonylation reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
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- 230000002110 toxicologic effect Effects 0.000 description 1
- 231100000027 toxicology Toxicity 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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CN201210277752.3A CN103570445B (zh) | 2012-08-02 | 2012-08-02 | 磷酸化浒苔寡糖粉剂肥料的制备方法 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103980040A (zh) * | 2014-04-17 | 2014-08-13 | 青岛海大生物集团有限公司 | 一种双藻寡糖颗粒肥及其制备方法 |
CN106008094A (zh) * | 2016-05-23 | 2016-10-12 | 青岛海大生物集团有限公司 | 一种海藻钾肥及其制备方法 |
CN106305721A (zh) * | 2016-08-21 | 2017-01-11 | 青岛海大生物集团有限公司 | 一种绿藻寡糖植物疫苗及其制备方法 |
CN107324915A (zh) * | 2017-08-16 | 2017-11-07 | 日照旭日复合材料有限公司 | 一种将浒苔磨浆酶解提取营养成分及制备浒苔有机复合肥的方法 |
CN107337498A (zh) * | 2017-08-16 | 2017-11-10 | 日照旭日复合材料有限公司 | 一种利用粕类物质生产富硒有机肥的方法、富硒有机肥及其应用 |
CN107473816A (zh) * | 2017-08-16 | 2017-12-15 | 日照旭日复合材料有限公司 | 一种将浒苔磨浆液化快速提取营养成分及浒苔有机复合肥的制备方法 |
CN107500856A (zh) * | 2017-08-16 | 2017-12-22 | 日照旭日复合材料有限公司 | 一种将浒苔快速液化生产富硒有机肥的方法、富硒有机肥及其应用 |
CN110041124A (zh) * | 2019-04-23 | 2019-07-23 | 浙江工业大学 | 一种水稻专用富锌营养液及其用于生产富锌大米的方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1473798A (zh) * | 2003-06-26 | 2004-02-11 | 中国海洋大学 | 一种海藻液体肥料的生产工艺 |
CN1944353A (zh) * | 2006-10-26 | 2007-04-11 | 上海交通大学 | 海藻氨基酸稀土复合叶面肥及其制备方法 |
CN101538172A (zh) * | 2009-04-29 | 2009-09-23 | 秦怀跃 | 海藻水解的方法 |
-
2012
- 2012-08-02 CN CN201210277752.3A patent/CN103570445B/zh active Active
Patent Citations (3)
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CN1473798A (zh) * | 2003-06-26 | 2004-02-11 | 中国海洋大学 | 一种海藻液体肥料的生产工艺 |
CN1944353A (zh) * | 2006-10-26 | 2007-04-11 | 上海交通大学 | 海藻氨基酸稀土复合叶面肥及其制备方法 |
CN101538172A (zh) * | 2009-04-29 | 2009-09-23 | 秦怀跃 | 海藻水解的方法 |
Non-Patent Citations (1)
Title |
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宋玥等: "磷酸化壳寡糖制备工艺研究", 《安徽农业科学》 * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103980040A (zh) * | 2014-04-17 | 2014-08-13 | 青岛海大生物集团有限公司 | 一种双藻寡糖颗粒肥及其制备方法 |
CN103980040B (zh) * | 2014-04-17 | 2016-08-17 | 威海温喜生物科技有限公司 | 一种双藻寡糖颗粒肥及其制备方法 |
CN106008094A (zh) * | 2016-05-23 | 2016-10-12 | 青岛海大生物集团有限公司 | 一种海藻钾肥及其制备方法 |
CN106305721A (zh) * | 2016-08-21 | 2017-01-11 | 青岛海大生物集团有限公司 | 一种绿藻寡糖植物疫苗及其制备方法 |
CN107324915A (zh) * | 2017-08-16 | 2017-11-07 | 日照旭日复合材料有限公司 | 一种将浒苔磨浆酶解提取营养成分及制备浒苔有机复合肥的方法 |
CN107337498A (zh) * | 2017-08-16 | 2017-11-10 | 日照旭日复合材料有限公司 | 一种利用粕类物质生产富硒有机肥的方法、富硒有机肥及其应用 |
CN107473816A (zh) * | 2017-08-16 | 2017-12-15 | 日照旭日复合材料有限公司 | 一种将浒苔磨浆液化快速提取营养成分及浒苔有机复合肥的制备方法 |
CN107500856A (zh) * | 2017-08-16 | 2017-12-22 | 日照旭日复合材料有限公司 | 一种将浒苔快速液化生产富硒有机肥的方法、富硒有机肥及其应用 |
CN110041124A (zh) * | 2019-04-23 | 2019-07-23 | 浙江工业大学 | 一种水稻专用富锌营养液及其用于生产富锌大米的方法 |
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Address after: 266003 Shandong province Qingdao City fish Road No. 5 Applicant after: Qingdao Seawin Biotech Group Co., Ltd. Address before: 266071, room 508, Science Park, Qingdao National University, 23 East Hongkong Road, Laoshan District, Shandong, Qingdao Applicant before: Qingdao Seawin Biotech Group Co., Ltd. |
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Denomination of invention: Preparation of phosphorylated Enteromorpha oligosaccharide powder fertilizer Effective date of registration: 20210622 Granted publication date: 20160302 Pledgee: Qingdao high tech Industrial Development Zone sub branch of China Construction Bank Co.,Ltd. Pledgor: QINGDAO SEAWIN BIOTECH GROUP Co.,Ltd. Registration number: Y2021370010037 |
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Address after: 266000 No. 127 Huizhiqiao Road, Qingdao High-tech Zone, Shandong Province Patentee after: Qingdao Haida biological Group Co.,Ltd. Address before: 266003 Shandong province Qingdao City fish Road No. 5 Patentee before: QINGDAO SEAWIN BIOTECH GROUP Co.,Ltd. |
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