CN103497873B - A kind of active Gastrodia elata original plasm wine and preparation method thereof - Google Patents
A kind of active Gastrodia elata original plasm wine and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of active Gastrodia elata original plasm wine and preparation method thereof, this active Gastrodia elata original plasm wine is formulated by fresh rhizoma Gastrodiae, white wine and ancillary additions, white wine adopts buckwheat wine, liquor made from sorghum or grain fermented wine, and ancillary additions adopts one or several extracts in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo; When preparation, first, by fresh rhizoma Gastrodiae peeling, the fresh rhizoma Gastrodiae of peeling is carried out to microwave enzyme killing processing; Then add white wine defibrination, then ultra micro emulsification treatment; Finally add ancillary additions, adjust alcoholic strength, after high-pressure homogeneous, degassed processing, be distributed into bottle and obtain Gastrodia tuber juice wine. The present invention has retained whole nutrition and the functional component of fresh rhizoma Gastrodiae, bioavilability obtains larger raising, strengthen and expanded treatment and the health care of rhizoma Gastrodiae to body, production technology is simple, with short production cycle, product is more easily preserved, is transported and uses, effectively avoid active ingredient loss and contamination of products in traditional rhizoma Gastrodiae process, ensured the best in quality of product.
Description
Technical field
The invention belongs to food or health food processing technique field, relate in particular to a kind of active Gastrodia elata original plasm wineAnd preparation method thereof.
Background technology
Rhizoma Gastrodiae has another name called DINGFENGCAO, clutch grass, celestial being's pin, yellow moccasin flower, rhizoma gastrodiae etc., belongs to the orchid family, rhizoma Gastrodiae family manyYear life heterotrophism herbaceous plant. Rhizoma Gastrodiae is the conventional rare Chinese medicine of doctor at all times, so far facing of existing two thousand yearsBed applicating history is also green health treasure. Rhizoma Gastrodiae with treatment dizziness and headache, convulsions tic, numb limb,The diseases such as rheumatism, body pain, language is unsuccessful, blood vessels are obstructed, phlegm carbuncle vapour lock are good at, therefore there be " three towns ", " threeAnti-", the saying of " one mends ". Be anti-epileptic, anticonvulsion, antirheumatic, calmness, antispastic, analgesia, qi-restoratives.Modern pharmacological research shows, rhizoma Gastrodiae mainly contains four large therapeutic actions: calmness to nerve center system, anti-frightenedFaint and analgesic activity; To the cardiotonic of cardiovascular system; There is the work of resisting oxygen lack and enhancing immunologic functionWith; Meanwhile, rhizoma Gastrodiae also has good health-care effect.
Taking rhizoma Gastrodiae as main vina, as ginseng gastrodia liquor, gastrodia liquor, tonic gastrodia tuber wine, sea snake gastrodia liquor, ginseng and pilose antlerGastrodia liquor, the strong nectar of rhizoma Gastrodiae etc. Among the people with rhizoma Gastrodiae or be aided with the self-control of other Chinese medicines and steep in wine, edible or medicinalVery enumerate.
Rhodiola root is Crassulaceae, rhodiola perennial herb or undershrub wild plant. It is a kind of medicine foodDual-purpose plant resources, has and delays senility, radiation proof, anti-anoxic, antifatigue, pre-preventing tumor, strengthens and exempt fromEpidemic disease and the plurality of health care functions such as antiviral, its main function factor is rhodioloside.
Pseudo-ginseng is Araliaceae, and Panax platymiscium is Chinese distinctive rare traditional Chinese medicine, and Ye Shi China the earliestOne of medicinal and edible plant, pseudo-ginseng be just acknowledged as since ancient times have significantly promoting blood circulation and removing blood stasis, detumescence is fixedPain effect, has the good reputation in " invaluable ", " southern part of the country god grass ". There is the hemostasis of the loose stasis of blood, detumescence ding-tong itEffect. Cure mainly: fall that to flutter the stasis of blood swollen, obstruction of qi in the chest angina, the cloudy stomachache of the stasis of blood, sore, carbuncle and painful swelling etc. Be applicable to cardiovascular and cerebrovascularDisease, hypertension, high fat of blood and anaemia crowd. Its major function factor is notoginsenoside.
Gynostemma pentaphylla is Curcurbitaceae, gynostemma pentaphyllum genus herbaceous perennial vine plant, have another name called seven leaf courages, Pentapanax leschenaultii,Radix Rhodiolae, has cerebral tonic tranquillizing, protects heart Bao Mai, regulating lipid and reducing weight, body-building brute force, hypotensive, anticancer meritEffect. Gynostemma pentaphylla is rich in panaxoside, polysaccharide, and flavones, its total soap examination content is four times of the total soap two of ginseng,Long-term edible having no side effect, is described as China's " southern ginseng ", " anticancer rising star ".
Ginkgo is the plant of Ginkgoaceae Ginkgo, ginkgo biloba p.e, and the major function factor is flavonoidThing, it has the treatment deficiency syndrome of the lung and coughs and breathe heavily, coronary heart disease, angina pectoris, high fat of blood, the effect stimulating circulation.
In the prior art, the preparation of gastrodia liquor adopts dry, the direct soaking technology of fresh rhizoma Gastrodiae conventionally, and rhizoma Gastrodiae hasEffective constituent can not fully leach, or adopts fresh rhizoma Gastrodiae to squeeze the juice, and filters, Rhizoma Gastrodiae juice is added in white wine,It has lost a lot of active ingredients in rhizoma Gastrodiae, or rhizoma Gastrodiae, walnut grind with sides such as the outstanding type gastrodia liquors of wine preparationMethod, it has lost polysaccharide component in rhizoma Gastrodiae, or fresh rhizoma Gastrodiae defibrination, alcohol lixiviate, slag mixed grain fermentation againMethod, it has lost the mineral element in rhizoma Gastrodiae, and above method all exists processing step many, operates consuming time etc.Problem.
Summary of the invention
The invention provides a kind of active Gastrodia elata original plasm wine and preparation method thereof, be intended to solve existing preparation dayThe method of fiber crops wine can not extract rhizoma Gastrodiae effective ingredient effectively, the step of preparation process of gastrodia liquor, and complexity,Operate consuming time, the higher problem of production cost.
The object of the present invention is to provide a kind of active Gastrodia elata original plasm wine, this active Gastrodia elata original plasm wine by fresh rhizoma Gastrodiae,White wine and ancillary additions are formulated; The preparation weight ratio of fresh rhizoma Gastrodiae and white wine is 1:5～20, auxiliary interpolationThe preparation weight ratio of thing and fresh rhizoma Gastrodiae is 1:1～8.
Further, the alcoholic strength of this active Gastrodia elata original plasm wine is 45～55 degree.
Further, white wine adopts buckwheat wine, liquor made from sorghum or grain fermented wine.
Further, one or several in ancillary additions employing rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo are carriedGet thing.
Further, the preparation method of ancillary additions is:
Choose one or several in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo, be crushed to 60～100 orders, with50～80% edible alcohols are solvent, and solid-to-liquid ratio is 1:5～15, get after 2 times by Microwave-assisted Extraction, and solution is usedMolecule cutting quantity 2000～5000D filter membrane is at pressure 0.1～0.5MPa, and 20～50 DEG C of temperature are carried out hyperfiltration treatment,Remove large molecule and suspended particulate substance in solution, obtain the alcohol of the active small molecular that comprises institute's extraction of substanceSolution, is ancillary additions.
Another object of the present invention is to provide a kind of preparation method of active Gastrodia elata original plasm wine, this active Gastrodia elataThe preparation method of original plasm wine comprises the following steps:
Step 1, by fresh rhizoma Gastrodiae peeling, carries out microwave enzyme killing processing, microwave power to the fresh rhizoma Gastrodiae of peeling600W～800W；
Step 2, adds white wine defibrination, then by the emulsification of supermicro mill ultra micro, ultramicronising is to granularity 0.5～1 μ m;
Step 3, adds ancillary additions, adjusts alcoholic strength, alcoholic strength 45～55 degree, then through high-pressure homogeneous,Degassed processing, is distributed into bottle and obtains Gastrodia tuber juice wine, high-pressure homogeneous pressure 40～50MPa, homogenizing temperature 30～60DEG C, degassed pressure 0.04～0.07MPa.
Further, in the preparation method of this active Gastrodia elata original plasm wine, the preparation weight ratio of fresh rhizoma Gastrodiae and white wine is1:5～20, the preparation weight ratio of ancillary additions and fresh rhizoma Gastrodiae is 1:1～8.
Further, the preparation method of this active Gastrodia elata original plasm wine is: the fresh rhizoma Gastrodiae of 10Kg, clean peeling, warpHeating using microwave is to without the white heart, puts into fiberizer and adds 5Kg60 degree white wine and carry out defibrination, and rhizoma Gastrodiae slurries are through supermicro millUltra micro emulsification, ultramicronising to granularity is less than 0.5 μ m and adds 100Kg60 degree white wine, obtains A liquid for subsequent use;
10Kg rhodiola root, 10Kg gynostemma pentaphylla, is crushed to 60～100 orders, with 60% (V/V) edible alcoholFor solvent, solid-to-liquid ratio is 1:10, gets 2 times by Microwave-assisted Extraction, and filtrate is concentrated, with molecule cutting quantity 5000DFilter membrane, at pressure 0.12MP, 40 DEG C of temperature are carried out hyperfiltration treatment, obtain removing large molecule and suspended particulateThe transparent alcoholic solution of the active small molecular that thing comprises institute's extraction of substance, obtains B liquid;
Get 40KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 50 degree, through 30～35MPaHigh-pressure homogeneous, 0.05MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
Further, the preparation method of this active Gastrodia elata original plasm wine is: the fresh rhizoma Gastrodiae of 10Kg, clean peeling, warpHeating using microwave is to without the white heart, puts into fiberizer and adds 5Kg60 degree white wine and carry out defibrination, and rhizoma Gastrodiae slurries are through supermicro millUltra micro emulsification, ultramicronising to granularity is less than 0.5 μ m and adds 150Kg60 degree white wine, obtains A liquid for subsequent use;
10Kg rhodiola root, 10Kg gynostemma pentaphylla, 10Kg pseudo-ginseng, is crushed to 60～100 orders, with 50% (V/V)Edible alcohol is solvent, and solid-to-liquid ratio is 1:15, gets 2 times by Microwave-assisted Extraction, and filtrate is concentrated, with moleculeCutting quantity 3000D filter membrane, at pressure 0.15MP, 35 DEG C of temperature are carried out hyperfiltration treatment, obtain removing large pointThe transparent alcoholic solution of the active small molecular that son and suspended particulate substance comprise institute's extraction of substance, obtains B liquid;
Get 50KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 52 degree, through 30～35MPaHigh-pressure homogeneous, 0.06MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
Further, the preparation method of this active Gastrodia elata original plasm wine is: the fresh rhizoma Gastrodiae of 10Kg, clean peeling, warpHeating using microwave is to without the white heart, puts into fiberizer and adds 5Kg50 degree white wine and carry out defibrination, and rhizoma Gastrodiae slurries are through supermicro millUltra micro emulsification, ultramicronising to granularity is less than 0.8 μ m, adds 190Kg50 degree white wine, obtains A liquid standby;
10Kg rhodiola root, 10Kg ginkgo leaf, 10Kg gynostemma pentaphylla, is crushed to 60～100 orders, with 70% (V/V)Edible alcohol is solvent, and solid-to-liquid ratio is 1:15, gets 2 times by Microwave-assisted Extraction, and filtrate is concentrated, with moleculeCutting quantity 2000D filter membrane, at pressure 0.20MP, 40 DEG C of temperature are carried out hyperfiltration treatment, obtain removing large pointThe transparent alcoholic solution of the active small molecular that son and suspended particulate substance comprise institute's extraction of substance, obtains B liquid;
Get 50KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 50 degree, through 35～40MPaHigh-pressure homogeneous, 0.05MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
Active Gastrodia elata original plasm wine provided by the invention and preparation method thereof, this active Gastrodia elata original plasm wine by fresh rhizoma Gastrodiae,White wine and ancillary additions are formulated, and white wine adopts buckwheat wine, liquor made from sorghum or grain fermented wine, auxiliary interpolationThing adopts one or several extracts in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo; When preparation, first willFresh rhizoma Gastrodiae peeling, carries out microwave enzyme killing processing to the fresh rhizoma Gastrodiae of peeling; Then add white wine defibrination, by superMicro-mill ultra micro emulsification treatment; Finally add ancillary additions, adjust alcoholic strength, through high-pressure homogeneous, degassed placeReason, is distributed into bottle and obtains Gastrodia tuber juice wine; The present invention has retained whole nutrition and the functional component of fresh rhizoma Gastrodiae, rawThing availability obtains larger raising, make the treatment of rhizoma Gastrodiae to body and health care obtain further strengthening andExpansion, production technology is simple, with short production cycle, and product is more easily preserved, is transported and uses, and effectively keeps awayExempt from active ingredient loss and contamination of products in traditional rhizoma Gastrodiae process, ensured active Gastrodia elata original plasm wineBest in quality, there is stronger propagation and employment and be worth.
Brief description of the drawings
Fig. 1 is the preparation method's of the active Gastrodia elata original plasm wine that provides of the embodiment of the present invention realization flow figure.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with accompanying drawing and realityExecute example, the present invention is described in further detail. Should be appreciated that specific embodiment described hereinOnly in order to explain the present invention, and be not used in and limit invention.
The object of the present invention is to provide a kind of active Gastrodia elata original plasm wine, this active Gastrodia elata original plasm wine by fresh rhizoma Gastrodiae,White wine and ancillary additions are formulated.
In embodiments of the present invention, the alcoholic strength of this active Gastrodia elata original plasm wine is 45～55 degree.
In embodiments of the present invention, white wine adopts buckwheat wine, liquor made from sorghum or grain fermented wine.
In embodiments of the present invention, ancillary additions adopts one in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgoPlant or several extracts.
In embodiments of the present invention, the preparation method of ancillary additions is:
Choose one or several in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo, be crushed to 60～100 orders, with50～80% edible alcohols are solvent, and solid-to-liquid ratio is 1:5～15, get after 2 times by Microwave-assisted Extraction, and solution is usedMolecule cutting quantity 2000～5000D filter membrane, at pressure 0.1～0.5MPa, 20～50 DEG C of temperature are entered carry out ultrafiltration placeReason, removes large molecule and suspended particulate substance in solution, the active small molecular that acquisition comprises institute's extraction of substanceAlcoholic solution, is ancillary additions.
Fig. 1 shows the preparation method's of the active Gastrodia elata original plasm wine that the embodiment of the present invention provides realization flow.
This preparation method comprises the following steps:
Step S101, by fresh rhizoma Gastrodiae peeling, carries out microwave enzyme killing processing to the fresh rhizoma Gastrodiae of peeling;
Step S102, adds white wine defibrination, then ultra micro emulsification;
Step S103, adds ancillary additions, adjusts alcoholic strength, through high-pressure homogeneous, degassed processing, packingEnter bottle and obtain Gastrodia tuber juice wine.
In embodiments of the present invention, the preparation weight ratio of fresh rhizoma Gastrodiae and white wine is 1:5～20, ancillary additions withThe preparation weight ratio of fresh rhizoma Gastrodiae is 1:1～8.
Below in conjunction with drawings and the specific embodiments, application principle of the present invention is further described.
The present invention adopts technical scheme as follows:
This active Gastrodia elata original plasm wine is taking rhizoma Gastrodiae and white wine as primary raw material, and it is formulated to add ancillary additions.
By the peeling of fresh rhizoma Gastrodiae, after microwave enzyme killing is processed, add proper amount of white spirit defibrination, then ultra micro emulsification, addAncillary additions, adjust alcoholic strength, then further through high-pressure homogeneous, degassed, be distributed into bottle rhizoma Gastrodiae formerSlurry wine;
Ancillary additions is one or several extracts in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo, pulverizesTo 60～100 orders, be taking 50～80% edible alcohols as solvent, solid-to-liquid ratio is 1:5～15, assists by microwaveExtract after 2 times, molecule cutting quantity 2000～5000D filter membrane for solution, in pressure 0.1～0.5MPa, temperature20～50 DEG C are carried out hyperfiltration treatment, remove the extract of large molecule and suspended particulate substance, comprise institute's extraction of substanceThe alcoholic solution of active small molecular.
The preparation weight ratio of fresh rhizoma Gastrodiae and white wine is 1:5～20, and white wine is that buckwheat wine, liquor made from sorghum or other grain are sent outThe wine of ferment, the preparation weight ratio of ancillary additions and fresh rhizoma Gastrodiae is 1:1～8.
The alcoholic strength of active Gastrodia elata original plasm wine is 45～55 degree.
Embodiment 1:
The fresh rhizoma Gastrodiae of 10Kg, cleans, peeling, and heated by microwave, to without the white heart, is put into fiberizer and is added 5Kg60Degree white wine carries out defibrination, and rhizoma Gastrodiae slurries are through the emulsification of supermicro mill ultra micro, and ultramicronising to granularity is less than 0.5 μ m and addsEnter 100Kg60 degree white wine, obtain A liquid for subsequent use.
10Kg rhodiola root, 10Kg gynostemma pentaphylla, is crushed to 60～100 orders, with 60% (V/V) edible alcoholFor solvent, solid-to-liquid ratio is 1:10, gets 2 times by Microwave-assisted Extraction, and filtrate is concentrated, with molecule cutting quantity 5000DFilter membrane, at pressure 0.12MP, 40 DEG C of temperature are carried out hyperfiltration treatment, obtain removing large molecule and suspended particulateThe transparent alcoholic solution of the active small molecular that thing comprises institute's extraction of substance, obtains B liquid.
Get 40KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 50 degree, through 30～35MPaHigh-pressure homogeneous, 0.05MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
Embodiment 2:
The fresh rhizoma Gastrodiae of 10Kg, cleans, peeling, and heated by microwave, to without the white heart, is put into fiberizer and is added 5Kg60Degree white wine carries out defibrination, and rhizoma Gastrodiae slurries are through the emulsification of supermicro mill ultra micro, and ultramicronising to granularity is less than 0.5 μ m and addsEnter 150Kg60 degree white wine, obtain A liquid for subsequent use.
10Kg rhodiola root, 10Kg gynostemma pentaphylla, 10Kg pseudo-ginseng, is crushed to 60～100 orders, with 50% (V/V)Edible alcohol is solvent, and solid-to-liquid ratio is 1:15, gets 2 times by Microwave-assisted Extraction, and filtrate is concentrated, with moleculeCutting quantity 3000D filter membrane, at pressure 0.15MP, 35 DEG C of temperature are carried out hyperfiltration treatment, obtain removing large pointThe transparent alcoholic solution of the active small molecular that son and suspended particulate substance comprise institute's extraction of substance, obtains B liquid.
Get 50KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 52 degree, through 30～35MPaHigh-pressure homogeneous, 0.06MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
Embodiment 3:
The fresh rhizoma Gastrodiae of 10Kg, cleans, peeling, and heated by microwave, to without the white heart, is put into fiberizer and is added 5Kg50Degree white wine carries out defibrination, and rhizoma Gastrodiae slurries are through the emulsification of supermicro mill ultra micro, and ultramicronising to granularity is less than 0.8 μ m,Add 190Kg50 degree white wine, obtain A liquid standby.
10Kg rhodiola root, 10Kg ginkgo leaf, 10Kg gynostemma pentaphylla, is crushed to 60～100 orders, with 70% (V/V)Edible alcohol is solvent, and solid-to-liquid ratio is 1:15, gets 2 times by Microwave-assisted Extraction, and filtrate is concentrated, with moleculeCutting quantity 2000D filter membrane, at pressure 0.20MP, 40 DEG C of temperature are carried out hyperfiltration treatment, obtain removing large pointThe transparent alcoholic solution of the active small molecular that son and suspended particulate substance comprise institute's extraction of substance, obtains B liquid.
Get 50KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 50 degree, through 35～40MPaHigh-pressure homogeneous, 0.05MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
The active Gastrodia elata original plasm wine that the present invention obtains, has retained whole nutrition and the functional component of fresh rhizoma Gastrodiae,Bioavilability obtains larger raising, and treatment and the health care of rhizoma Gastrodiae to body further strengthenedAnd expansion, product is more easily preserved, is transported and uses, due to the work of having avoided in traditional rhizoma Gastrodiae processProperty composition loss and contamination of products, ensured the best in quality of this product.
Active Gastrodia elata original plasm wine that the embodiment of the present invention provides and preparation method thereof, this active Gastrodia elata original plasm wine byFresh rhizoma Gastrodiae, white wine and ancillary additions are formulated, and white wine adopts buckwheat wine, liquor made from sorghum or grain fermented wine,Ancillary additions adopts one or several extracts in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo; When preparation,First by fresh rhizoma Gastrodiae peeling, the fresh rhizoma Gastrodiae of peeling is carried out to microwave enzyme killing processing; Then add white wine defibrination,After ultra micro emulsification treatment; Finally add ancillary additions, adjust alcoholic strength, through high-pressure homogeneous, degassedProcess, be distributed into bottle and obtain Gastrodia tuber juice wine; The present invention has retained whole nutrition and the functional component of fresh rhizoma Gastrodiae,Bioavilability obtains larger raising, and treatment and the health care of rhizoma Gastrodiae to body further strengthenedAnd expansion, production technology is simple, with short production cycle, and product is more easily preserved, is transported and uses, effectivelyAvoid active ingredient loss and contamination of products in traditional rhizoma Gastrodiae process, ensured active Gastrodia elata original plasm wineBest in quality, there is stronger propagation and employment and be worth.
These are only preferred embodiment of the present invention, not in order to limit the present invention, all of the present inventionAny amendment of doing within spirit and principle, be equal to replacement and improvement etc., all should be included in guarantor of the present inventionWithin protecting scope.
Claims (4)
1. an active Gastrodia elata original plasm wine, is characterized in that, this active Gastrodia elata original plasm wine is joined by fresh rhizoma Gastrodiae, white wine and ancillary additionsSystem forms; The preparation weight ratio of fresh rhizoma Gastrodiae and white wine is 1: 5～20, the preparation weight ratio of ancillary additions and fresh rhizoma Gastrodiae be 1: 1～8；
The alcoholic strength of this active Gastrodia elata original plasm wine is 45～55 degree;
White wine adopts buckwheat wine or liquor made from sorghum;
Ancillary additions adopts one or several extracts in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo;
The preparation method of this active Gastrodia elata original plasm wine comprises the following steps:
Step 1, by fresh rhizoma Gastrodiae peeling, carries out microwave enzyme killing processing, microwave power 600W～800W to the fresh rhizoma Gastrodiae of peeling;
Step 2, adds white wine defibrination, then by the emulsification of supermicro mill ultra micro, ultramicronising is to granularity 0.5～1 μ m;
Step 3, adds ancillary additions, adjusts alcoholic strength, alcoholic strength 45～55 degree, then through high-pressure homogeneous, degassed placeReason, is distributed into bottle and obtains Gastrodia tuber juice wine, high-pressure homogeneous pressure 40～50MPa, 30～60 DEG C of homogenizing temperatures, degassed pressure0.04～0.07MPa；
The preparation method of ancillary additions is:
Choose one or several in rhodiola root, pseudo-ginseng, gynostemma pentaphylla, ginkgo, be crushed to 60～100 orders, with 50～80% foodsWith alcohol be solvent, solid-to-liquid ratio is 1: 5～15, get after 2 times by Microwave-assisted Extraction, molecule cutting quantity 2000 for solution～5000D filter membrane is at pressure 0.1～0.5MPa, and 20～50 DEG C of temperature are carried out hyperfiltration treatment, remove large molecule and suspension in solutionParticle, the alcoholic solution of the active small molecular that acquisition comprises institute's extraction of substance, is ancillary additions.
2. a preparation method for active Gastrodia elata original plasm wine, is characterized in that, the preparation method of this active Gastrodia elata original plasm wine is: 10KgFresh rhizoma Gastrodiae, cleans, peeling, and heated by microwave is to without the white heart, puts into fiberizer and adds 5Kg60 degree white wine and carry out defibrination, rhizoma GastrodiaeSlurries are through the emulsification of supermicro mill ultra micro, and ultramicronising to granularity is less than 0.5 μ m and adds 100Kg60 degree white wine, obtains A liquid standbyWith;
10Kg rhodiola root, 10Kg gynostemma pentaphylla, is crushed to 60～100 orders, and taking 60% edible alcohol as solvent, solid-to-liquid ratio is1: 10, to get 2 times by Microwave-assisted Extraction, filtrate is concentrated, with molecule cutting quantity 5000D filter membrane, at pressure 0.12MPa,40 DEG C of temperature are carried out hyperfiltration treatment, obtain removing active small molecular that large molecule and suspended particulate substance comprise institute's extraction of substance thoroughlyBright solution B liquid;
Get 40KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 50 degree, equal through 30～35MPa high pressureMatter, 0.05MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
3. a preparation method for active Gastrodia elata original plasm wine, is characterized in that, the preparation method of this active Gastrodia elata original plasm wine is: 10KgFresh rhizoma Gastrodiae, cleans, peeling, and heated by microwave is to without the white heart, puts into fiberizer and adds 5Kg60 degree white wine and carry out defibrination, rhizoma GastrodiaeSlurries are through the emulsification of supermicro mill ultra micro, and ultramicronising to granularity is less than 0.5 μ m and adds 150Kg60 degree white wine, obtains A liquid standbyWith;
10Kg rhodiola root, 10Kg gynostemma pentaphylla, 10Kg pseudo-ginseng, is crushed to 60～100 orders, taking 50% edible alcohol as moltenAgent, solid-to-liquid ratio is 1: 15, gets 2 times by Microwave-assisted Extraction, filtrate is concentrated, and with molecule cutting quantity 3000D filter membrane, is pressingPower 0.15MPa, 35 DEG C of temperature are carried out hyperfiltration treatment, obtain removing the activity that large molecule and suspended particulate substance comprise institute's extraction of substanceMicromolecular clear solution B liquid;
Get 50KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 52 degree, equal through 30～35MPa high pressureMatter, 0.06MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
4. a preparation method for active Gastrodia elata original plasm wine, is characterized in that, the preparation method of this active Gastrodia elata original plasm wine is: 10KgFresh rhizoma Gastrodiae, cleans, peeling, and heated by microwave is to without the white heart, puts into fiberizer and adds 5Kg50 degree white wine and carry out defibrination, rhizoma GastrodiaeSlurries are through the emulsification of supermicro mill ultra micro, and ultramicronising to granularity is less than 0.8 μ m, add 190Kg50 degree white wine, obtain A liquid standbyWith;
10Kg rhodiola root, 10Kg ginkgo leaf, 10Kg gynostemma pentaphylla, is crushed to 60～100 orders, taking 70% edible alcohol asSolvent, solid-to-liquid ratio is 1: 15, gets 2 times by Microwave-assisted Extraction, filtrate is concentrated, with molecule cutting quantity 2000D filter membrane,Pressure 0.20MPa, 40 DEG C of temperature are carried out hyperfiltration treatment, obtain removing the work that large molecule and suspended particulate substance comprise institute's extraction of substanceThe micromolecular clear solution B liquid of property;
Get 50KgB liquid and add in A liquid, mix, adjusting alcoholic strength is 50 degree, equal through 35～40MPa high pressureMatter, 0.05MPa is degassed, be distributed into bottle Gastrodia tuber juice wine.
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| CN1566316A (en) * | 2003-07-08 | 2005-01-19 | 刘建华 | Process for making tuber of elevated gastrodia wine |
| CN1522747A (en) * | 2003-08-26 | 2004-08-25 | 江苏康缘药业股份有限公司 | Drug for treating coronary heart disease or coronary disease and cardiac insufficiency, and its preparation method |
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Effective date of registration: 20231125 Address after: No. 101, Building 10, Wumenggu Town, Longquan Street, Zhaoyang District, Zhaotong City, Yunnan Province, 657099 Patentee after: Yunnan Bangming Tianma Biotechnology Co.,Ltd. Address before: 650224 School of Science, Southwest Forestry University, Xiaoba Bailong Temple, Kunming City, Yunnan Province Patentee before: Liu Xiangyi |