CN103556492B - A kind of cameleon fibre, variable color fiber dyed yarn and fabric and working method thereof - Google Patents
A kind of cameleon fibre, variable color fiber dyed yarn and fabric and working method thereof Download PDFInfo
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- CN103556492B CN103556492B CN201310515069.3A CN201310515069A CN103556492B CN 103556492 B CN103556492 B CN 103556492B CN 201310515069 A CN201310515069 A CN 201310515069A CN 103556492 B CN103556492 B CN 103556492B
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Abstract
The present invention relates to a kind of cameleon fibre, variable color fiber dyed yarn and fabric and working method thereof, produce according to following step, cotton fibre is carried out pre-treatment, carry out cation-modified process afterwards, improve the cationic of cotton fibre, the thermochromic dye of microcapsule structure is adopted to dye again, finally by fixation and oven dry, obtain temperature and become variable color cotton fibre, then adopt the spinning process of colour-spun yarns to carry out spinning and obtain variable color fiber dyed yarn, and adopt that variable color fiber dyed yarn carries out face weave, the rear operation such as whole obtains variable color look textile fabric. It is strong that product of the present invention not only has the dim sense of colour-spun yarns, stereoscopic sensation, the feature that color is implicit, natural, have levels, and there is the style that colour-changeable yarn color is changeable, randomness is strong, the present invention simultaneously adopts fiber to carry out modification, dyeing, a large amount of water resourcess can be saved, being combined by ionic linkage between dyestuff and fiber, washing fastness and color fastness are all fine, are fiber dyed yarn and the fabric of a kind of brand-new style.
Description
Technical field
The present invention relates to textile technology field, for the cameleon fibre of a kind of novel style, variable color fiber dyed yarn or fabric, specifically fiber is processed by a kind of employing microcapsule Thermo-color Dyes, then carry out spinning and face weave, obtain a kind of cameleon fibre, variable color fiber dyed yarn and the variable color look textile fabric that can vary with temperature and occur color to change.
Background technology
Fiber dyed yarn is generally with the fibre spinning resultant yarn of two kinds and two or more different color and lusters or different performance, due to the difference of various filament contraction or colouring property, during arrangement after yarn is made into cloth is processed, the style that cloth cover presents multicolour, feel is soft, surface sense is plentiful can be made, it is to increase value-added content of product. Conventional short-staple all adopts dyeing keratin-fiber to obtain coloured fibre then to carry out spinning into fiber dyed yarn, and chemical fibre adopts original liquid coloring technology to add Masterbatch in spinning solution to carry out melt-spinning fibroblast and then carry out look spinning processing substantially. Colour-spun yarns has that low cost and high added value, range of product variability be strong and multinomial advantage and the feature such as production process energy-conserving and environment-protective, changes traditional technology, it is achieved that without discharge dyeing, solves the problem that dyeing is polluted from source.
Reversible temperature-sensitive chromotropic dye is a kind of microcapsule repeatedly changing color with rise in temperature or decline, it has the organic compound objects system preparation of special chemical structure by a class, its molecule is relatively big, water-soluble poor, and dyestuff itself does not have and the functional group that cotton fibre macromole is combined. Within specified temperatures because transfer transport makes the molecular structure of this organism change, thus realize the transformation of color. Not only color is bright-coloured for this kind of Thermo-color Dyes, and repeatedly can realize the change from coloured to colourless or from colourless to coloured. Microcapsule have 0.2��0.5 micron and neither dissolve also nonfused transparent outer cover, and heat discoloration body is coated on inside by it, protect them not by the erosion of other chemical substance extraneous such that it is able to repeatedly reversible use.
Chromotropic dye is applied on fabric, mainly adopt coating interpolation tackiness agent to carry out high temperature to bake, or adopt pigment printing and coating to realize, but generally there is the defect of colour fastness difference, Boardy Feeling, poor durability, if it is unworkable for adopting conventional chromotropic dye dyeing to carry out cotton fiber dyeing, major cause has:
1, cotton fibre dyes when fluffy, if interpolation tackiness agent carries out set can make to produce between cotton fibre serious adhesion, it is very difficult to separately, also just cannot carry out the spinning processing in rear road;
2, need to carry out the washing processing in many roads after being made into fabric due to colour-spun yarns, the fastness of conventional chromotropic dye dyeing can not carry out the washing of many roads, otherwise it is serious to fade, and cannot use.
The patent No. be ZL200710032110.6 patent in also mention and adopt cation-modified liquid process cotton fabric, then adopt natural dyestuff to dye, it is to increase the dye uptake of cotton fabric, color depth and dyeing uniformity. ZL201010195278.0 also mentions and adopts cation modifier process bombax cotton, then adopt anionic dyestuff to dye, it is to increase dye uptake and shortening dyeing time, reduce the interpolation of dyeing accelerant.
But their method of modifying cannot use in microcapsule chromotropic dye, mainly there is following problem:
1, the anionic property of microcapsule is very weak, it is the shell of a kind of ball, inside is coated with heat discoloration body, the anionic property of itself is very weak, it is different from the anionic property of anionic dyestuff and natural dyestuff, if so only wishing to be combined with dyestuff by modified cation group, then dye uptake and every fastness do not reach requirement certainly, cannot use;
2, the consumption of properties-correcting agent and caustic soda is very big, properties-correcting agent is more than 10g/L, processing cost is very high, being difficult in actual production adopt, and the color of natural dyestuff is very dim, kind is also little, look flower when the uneven meeting of modification causes dyestuff to be painted, market does not have the product of Pure natural dye occur, also not to marketing, very immature.
The staining technique of chromotropic dye is applied in fiber treatment by the present invention, play the advantage of color-change technology in colour-spun yarns field and feature, change and promote the style and characteristic of colour-spun yarns, invent a kind of varying with temperature and the warm of variable color becomes the feature that fiber dyed yarn is the present invention.
Summary of the invention
The present invention provide a kind of have vary with temperature and novel cameleon fibre, variable color fiber dyed yarn and fabric that color and style change.
The present invention adopts high performance cation modifier process cotton fabric, providing cotton fabric strong cation, consumption is few, efficiency height, fully can be combined with microcapsule and form ionic linkage, adopt reactive fixing agent coating dye to be formed on the surface of fabric more firmly to combine, it is to increase every colour fastness of dyestuff and washing performance simultaneously, thus meet the service requirements of process for processing and human consumer.
Product of the present invention also realizes, by the mutual collocation of different transition interval dyestuff, a kind of mannerism presenting multiple different colours effect at different temperatures. Product of the present invention realizes mainly through techniques such as pre-treatment, cation-modified, Thermo-color Dyes specific stain, special fixation.
In order to realize the cameleon fibre of a kind of mannerism, fiber dyed yarn or fabric, reaching above-mentioned technique effect, the present invention provides following technical scheme:
A kind of cameleon fibre working method, comprises the steps:
A, pre-treatment: cotton fibre adopts scouring enzyme carry out pre-treatment, it is to increase the water absorbing properties of cotton fibre;
B, modification: adopt cation modifier that cotton fibre is carried out modification, it is to increase the cationic of fiber;
C, dyeing: adopt the Thermo-color Dyes of microcapsule structure to be dyeed by cotton fibre;
D, fixation: adopt reactive fixing agent to carry out fixation treatment, it is to increase the colour fastness of dyestuff;
E, washing, oven dry.
Preferably, in step a, scouring enzyme CBS consumption is 0.5% ~ 8%, permeate agent 1 ~ 3g/L, and temperature is 40 ~ 80 DEG C, and the time is 20 ~ 40 minutes.
Preferably, in step b, amount of modifier is 1 ~ 6g/L, and caustic soda consumption is 0.5 ~ 1.5g/L, and treatment temp is 60 ~ 80 DEG C, and the time is 20 ~ 40 minutes.
Preferably, in step c, the consumption of dyestuff is 0.01 ~ 10%(owf), dyeing temperature is 60 ~ 80 DEG C, and the consumption of levelling agent is 1 ~ 2g/L.
Preferably, in steps d, the consumption of laking agent is 10 ~ 30g/L, and temperature is 65 ~ 85 DEG C, and the time is 10 ~ 30 minutes.
Preferably, the material of fiber used is short-staple cellulose fiber, such as cotton, sky silk, Modal, viscose glue, flax.
Preferably, in step c, the transition interval of Thermo-color Dyes is 20��80 DEG C.
Preferably, in the present invention, laking agent is reactive netted film-forming color fixing agent, and dyestuff is enveloped by the reticulated structure completely fine and close in the surface formation of fabric, thus improve fastness and the washing fastness of its dyeing, the consumption of laking agent is 10 ~ 30g/L, and temperature is 65 ~ 85 DEG C, and the time is 10 ~ 30min.
The present invention also provides a kind of variable color fiber dyed yarn, and adopting above-mentioned special cameleon fibre to spin spinning system according to look, to carry out spinning obtained, obtain a kind of can with temperature variable color a kind of novel variable color fiber dyed yarn of variable color.
The present invention also provides a kind of variable color look textile fabric, be above-mentioned variable color fiber dyed yarn is carried out face weave, a kind of novel variable color look textile fabric that Final finishing obtains.
The present invention has following advantage or feature:
1, fiber is carried out cation-modified, it is to increase the ionic linkage between dyestuff and fiber combines, and adds the dye uptake of chromotropic dye, it is to increase colour fastness and weather resistance;
2, impart fiber dyed yarn and feature that fabric varies with temperature and color changes, it is a kind of brand-new fiber dyed yarn kind, unique style, it is possible to be widely used in knitting, the field such as shuttle is knitted, sweater;
3, adopting reactive fixing agent that micro-capsule dyes is carried out fixation, the surface making dyestuff be fixed on fabric forms stable combination, it is to increase the colour fastness of dyestuff and washing fastness.
Embodiment
Hereinafter the preferred embodiments of the present invention are described, it will be appreciated that preferred embodiment described herein, only for instruction and explanation of the present invention, is not intended to limit the present invention.
Embodiment 1
A working method for 60S/2 cameleon fibre, variable color colour-spun yarns and variable color fabric, comprises following procedure of processing:
1, pre-treatment: loaded in cage by egyptian cotton fiber, and compress, then carries out washing, scouring enzyme pre-treatment, removes the pectin on fiber, wax etc., and technique is: scouring enzyme 0.5g/L, permeate agent 1g/L, 80 DEG C of process 40min;
2, modification: adopting cation modifier that cotton fibre is carried out modification processing, technique is properties-correcting agent Q-01(Lu Daofu chemical industry) 5g/L and liquid caustic soda 0.5g/L, 60 DEG C of process 40min;
3, dye: cotton fibre adopts the Thermo-color Dyes of microcapsule structure dye. The formula of dyestuff is NatureGreen0.01%(owf) (Korea S Jing Ren), levelling agent 1g/L, dyeing temperature is 60 DEG C, and temperature sensing color changing temperature is 30 DEG C;
4, fixation: adopt reactive fixing agent B-6 carry out fixation processing, it is to increase every colour fastness, wherein laking agent name be called B-6(Shanghai good and) 10g/L, color fixing temperature is 65 DEG C, and the time is 30min;
5, wash;
6, dry;
7, spin: coloured fibre and the cotton essential color fiber of 80% by 20% are spun into 60S/2 variable color colour-spun yarns through mixed cotton, comb and parallel cotton fibers prior to spinning, rove, spun yarn, winder and doubling processing;
8, face weave: carrying out the colour-changeable yarn spun after singing justifying woven making, specification is 30 cun of 28 pin, obtained knit fabric;
9, Final finishing: fabric is carried out processing of washing, dry and shape, obtained 60S/2 variable color fabric.
Embodiment 2
A working method for 70S/1 cameleon fibre, polyester-cotton blend variable color colour-spun yarns and variable color fabric, comprises following procedure of processing:
1, pre-treatment: egyptian cotton fiber is loaded in cage, and compresses, then carry out washing, scouring enzyme process improve capillary effect, technique is: scouring enzyme CBS8g/L, permeate agent 3g/L, 40 DEG C of process 20min;
2, modification: adopting cation modifier that cotton fibre is carried out modification processing, technique is properties-correcting agent Q-01(Lu Daofu chemical industry) 3.5g/L and liquid caustic soda 1.5g/L, 80 DEG C of process 20min;
3, dye: cotton fibre adopts the Thermo-color Dyes of microcapsule structure dye. The formula of dyestuff is DarkBlue8%(owf) (Korea S Jing Ren), levelling agent 2g/L, dyeing temperature is 75 DEG C, and temperature sensing color changing temperature is 20 DEG C.
4, fixation: adopt reactive fixing agent B-6 carry out fixation processing, it is to increase every colour fastness, wherein laking agent name be called B-6(Shanghai good and) 30g/L, color fixing temperature is 85 DEG C, and the time is 10min;
5, wash;
6, dry;
7, spin: the coloured fibre of 50% and the polyster fibre of 50% are spun into 70S/1 variable color fiber dyed yarn through mixed cotton, comb and parallel cotton fibers prior to spinning, rove, spun yarn, winder and doubling processing;
8, face weave: by the colour-changeable yarn spun through adopting two-sided large circle machine weave, specification is 40 cun of 34 pin, obtained knit fabric;
9, Final finishing: fabric is carried out processing of washing, dry and shape, obtained 70S/1 variable color look textile fabric.
Embodiment 3
A working method for 40S/1 variable color viscose fiber, variable color colour-spun yarns and variable color fabric, comprises following procedure of processing:
1, pre-treatment: loaded in cage by viscose fiber, and compressing, then carries out washing, scouring enzyme pre-treatment, and technique is: scouring enzyme 0.5g/L, permeate agent 1g/L, 80 DEG C of process 20min;
2, modification: adopting cation modifier that cotton fibre is carried out modification processing, technique is properties-correcting agent Q-01(Lu Daofu chemical industry) 1g/L and liquid caustic soda 1.0g/L, 70 DEG C of process 30min;
3, dye: cotton fibre adopts the Thermo-color Dyes of microcapsule structure dye. The formula of dyestuff is BlackB5%(owf) (Korea S Jing Ren), levelling agent 1.5g/L, dyeing temperature is 80 DEG C, and temperature sensing color changing temperature is 30 DEG C;
4, fixation: adopt reactive fixing agent B-6 carry out fixation processing, it is to increase every colour fastness, wherein laking agent name be called B-6(Shanghai good and) 20g/L, color fixing temperature is 50 DEG C, and the time is 20min;
5, wash;
6, dry;
7, spin: coloured fibre and the viscose glue essential color fiber of 60% by 40% are spun into 40S/1 variable color colour-spun yarns through mixed cotton, rove, spun yarn, winder and doubling processing;
8, face weave: undertaken justifying woven making by the colour-changeable yarn spun, specification is 30 cun of 30 pin, obtained knit fabric;
9, Final finishing: fabric is carried out processing of washing, dry and shape, obtained 40S/1 variable color fabric.
Embodiment 4
A working method for 60S/1 variable color tencel fiber, variable color colour-spun yarns and variable color fabric, comprises following procedure of processing:
1, pre-treatment: loaded in cage by tencel fiber, and compressing, then carries out washing, scouring enzyme pre-treatment, and technique is: scouring enzyme 4.5g/L, permeate agent 2g/L, 80 DEG C of process 30min;
2, modification: adopting cation modifier that cotton fibre is carried out modification processing, technique is properties-correcting agent Q-01(Lu Daofu chemical industry) 3g/L and liquid caustic soda 1.2g/L, 65 DEG C of process 25min;
3, dye: cotton fibre adopts the Thermo-color Dyes of microcapsule structure dye. The formula of dyestuff is Navy6.2%(owf) (Korea S Jing Ren), levelling agent 2.0g/L, dyeing temperature is 60 DEG C, and temperature sensing color changing temperature is 80 DEG C;
4, fixation: adopt reactive fixing agent B-6 carry out fixation processing, it is to increase every colour fastness, wherein laking agent name be called B-6(Shanghai good and) 30g/L, color fixing temperature is 85 DEG C, and the time is 30min;
5, wash;
6, dry;
7, spin: coloured fibre and the sky silk essential color fiber of 50% by 50% are spun into 60S/1 variable color colour-spun yarns through mixed cotton, rove, spun yarn, winder and doubling processing;
8, face weave: undertaken justifying woven making by the colour-changeable yarn spun, specification is 30 cun of 36 pin, obtained knit fabric;
9, Final finishing: fabric is carried out processing of washing, dry and shape, obtained 60S/1 variable color fabric.
Embodiment 5
A working method for 32S/1 variable color flax fiber, variable color colour-spun yarns and variable color fabric, comprises following procedure of processing:
1, pre-treatment: loaded in cage by flax fiber, and compressing, then carries out washing, scouring enzyme pre-treatment, and technique is: scouring enzyme 8g/L, permeate agent 3g/L, 60 DEG C of process 40min;
2, modification: adopting cation modifier that cotton fibre is carried out modification processing, technique is properties-correcting agent Q-01(Lu Daofu chemical industry) 4g/L and liquid caustic soda 1.5g/L, 80 DEG C of process 40min;
3, dye: cotton fibre adopts the Thermo-color Dyes of microcapsule structure dye. The formula of dyestuff is RED10%(owf) (Korea S Jing Ren), levelling agent 1.5g/L, dyeing temperature is 70 DEG C, and temperature sensing color changing temperature is 60 DEG C;
4, fixation: adopt reactive fixing agent B-6 carry out fixation processing, it is to increase every colour fastness, wherein laking agent name be called B-6(Shanghai good and) 30g/L, color fixing temperature is 80 DEG C, and the time is 20min;
5, wash;
6, dry;
7, spin: coloured fibre and flax essential color fiber of 75% by 25% are spun into 32S/1 variable color colour-spun yarns through mixed cotton, comb and parallel cotton fibers prior to spinning, rove, spun yarn, winder and doubling processing;
8, face weave: undertaken justifying woven making by the colour-changeable yarn spun, specification is 30 cun of 26 pin, obtained knit fabric;
9, Final finishing: fabric is carried out mercerising, oven dry and sizing processing, obtained 32S/1 variable color fabric.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, technical scheme described in foregoing embodiments still can be modified by it, or wherein part technology feature carries out equivalent replacement. Within the spirit and principles in the present invention all, any amendment of doing, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (4)
1. a cameleon fibre working method, it is characterised in that, comprise the steps:
A, pre-treatment: cotton fibre adopts scouring enzyme carry out pre-treatment, it is to increase the water absorbing properties of cotton fibre;
B, modification: adopt cation modifier that cotton fibre is carried out modification, it is to increase the cationic of cotton fibre;
C, dyeing: adopt the Thermo-color Dyes of microcapsule structure to be dyeed by cotton fibre;
D, fixation: adopt reactive fixing agent to carry out fixation treatment, it is to increase the colour fastness of dyestuff;
E, washing, oven dry;
In step a, scouring enzyme CBS consumption is 0.5% ~ 8%, permeate agent 1 ~ 3g/L, and temperature is 40 ~ 80 DEG C, and the time is 20 ~ 40 minutes;
In step b, amount of modifier is 1 ~ 6g/L, and caustic soda consumption is 0.5 ~ 1.5g/L, and treatment temp is 60 ~ 80 DEG C, and the time is 20 ~ 40 minutes;
In step c, the consumption of dyestuff is 0.01 ~ 10%(owf), dyeing temperature is 60 ~ 80 DEG C, and the consumption of levelling agent is 1 ~ 2g/L;
In steps d, the consumption of laking agent is 10 ~ 30g/L, and temperature is 65 ~ 85 DEG C, and the time is 10 ~ 30 minutes.
2. a kind of cameleon fibre working method according to claim 1, it is characterised in that: in step c, the transition interval of Thermo-color Dyes is 20��80 DEG C.
3. a variable color fiber dyed yarn, it is characterised in that: the working method cameleon fibre that obtains of processing according to the arbitrary item of claim 1-2 is carried out pure spin or blended spinning obtains according to colour-spun yarns spinning process.
4. a variable color look textile fabric, it is characterised in that: variable color fiber dyed yarn according to claim 3 is carried out face weave, Final finishing obtains.
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| CN201310515069.3A CN103556492B (en) | 2013-10-28 | 2013-10-28 | A kind of cameleon fibre, variable color fiber dyed yarn and fabric and working method thereof |
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| CN103774307A (en) * | 2014-02-12 | 2014-05-07 | 太仓明静纺织有限公司 | Color-variable fiber and manufacturing method thereof |
| CN104499298A (en) * | 2015-01-04 | 2015-04-08 | 哈尔滨工业大学 | Temperature-indicating fiber and preparation method thereof |
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| CN105220335A (en) * | 2015-08-28 | 2016-01-06 | 太仓市鑫泰针织有限公司 | A kind of variable color viscose knit fabric |
| CN106521973A (en) * | 2016-08-31 | 2017-03-22 | 浙江科艺纺织有限公司 | Reversible thermochromic fabric |
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| CN109252367B (en) * | 2018-08-30 | 2021-12-10 | 汕头市珂玲服饰有限公司 | Thermosensitive color-changing composite fabric and preparation process thereof |
| CN108999003A (en) * | 2018-09-11 | 2018-12-14 | 陈光勇 | A kind of environmental protection surface treatment dyeing of cotton products |
| CN109208163A (en) * | 2018-10-11 | 2019-01-15 | 浙江浅秋针织服饰有限公司 | Changeable colour knitted side material manufacturing technique |
| CN109610057A (en) * | 2018-10-31 | 2019-04-12 | 武汉纺织大学 | A kind of electrochromism yarn and preparation method thereof |
| CN111621893B (en) * | 2020-05-29 | 2022-10-18 | 安踏（中国）有限公司 | Fancy yarn preparation method |
| CN112252054A (en) * | 2020-09-22 | 2021-01-22 | 鲁泰纺织股份有限公司 | Method for dyeing pure cotton yarn on line by vegetable dye |
| CN112553920B (en) * | 2020-12-10 | 2022-12-23 | 王后家纺科技有限公司 | High-quality dyeing process for cotton spinning yarns |
| CN116219771A (en) * | 2023-01-10 | 2023-06-06 | 泉州渡善科技有限公司 | Thermochromic fabric and dyeing process thereof |
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