CN103505391A - A cream composition capable of being applied in spray form and its preparation method - Google Patents
A cream composition capable of being applied in spray form and its preparation method Download PDFInfo
- Publication number
- CN103505391A CN103505391A CN201310407934.2A CN201310407934A CN103505391A CN 103505391 A CN103505391 A CN 103505391A CN 201310407934 A CN201310407934 A CN 201310407934A CN 103505391 A CN103505391 A CN 103505391A
- Authority
- CN
- China
- Prior art keywords
- ammonium salt
- cream
- polyquaternary ammonium
- tridecyl alcohol
- alcohol polyethers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a cream composition capable of being applied in a spray form and a preparation method thereof. The composition is characterized by having a cosmetic cream-like appearance, being applicable to the skin in a spray form when being filled into a common spray bottle for cosmetics, and having a good moisturizing and skin-care effect. The preparation steps are as follows: 1) weighing the grease, the high molecular polymer and the surfactant according to the weight ratio of the substances, heating to 55 ℃ for dissolving, and mixing and stirring uniformly. 2) Weighing polyhydric alcohol according to the weight ratio, adding the polyhydric alcohol into water, heating and stirring the mixture to 55 ℃, stirring the mixture to dissolve the polyhydric alcohol, then adding the mixture prepared in the step 1), homogenizing the mixture for 5min by using a high-speed shearing homogenizer, and cooling the mixture by cooling and stirring to obtain the cream.
Description
Technical field
The present invention relates to a kind of cream cream composition that can use with Sprayable, belong to cosmetic field.
Background technology
Cream frost be dosage form common in cosmetic preparation for skin care product, traditional cream frost because thering is larger viscosity, conventionally can only be kept in wide mouthed bottle, and using method can only be confined to provoke the mode that mastic is smeared.The present invention adopts the collocation of surfactant and high molecular polymer, can form the cream frost with shear shinning characteristic, this cream frost there is no obvious difference with common cream frost in appearance, it is characterized in that packing into after cosmetic spray bottle, be subject in use under the extruding force effect of spraying pump head, can fast emulsion breaking, become and there is aqueous compared with high fluidity, thereby can use with Sprayable.
The preparation of cream frost need to realize by emulsifying process, and conventional emulsification temperature need to heat 70-80 ℃.The emulsifying temperature of cream cream composition of the present invention only need be heated to 55 ℃, not only can save the required heat of heating, also reduces heating-up temperature time and temperature fall time simultaneously, has improved production efficiency, has advantages of energy-conservation, low-carbon (LC).
Summary of the invention
The object of this invention is to provide a kind of cream cream composition that can use with Sprayable and preparation method thereof.
To achieve the object of the present invention, the present invention has adopted following technical scheme:
A cream cream composition of using with Sprayable, is characterized in that the component that comprises following percentage by weight:
Oils and fats in described compositions is any multiple combination of coconut oil Octyl Nitrite, Parleam, dicaprylyl carbonate, the different pelargonate of different tridecanoic acid, PPG-3 phenyl ether myristinate, isomery hexadecane, spermol ethylhexoate, Cyclomethicone, polydimethylsiloxane.
High molecular polymer in described compositions is any one or the multiple combination in sodium polyacrylate, ammonium polyacrylate, polyacrylic acid potassium, polyquaternary ammonium salt-30, polyquaternary ammonium salt-31, polyquaternium-32, polyquaternary ammonium salt-33, polyquaternary ammonium salt-34, polyquaternary ammonium salt-35, polyquaternary ammonium salt-36, polyquaternary ammonium salt-37, polyquaternary ammonium salt-38, polyquaternary ammonium salt-39, polyquaternary ammonium salt-40.
Surfactant in described compositions is one or more combinations in polysorbate-20, polysorbate-40, polysorbate-60, Polyoxyethylene Sorbitan Monooleate, polysorbate-81, tridecyl alcohol polyethers-2, tridecyl alcohol polyethers-3, tridecyl alcohol polyethers-4, tridecyl alcohol polyethers-5, tridecyl alcohol polyethers-6, tridecyl alcohol polyethers-7, tridecyl alcohol polyethers-8, tridecyl alcohol polyethers-9.
Polyhydric alcohol in described compositions is glycerol, propylene glycol, butanediol, dipropylene glycol, sorbitol, PEG-8,1, any one in 2-pentanediol, 1,3-PD or multiple combination.
The cream cream composition that can use with Sprayable of the present invention, except containing as above component, can also suitably add as required and be applicable to the common composition that cosmetics are used, as compositions such as chelating agen, antioxidant, antiseptic, essence.
The preparation method of the cream cream composition that can use with Sprayable of the present invention, concrete steps are:
(1) oils and fats, high molecular polymer, surfactant are dropped in oil phase pot successively, be heated to 55 ℃, be uniformly mixed, make it to dissolve completely, stand-by.
(2) water, polyhydric alcohol are put into emulsifying pot and be heated to 55 ℃, be uniformly mixed, make it perfect person and dissolve.
(3) by material suction emulsifying pot in oil phase pot, use while stirring high speed shear homogenizer homogenizing 5min, stir.
(4) be cooled to 40 ℃ and add essence, antiseptic, active matter, stir.
(5) evacuation, stirs, and is cooled to 35 ℃ of dischargings.
Accompanying drawing explanation
Fig. 1 is a kind of degree of hydration rate of change of the cream cream composition (I) that can use with Sprayable.
The specific embodiment
By specific embodiment, come below that the present invention is further illustrated, but these embodiment are just in order to illustrate, are not limitations of the present invention.
Embodiment 1: a kind of cream cream composition (I) that can use with Sprayable
Compositions is shown in formula table 1
Table 1
Preparation method is as follows:
(1) A component is put into oil phase pot and be heated to 55 ℃, be uniformly mixed, it is dissolved completely, stand-by.
(2) B component is put into emulsifying pot and be heated to 55 ℃, be uniformly mixed, it is dissolved completely, stand-by.
(3) A component is drawn into emulsifying pot, uses while stirring high speed shear homogenizer homogenizing 5 minutes, stir.
(4) cool to 40 ℃ C component is added to emulsifying pot, stir.
(5) stir, evacuation, cools to 35 ℃ of dischargings.
Embodiment 2: a kind of cream cream composition (II) that can use with Sprayable
Compositions is shown in formula table 2.
Table 2
Preparation method is as follows:
(1) A component is put into oil phase pot and be heated to 55 ℃, be uniformly mixed, it is dissolved completely, stand-by.
(2) B component is put into emulsifying pot and be heated to 55 ℃, be uniformly mixed, it is dissolved completely, stand-by.
(3) A component is drawn into emulsifying pot, uses while stirring high speed shear homogenizer homogenizing 5 minutes, stir.
(4) cool to 40 ℃ C component is added to emulsifying pot, stir.
(5) stir, evacuation, cools to 35 ℃ of dischargings.
Embodiment 3: a kind of cream cream composition (III) that can use with Sprayable
Compositions is shown in formula table 3.
Table 3
Preparation method is as follows:
(1) A component is put into oil phase pot and be heated to 55 ℃, be uniformly mixed, it is dissolved completely, stand-by.
(2) B component is put into emulsifying pot and be heated to 55 ℃, be uniformly mixed, it is dissolved completely, stand-by.
(3) A component is drawn into emulsifying pot, uses while stirring high speed shear homogenizer homogenizing 5 minutes, stir.
(4) cool to 40 ℃ C component is added to emulsifying pot, stir.
(5) stir, evacuation, cools to 35 ℃ of dischargings.
Embodiment 4: moisture-keeping efficacy evaluation experimental
(1) principle: the hydration status that adopts Comermeter CM825 test keratodermatitis.After test probe and contact skin, test, to the relative variation of capacitance, can obtain characterizing relative value's (degree of hydration rate of change) of hydration status by the calculating of instrument internal.Degree of hydration is less, moisture is less, and moisture is larger conversely.The calculating of degree of hydration is calculated by formula (1)
(2) experimental apparatus: Comermeter CM825 (German Courage+Khazaha company)
(3) experimental technique: 20 of healthy volunteers, 10 of male, 10 of women, the age is in 25-50 year.At isoperibol (22 ± 1 ℃), relative humidity 50 ± 5%, had a rest after 1 hour.Get appropriate sample (sample that the cream cream composition (I) that can use with Sprayable of employing is worked it out) and be applied to experimenter's left hand forearm inner side (4cm * 4cm) and right forearm inner side (4cm * 4cm).Blank (not being coated with) is tested simultaneously.Respectively at the degree of hydration state that uses 30 minutes, 1 hour, 2 hours, 3 hours, 4 hours test skin of sample.
(4) experimental result: the results are shown in shown in Fig. 1 of accompanying drawing.
Result shows, after 4 hours, the degree of hydration of sample still has 47.72%, and the cream cream composition (I) that explanation can be used with Sprayable has good moistening effect.
Claims (6)
1. the cream cream composition that energy is used with Sprayable, this cream cream composition is characterised in that the outward appearance with ordinary cosmetics cream frost, packs in the common spray bottle of used for cosmetic and can be applied to skin with Sprayable, and have well instant moistening effect; This cream cream composition is characterised in that the component that comprises following percentage by weight:
2. compositions according to claim 1, wherein said oils and fats is any multiple combination of coconut oil Octyl Nitrite, Parleam, dicaprylyl carbonate, the different pelargonate of different tridecanoic acid, PPG-3 phenyl ether myristinate, isomery hexadecane, spermol ethylhexoate, Cyclomethicone, polydimethylsiloxane.
3. compositions according to claim 1, wherein said high molecular polymer is any one or the multiple combination in sodium polyacrylate, ammonium polyacrylate, polyacrylic acid potassium, polyquaternary ammonium salt-30, polyquaternary ammonium salt-31, polyquaternium-32, polyquaternary ammonium salt-33, polyquaternary ammonium salt-34, polyquaternary ammonium salt-35, polyquaternary ammonium salt-36, polyquaternary ammonium salt-37, polyquaternary ammonium salt-38, polyquaternary ammonium salt-39, polyquaternary ammonium salt-40.
4. compositions according to claim 1, wherein said surfactant is one or more combinations in polysorbate-20, polysorbate-40, polysorbate-60, Polyoxyethylene Sorbitan Monooleate, polysorbate-81, tridecyl alcohol polyethers-2, tridecyl alcohol polyethers-3, tridecyl alcohol polyethers-4, tridecyl alcohol polyethers-5, tridecyl alcohol polyethers-6, tridecyl alcohol polyethers-7, tridecyl alcohol polyethers-8, tridecyl alcohol polyethers-9.
5. compositions according to claim 1, wherein said polyhydric alcohol is glycerol, propylene glycol, butanediol, dipropylene glycol, sorbitol, PEG-8,1, any one in 2-pentanediol, 1,3-PD or multiple combination.
6. the preparation method of the cream cream composition that can use with Sprayable claimed in claim 1, is characterized in that concrete steps are:
(1) oils and fats, high molecular polymer, surfactant are dropped in oil phase pot successively, be heated to 55 ℃, be uniformly mixed, make it to dissolve completely, stand-by.
(2) water, polyhydric alcohol are put into emulsifying pot and be heated to 55 ℃, be uniformly mixed, make it perfect person and dissolve.
(3) by material suction emulsifying pot in oil phase pot, use while stirring high speed shear homogenizer homogenizing 5min, stir.
(4) be cooled to 40 ℃ and add essence, antiseptic, active matter, stir.
(5) evacuation, stirs, and is cooled to 35 ℃ of dischargings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310407934.2A CN103505391B (en) | 2013-09-10 | 2013-09-10 | A cream composition capable of being applied in spray form and its preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310407934.2A CN103505391B (en) | 2013-09-10 | 2013-09-10 | A cream composition capable of being applied in spray form and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103505391A true CN103505391A (en) | 2014-01-15 |
| CN103505391B CN103505391B (en) | 2015-05-27 |
Family
ID=49889167
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310407934.2A Active CN103505391B (en) | 2013-09-10 | 2013-09-10 | A cream composition capable of being applied in spray form and its preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103505391B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105997837A (en) * | 2016-06-17 | 2016-10-12 | 广州岚萃贸易有限公司 | Formula of spray for removing cutin |
| CN114617781A (en) * | 2021-09-02 | 2022-06-14 | 中山中研化妆品有限公司 | Cooling and moisturizing spray and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101945644A (en) * | 2008-02-11 | 2011-01-12 | 宝洁公司 | Method and composition for reducing the drying time of hair |
-
2013
- 2013-09-10 CN CN201310407934.2A patent/CN103505391B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101945644A (en) * | 2008-02-11 | 2011-01-12 | 宝洁公司 | Method and composition for reducing the drying time of hair |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105997837A (en) * | 2016-06-17 | 2016-10-12 | 广州岚萃贸易有限公司 | Formula of spray for removing cutin |
| CN114617781A (en) * | 2021-09-02 | 2022-06-14 | 中山中研化妆品有限公司 | Cooling and moisturizing spray and preparation method thereof |
| CN114617781B (en) * | 2021-09-02 | 2023-10-24 | 中山中研化妆品有限公司 | Cooling and moisturizing spray and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103505391B (en) | 2015-05-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103191027A (en) | Solid makeup removing cream having warm sense in using process | |
| CN103202772A (en) | Cream composition with stable liquid crystal structure and preparation method thereof | |
| CN104546562A (en) | Cream for chap removal | |
| CN106491400A (en) | A kind of warm clean skin make-up remover | |
| CN105520840A (en) | Convenient, gentle and efficient no-clean cleansing spray sponge aerosol and preparation method thereof | |
| CN103505381B (en) | Double-layer makeup removal emulsion and preparation method thereof | |
| CN103505391B (en) | A cream composition capable of being applied in spray form and its preparation method | |
| CN107760498A (en) | Lemon grass craft essential oil soap and preparation method thereof | |
| CN103932896A (en) | Nano emulsion composition capable of being smeared to cream and preparation method thereof | |
| CN104490661A (en) | O/W type nano emulsion containing lemon essential oil and preparation method thereof | |
| CN105616208B (en) | A kind of aqueous full oil base color make-up composition and preparation method thereof | |
| CN106580758B (en) | A kind of oil-control water-setting cream and preparation method thereof | |
| CN104784061B (en) | Lecithin emulsification thickened systems are preparing the application in sprayable cream | |
| JP6628580B2 (en) | Hair cosmetic composition | |
| CN103054756A (en) | Ethanol-free perfume | |
| CN111110599A (en) | Transparent makeup removing cream, preparation method thereof and double-head product | |
| CN112451396B (en) | Refreshing water-in-oil type cream without silicone oil | |
| CN103479535A (en) | Cleansing oil | |
| TW201817866A (en) | Microemulsion-containing solid soap composition | |
| CN103405346B (en) | Preparation method of solid perfume | |
| EP2838492B1 (en) | Pre-blended mixtures of specific naturally sourced liquid materials structured with naturally sourced high melting point structuring material | |
| CN107822928B (en) | Face cream and preparation method thereof | |
| CA2795941A1 (en) | Shaving composition | |
| CN105769618A (en) | Surfactant composition bearing high-content oil phase | |
| KR101577796B1 (en) | Integrated cosmetic compound of basic makeup with high moisture for impregnating to pad and impregnated pad using thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 510663 No. 15, Colin Road, Guangzhou Science City, Guangzhou high tech Industrial Development Zone, Guangdong Province Patentee after: Guangzhou Huanya cosmetics technology Co.,Ltd. Address before: 510663 No. 15, Colin Road, Guangzhou Science City, Guangzhou high tech Industrial Development Zone, Guangdong Province Patentee before: GUANGZHOU HUANYA COSMETICS TECHNOLOGY Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20140115 Assignee: Guangzhou nabion Biotechnology Co.,Ltd. Assignor: Guangzhou Huanya cosmetics technology Co.,Ltd. Contract record no.: X2022980010117 Denomination of invention: The invention relates to a cream composition that can be applied in the form of spray and a preparation method thereof Granted publication date: 20150527 License type: Common License Record date: 20220712 |
|
| EE01 | Entry into force of recordation of patent licensing contract |