CN103524169B - Missible oil liquid capable of preventing and treating apple valsa canker, as well as preparation method of missible oil liquid - Google Patents
Missible oil liquid capable of preventing and treating apple valsa canker, as well as preparation method of missible oil liquid Download PDFInfo
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- CN103524169B CN103524169B CN201210227614.4A CN201210227614A CN103524169B CN 103524169 B CN103524169 B CN 103524169B CN 201210227614 A CN201210227614 A CN 201210227614A CN 103524169 B CN103524169 B CN 103524169B
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- oil liquid
- missible oil
- temperature
- water
- preventing
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- 239000007788 liquid Substances 0.000 title claims abstract description 18
- 241001645362 Valsa Species 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 30
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 13
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 13
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 13
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 13
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 11
- 229930006000 Sucrose Natural products 0.000 claims abstract description 11
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000004202 carbamide Substances 0.000 claims abstract description 10
- 239000000052 vinegar Substances 0.000 claims abstract description 9
- 235000021419 vinegar Nutrition 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 4
- 238000001802 infusion Methods 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 3
- 239000012634 fragment Substances 0.000 claims description 3
- 239000013589 supplement Substances 0.000 claims description 3
- 244000061458 Solanum melongena Species 0.000 claims description 2
- 238000006073 displacement reaction Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims 1
- 235000011430 Malus pumila Nutrition 0.000 abstract description 17
- 235000015103 Malus silvestris Nutrition 0.000 abstract description 17
- 244000141359 Malus pumila Species 0.000 abstract description 14
- 241000220225 Malus Species 0.000 abstract 3
- 229910000365 copper sulfate Inorganic materials 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 1
- 230000008014 freezing Effects 0.000 abstract 1
- 238000007710 freezing Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- SWGJCIMEBVHMTA-UHFFFAOYSA-K trisodium;6-oxido-4-sulfo-5-[(4-sulfonatonaphthalen-1-yl)diazenyl]naphthalene-2-sulfonate Chemical compound [Na+].[Na+].[Na+].C1=CC=C2C(N=NC3=C4C(=CC(=CC4=CC=C3O)S([O-])(=O)=O)S([O-])(=O)=O)=CC=C(S([O-])(=O)=O)C2=C1 SWGJCIMEBVHMTA-UHFFFAOYSA-K 0.000 abstract 1
- 238000010792 warming Methods 0.000 abstract 1
- 150000001413 amino acids Chemical class 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 239000003905 agrochemical Substances 0.000 description 3
- 239000003899 bactericide agent Substances 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002420 orchard Substances 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 240000001592 Amaranthus caudatus Species 0.000 description 1
- 235000009328 Amaranthus caudatus Nutrition 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000012735 amaranth Nutrition 0.000 description 1
- 239000004178 amaranth Substances 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- UGWKCNDTYUOTQZ-UHFFFAOYSA-N copper;sulfuric acid Chemical compound [Cu].OS(O)(=O)=O UGWKCNDTYUOTQZ-UHFFFAOYSA-N 0.000 description 1
- 230000007914 freezing tolerance Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
The invention discloses missible oil liquid capable of preventing and treating apple valsa canker as well as a preparation method of the missible oil liquid. The preparation method of the missible oil liquid capable of preventing and treating the apple valsa canker comprises the following steps of cutting a piece of fresh pig skin into broken blocks of 1cm by a cutter, putting the cut pieces of fresh pig skin into a container, adding appropriate water, warming to 100 DEG C, at the same time, adding appropriate sodium hydroxide, and stewing continuously; adding a small amount of hot water for supplying evaporated moisture, stewing for about 5 hours, and adding appropriate copper sulfate when the pig skin in the container is dissolved into the water completely; adding appropriate ferrous sulfate after the copper sulfate is dissolved completely; adding vinasse vinegar, white sugar and urea sequentially when the ferrous sulfate and the copper sulfate are subjected to replacement reaction and the solution is in a color of purple red; stirring continuously at the temperature of 100 DEG C for 20 minutes; then putting out a fire and reducing the temperature; filtering when the temperature is reduced to normal temperature, and packaging into bottles, so as to obtain finished products. The missible oil liquid capable of preventing and treating the apple valsa canker is difficult to volatilize on an apple tree, resists rain wash, and simultaneously can increase the drought-resistant and freezing-resistant capabilities of tree bodies.
Description
Technical field
The present invention relates to a kind of missible oil liquid and the preparation method that can prevent and apple valsa canker can be treated, belong to agriculture field.
Background technology
Apple valsa canker is the most serious a kind of disease threatening and restrict northern China apple production, and the incidence of disease is many at 20-40%, has indivedual orchard up to more than 70%, also has many orchards to go to wreck because rot harm is serious.What use on producing for many years is all Agro-chemicals control rot, and chemicals also exists the disadvantage that namely chance water run off and simple sterilization can not have additional nutrients to tree, therefore, effect is all not satisfactory, and a kind of missible oil liquid treating apple valsa canker that can prevent provided by the invention, owing to being grease series bactericidal agent, therefore adhesion is good on tree body, retention time is long, moreover the several amino acids contained by missible oil liquid can strengthen trunk infusion, thus can improve the resistance against diseases of tree body.
Summary of the invention
The object of the present invention is to provide a kind of missible oil liquid and the preparation method that can prevent and apple valsa canker can be treated, the missible oil liquid obtained by the inventive method is used on apple tree not only not volatile, but also resistance of rainwater washing against, pollution-free to Fruits production, without poisoning, it is the ideal control agricultural chemicals producing green fruit, this product not only can prevention and therapy apple valsa canker, can also increase the drought resisting freezing tolerance of fruit tree simultaneously.
For achieving the above object, the missible oil liquid that can prevent and can treat apple valsa canker of the present invention, is characterized in that it is by the formulated agricultural chemicals of the component of following percentage by weight:
Pigskin (fresh) 4-16%
Water 30-50%
Sodium hydroxide 0.1-0.5%
Sake cake vinegar 25-55%
Copper sulphate 0.5-2%
White sugar 3-12%
Ferrous sulfate 0.5-2%
Urea 2-15%
Can prevent and can treat missible oil liquid and the preparation method of apple valsa canker, it is characterized in that it comprises the following steps:
Fresh pig skin is cleaned, be cut into the fragment of about 1 centimeter square by knife, put into container to add suitable quantity of water and heat to 100 DEG C, at this moment add appropriate sodium hydroxide and continue infusion, and constantly add some hot water and supplement the moisture content evaporated, about infusion is after 5 hours, after the pigskin in container is completely soluble in water, add moderate amount of sulfuric acid copper, moderate amount of sulfuric acid ferrous iron is added after copper sulphate dissolves completely, when copper sulphate displacement is aubergine by ferrous sulfate, successively by sake cake vinegar, white sugar and urea add, and constantly stir, 20 minutes are maintained at 100 DEG C of temperature, then fire extinguishing cooling.Filter when temperature is down to normal temperature, bottling is finished product.
A kind of missible oil liquid and preparation method that can prevent and apple valsa canker can be treated of the present invention, each component in component effect of rising be:
Pigskin: pigskin is decomposed into amino acid easily absorbed by crops through sodium hydroxide in the process of infusion, moreover because of pigskin toughness, on tree body, adhesive force is very strong on the one hand, can keep for a long time on the other hand.
Sodium hydroxide: the collagen inside pigskin can be transformed into the amino acid that can be absorbed by plants by sodium hydroxide.
Copper sulphate: copper sulphate is the natural bactericidal agent of pollution-free noresidue, be also the trace element that can be absorbed and used by plants, it can also neutralize the alkalescence in this component simultaneously.
Ferrous sulfate: ferrous sulfate is the natural bactericidal agent of pollution-free noresidue is also the trace element that can be absorbed by plants, and can also neutralize this organizes in one's duty alkalescence to ferrous sulfate simultaneously.
Sake cake vinegar: containing several amino acids in vinegar, can be absorbed and used by plants, simultaneously acetic acid and alkali neutralize crop can be made safer absorb this product.
White sugar: acid at high temperature met by white sugar can change into several amino acids.
Urea: acid at high temperature met by urea can change into several amino acids by white sugar better, can make self to transform into amino-acid nitrogen simultaneously.
embodiment:
Following examples are that the present invention is further elaborated:
Embodiment: a kind of technical ability prevention can treat again the missible oil liquid of apple valsa canker, and its component is:
Pigskin (fresh) 8%
Water 37%
Sodium hydroxide 0.2%
Sake cake vinegar 38.8%
Copper sulphate 1%
White sugar 6%
Ferrous sulfate 1%
Urea 8%
A kind of preparation method of the missible oil liquid that can prevent and can treat apple valsa canker is:
8 ㎏ fresh pig skins are cleaned, be cut into the fragment of 1 centimeter square by knife, put into container, add 37 ㎏ water, heat to 100 DEG C, at this moment add 0.2 ㎏ sodium hydroxide and continue infusion, and constantly add some hot water and supplement the moisture evaporated, about infusion is after 5 hours, 1 ㎏ copper sulphate is added after the pigskin in container is completely soluble in water, 1 ㎏ ferrous sulfate is added after copper sulphate dissolves completely, when ferrous sulfate, copper sulphate being replaced displaing amaranth is, successively by sake cake vinegar 38.8 ㎏, white sugar 6 ㎏, urea 8 ㎏ adds, continuous stirring, after white sugar and urea dissolve completely, 20 minutes are maintained at the temperature of 100 DEG C, then fire extinguishing cooling.Filter when temperature is down to normal temperature, bottling is finished product.
Claims (1)
1. can prevent and can treat a missible oil liquid for apple valsa canker, it is characterized in that it is made up of the raw material of following percentage by weight:
Fresh pig skin 4-16% water 30-50% sodium hydroxide 0.1-0.5% sake cake vinegar 25-55% copper sulphate 0.5-2% white sugar 3-12% ferrous sulfate 0.5-2% urea 2-15%,
Its preparation method comprises the following steps:
Fresh pig skin is cleaned, be cut into the fragment of about 1 centimeter square by knife, put into container to add suitable quantity of water and heat to 100 DEG C, at this moment add appropriate sodium hydroxide and continue infusion, and constantly add some hot water and supplement the moisture evaporated, after about enduring 5 hours, after the pigskin in container is completely soluble in water, add copper sulphate, ferrous sulfate is added after copper sulphate dissolves completely, when copper sulphate displacement is aubergine by ferrous sulfate, successively by sake cake vinegar, white sugar and urea add, and constantly stir, 20 minutes are maintained at 100 DEG C of temperature, then fire extinguishing cooling, filter when temperature is down to normal temperature, bottling is finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210227614.4A CN103524169B (en) | 2012-07-04 | 2012-07-04 | Missible oil liquid capable of preventing and treating apple valsa canker, as well as preparation method of missible oil liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210227614.4A CN103524169B (en) | 2012-07-04 | 2012-07-04 | Missible oil liquid capable of preventing and treating apple valsa canker, as well as preparation method of missible oil liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103524169A CN103524169A (en) | 2014-01-22 |
| CN103524169B true CN103524169B (en) | 2015-07-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210227614.4A Expired - Fee Related CN103524169B (en) | 2012-07-04 | 2012-07-04 | Missible oil liquid capable of preventing and treating apple valsa canker, as well as preparation method of missible oil liquid |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104996502A (en) * | 2015-07-15 | 2015-10-28 | 辛义华 | Drug for prevention and treatment of blossom blight of apple trees |
| CN108990971A (en) * | 2017-06-06 | 2018-12-14 | 史占彪 | The production method of seed pelleting liquid |
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| CN1048786A (en) * | 1989-07-21 | 1991-01-30 | 天津师范专科学校 | Synthetic and the application of multifunctional agricultural element |
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| CN1068561A (en) * | 1992-06-10 | 1993-02-03 | 路传章 | Production method of high-efficiency photosynthetic organic liquid fertilizer |
| CN1125040A (en) * | 1994-12-19 | 1996-06-26 | 胡瑞省 | Fruit tree germicide and preparing method thereof |
| CN1235765A (en) * | 1998-05-14 | 1999-11-24 | 黄银宝 | Pesticide for preventing and treating rot of apple tree |
| CN1248403A (en) * | 1998-09-22 | 2000-03-29 | 史占彪 | Ointment for preventing and curing rot of apple-tree and protecting wound on tree trunk, and preparation method |
| CN1294103A (en) * | 1999-10-20 | 2001-05-09 | 朱家林 | Process for preparing culture liquid used in quick soilless culture of vegetables |
| CN1413469A (en) * | 2002-06-14 | 2003-04-30 | 山西省农业科学院农产品综合利用研究所 | Chinese herbal medicine ointment preparation for preventing and curing rot of fruit tree |
| CN1844056A (en) * | 2006-04-30 | 2006-10-11 | 郜凤彬 | Multi-element high-efficiency foliar fertilizer enriched in organic matter and method for manufacturing the same |
| JP2010180069A (en) * | 2009-02-03 | 2010-08-19 | Tree Work:Kk | Pyroligneous acid addition compost and white root-rot prevention method |
| CN102276354A (en) * | 2011-06-28 | 2011-12-14 | 云南金星化工有限公司 | Foliar fertilizer with high activity organic acid and preparation process thereof |
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2012
- 2012-07-04 CN CN201210227614.4A patent/CN103524169B/en not_active Expired - Fee Related
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1048786A (en) * | 1989-07-21 | 1991-01-30 | 天津师范专科学校 | Synthetic and the application of multifunctional agricultural element |
| CN1067155A (en) * | 1991-05-30 | 1992-12-23 | 山东省化工技术开发公司 | Agricultural compound bactericide octicin solution and uses thereof |
| CN1068561A (en) * | 1992-06-10 | 1993-02-03 | 路传章 | Production method of high-efficiency photosynthetic organic liquid fertilizer |
| CN1125040A (en) * | 1994-12-19 | 1996-06-26 | 胡瑞省 | Fruit tree germicide and preparing method thereof |
| CN1235765A (en) * | 1998-05-14 | 1999-11-24 | 黄银宝 | Pesticide for preventing and treating rot of apple tree |
| CN1248403A (en) * | 1998-09-22 | 2000-03-29 | 史占彪 | Ointment for preventing and curing rot of apple-tree and protecting wound on tree trunk, and preparation method |
| CN1294103A (en) * | 1999-10-20 | 2001-05-09 | 朱家林 | Process for preparing culture liquid used in quick soilless culture of vegetables |
| CN1413469A (en) * | 2002-06-14 | 2003-04-30 | 山西省农业科学院农产品综合利用研究所 | Chinese herbal medicine ointment preparation for preventing and curing rot of fruit tree |
| CN1844056A (en) * | 2006-04-30 | 2006-10-11 | 郜凤彬 | Multi-element high-efficiency foliar fertilizer enriched in organic matter and method for manufacturing the same |
| JP2010180069A (en) * | 2009-02-03 | 2010-08-19 | Tree Work:Kk | Pyroligneous acid addition compost and white root-rot prevention method |
| CN102276354A (en) * | 2011-06-28 | 2011-12-14 | 云南金星化工有限公司 | Foliar fertilizer with high activity organic acid and preparation process thereof |
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| CN103524169A (en) | 2014-01-22 |
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