CN103484240A - Barley pest larva cosmetic matrix oil and preparing method thereof - Google Patents
Barley pest larva cosmetic matrix oil and preparing method thereof Download PDFInfo
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- CN103484240A CN103484240A CN201310420644.1A CN201310420644A CN103484240A CN 103484240 A CN103484240 A CN 103484240A CN 201310420644 A CN201310420644 A CN 201310420644A CN 103484240 A CN103484240 A CN 103484240A
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Abstract
The invention relates to barley pest larva cosmetic matrix oil and a preparing method thereof. According to the preparingn method, a series of processes like drying dehydration, squeezing oil extraction and oil purification are conducted to obtain barley pest larva cosmetic matrix oil. The preparing method avoids the situation that frequently-used extraction methods like organic solvent lixiviation process and heating dissolving process, and purification processes like hydration degumming and caustic refining deacidification cause pollution of chemical reagent and loss of Vitamin E and other functional components. The barley pest larva cosmetic matrix oil prepared in the method is shallow in color and luster, high in transparency, rich in unsaturated essential fatty acid, keeps active ingredients in barley pest oil, and therefore has the advantages of being strong in moisture retention and good in oxidation resistance effect. The barley pest larva cosmetic matrix oil prepared in the method contains collagen, has the advantages of animal oil and vegetable oil, and therefore is suitable for skin types of various people, has better affinity, permeability and the like, and is absorbed and used by skin easily, and the skin is smooth and not greasy after using the barley pest larva cosmetic matrix oil.
Description
Technical field
The present invention relates to a kind of cosmetic base oil and preparation method thereof, refer in particular to a kind of barley worm larva cosmetic base oil and preparation method thereof, belong to the makeup technical field.
Background technology
Grease can suppress the moisture evaporation, prevents chapped skin, makes the stratum corneum of dry skin and sclerosis rehydrated, makes stratum corneum recover softness and elasticity, and therefore, grease is moisturizing and moisturizing composition main in makeup.At present, the grease used in makeup is mainly mineral oil, vegetables oil, animal oil and Synthetic Oil, wherein the animal quasi-grease only have lanolin and snake oil etc. a few, as for insect oil, also in makeup, do not apply.The raw material of production cosmetic base oil involved in the present invention is the current insect larvae of large-scale cultivation; these insect fecundities are strong, feeding cost is low; and the functional components such as rich in vitamin E, Sitosterol, Yelkin TTS, collagen protein in its grease; there is the flexibility that keeps skin and there is the effect of the external environment resisted to the infringement of skin; in addition; also being rich in these insect greases that oleic acid, linolic acid etc. are undersaturated must lipid acid, for the nutrition of promoting skin and prevent the lost significant of epidermis moisture.
At present; applying more grease extracting method is organic solvent lixiviation process, heating stripping method and supercritical extraction etc.; purification process commonly used is hydration degum; alkali-refining deacidification; activated carbon decolorizing etc.; these extract and purification process often can bring the functional components such as the pollution of chemical reagent and vitamin-E, Sitosterol, Yelkin TTS to lose, and make the use of the cosmetic base oil produced be subject to certain limitation and reduce its nutritive value.
Summary of the invention
In view of this, the object of the present invention is to provide a kind of barley worm larva cosmetic base oil and preparation method thereof, this matrix oil be the grease of the barley worm larva that cultivates be prepared by raw material.
For achieving the above object, the invention provides a kind of preparation method of barley worm larva cosmetic base oil, comprise the following steps:
1) sterilizing and drying and dehydrating: will screen and clean (through the washed with de-ionized water 3-5min of 60-90 ℃, to remove dirt and to make barley worm larva not creep) the barley worm larva that crosses is laid on the travelling belt of microwave dryer and carries out sterilizing and drying and dehydrating, store at the temperature of 0-5 ℃ after the barley worm larva after drying and dehydrating utilizes plastic sealing bag to seal up for safekeeping;
2) oil is carried in squeezing:
2.1) preheat: the barley worm larva of storage is laid on the travelling belt of microwave dryer and is preheated;
2.2) the hydraulic pressure squeezing: the barley worm larva after preheating is packed into rapidly in the cavity of hydraulic oil press to pressurised extraction 2-15min;
3) clarifying grease:
3.1) dregs of fat separation: the temperature that the hydraulic pressure squeezing is obtained is carried out dregs of fat separation to obtain thick oil by flame filter press at once at the crude oil of 50-80 ℃, and change in time filter cloth (with the temperature that guarantees grease in filtration procedure at 50-80 ℃, thus prevent temperature reduce the grease viscosity of bringing increase the dregs of fat are separated to the impact caused);
3.2) the de-flavor of decolouring: the thick oil obtained directly is preheating to 40-80 ℃, add and the synthermal sorbent material of oil, stir while adding, churning time is 20-90min, stirring velocity is 60-200r/min, get the top absolute oil after staticly settling 30-40 minute after stirring, obtain described barley worm larva cosmetic base oil.
As preferred version, step 1 wherein) density of putting of described barley worm larva is 10-40 bar/square decimeter.
As preferred version, step 1 wherein) service rating of described microwave dryer is 1-18KW.
As preferred version, step 1 wherein) the travelling belt travelling speed of described microwave dryer is 2-10mm/s, and the travelling belt width is 40-120cm.
As preferred version, step 1 wherein) water content of the barley worm larva polypide after described drying and dehydrating is 3-9%, and surface color is without crossing thermogenetic coke black.
As preferred version, step 2 wherein) density of putting of described barley worm larva is 10-30 bar/square decimeter.
As preferred version, step 2 wherein) service rating of described microwave dryer is 1-10KW.
As preferred version, step 2 wherein) the travelling belt travelling speed of described microwave dryer is 5-15mm/s, and the travelling belt width is 40-120cm.
As preferred version, step 2 wherein) described pre-warmed temperature is 50-80 ℃, and the polypide temperature after described preheating is 50-80 ℃.
As preferred version, step 2 wherein) cavity volume of described hydraulic oil press is 2-20L, and squeeze pressure is 10-50MP, and cavity temperature is 60-90 ℃.
As preferred version, step 3 wherein) the filter screen particle diameter of described flame filter press is the 30-60 order.
As preferred version, step 3 wherein) consisting of of described sorbent material: 60-100 purpose silicon-dioxide or atlapulgite 50-80wt%; The fat-soluble silica gel 10-30wt% of 100-200 purpose; 100-200 purpose aluminum oxide 10-20wt%.
The present invention also provides a kind of barley worm larva cosmetic base oil, and described barley worm larva cosmetic base oil makes by above-mentioned preparation method.
Those skilled in the art can pass through in conjunction with prior art or common practise, utilize preparation method of the present invention good to loft, fat content is higher, and the raw material that is rich in the fat-soluble functional components such as unsaturated fatty acids and vitamin-E, Sitosterol, collagen protein in grease is processed to produce cosmetic base oil.The preparation method of barley worm larva of the present invention, go for the larva of all tenebrionids such as tenebrio molitor, brown mealworm, dark mealworm.
The present invention has following beneficial effect:
1, the present invention is by microwave drying, the squeezing of low temperature hydraulic pressure and physical method purify the barley worm larva cosmetic base oil of preparation, avoided organic solvent lixiviation process commonly used, extracting method and the hydration degums such as heating stripping method, the loss of the functional components such as the pollution of the chemical reagent that the purification process such as alkali-refining deacidification bring and vitamin-E, prepared matrix oil lighter color, transparency is high, when being rich in undersaturated necessary lipid acid, also retained to greatest extent the activeconstituents in barley worm grease, therefore there is performance of keeping humidity strong, the advantages such as antioxidant effect is good,
2, preparation method of the present invention, its technique is simple, workable, adopt the fecundity of barley worm strong, feeding cost is low, and, because protein content in the grouts that obtain after low temperature pressing is high, nutritive ingredient is destroyed few, without chemical agent residue, make it there is lower production cost;
3, the prepared barley worm larva cosmetic base oil of the present invention, contain collagen protein, have the advantage of animal grease and Vegetable oil lipoprotein concurrently, therefore be suitable for all kinds of crowds' skin type, there is affinity, perviousness, diffustivity, the gentle skin of moisturizing preferably, easily be absorbed by the skin utilization, with rear smooth and non-greasy;
4, preparation method of the present invention, its from former expect extract and scavenging process all meets the advanced persons' such as green, natural, environmental protection consumption requirement and theory fully, therefore, its application prospect in cosmetic industry is extensive.
Embodiment:
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
The preparation method of the barley worm larva cosmetic base oil that the present embodiment provides comprises the following steps:
1) sterilizing and drying and dehydrating: will screen and clean (through the washed with de-ionized water 3-5min of 60-90 ℃, to remove dirt and to make barley worm larva not creep) the barley worm larva that crosses is (commercial, the heavy 0.6-0.8g of worm) be laid on the travelling belt of microwave dryer and carry out sterilizing and drying and dehydrating (instantaneous reach 100 ℃, can not make the active substance inactivation in barley worm larva); Wherein putting density is 20-25 bar/square decimeter, the travelling belt travelling speed is 5mm/s, and the travelling belt width is 50cm, and the service rating of microwave dryer is 15KW, the water content of barley worm larva polypide after drying and dehydrating is 8%, and surface color is without crossing thermogenetic coke black; After utilizing plastic sealing bag to seal up for safekeeping, barley worm larva after dehydration stores at the temperature of 0-5 ℃;
2) oil is carried in squeezing:
2.1) preheat: the barley worm larva of storage is laid on the travelling belt of microwave dryer and is preheated (65-70 ℃); Wherein putting density is 20-25 bar/square decimeter, and the travelling belt travelling speed is 10mm/s, and the travelling belt width is 50cm, and the service rating of microwave dryer is 8KW, and after heating, the temperature of barley worm larva polypide is 65-70 ℃;
2.2) hydraulic pressure squeezing: the barley worm larva after preheating is packed into rapidly in the cavity of hydraulic oil press and carries out the hydraulic pressure squeezing; Wherein cavity volume is 10L, and squeeze pressure is 40MP, and cavity temperature is 80 ℃, and the pressurised extraction time is 10min;
3) clarifying grease:
3.1) dregs of fat separate: the temperature that the hydraulic pressure squeezing is obtained at the crude oil of 65-70 ℃ at once by flame filter press (the filter screen particle diameter is the 30-60 order), and change in time filter cloth carry out dregs of fat separation (with the temperature that guarantees grease in filtration procedure at 65-70 ℃, thus prevent temperature reduce the grease viscosity of bringing increase the dregs of fat are separated to the impact caused) to obtain thick oil;
3.2) the de-flavor of decolouring: the thick oil obtained directly is preheating to 50 ℃, and add and the synthermal sorbent material of thick oil, stir while adding, churning time is 40min, stirring velocity is 100r/min, get the top absolute oil after staticly settling 30min after stirring, obtain described barley worm larva cosmetic base oil, its physical and chemical index is as shown in table 1.
Step 3 wherein) consisting of of described sorbent material: 60-100 purpose silicon-dioxide 80wt%; The fat-soluble silica gel 10wt of 100-200 purpose %; 100-200 purpose aluminum oxide 10wt %.
The physical and chemical index analysis of the resulting barley worm of embodiment 1 larva cosmetic base oil and makeup vegetables oil commonly used
The physical and chemical index of table 1 barley worm larva cosmetic base oil
The physical and chemical index of table 2 makeup vegetables oil commonly used
By table 1, table 2, can be found out, vegetables oil comparing result commonly used in the physical and chemical index of the barley worm larva cosmetic base oil before and after refining and makeup shows:
(1) the barley worm oil after refining substantially meets the standard of cosmetic oil on acid number;
(2) iodine number, saponification value and the Prunus amygdalus oil of barley worm larva cosmetic base oil are more approaching, belong to typical nondrying oil; Be widely used as the base starting material of the oil-based cosmetic preparations such as cream kind makeup and hair oil due to Prunus amygdalus oil, and there is good skin care, hair care, the effect such as soft and smooth, moist, can infer that barley worm larva cosmetic base oil also can add in cosmetic base, and there is certain skin care humidity-holding effect;
(3) density of contrast barley worm larva cosmetic base oil and vegetables oil can be found out, the density of barley worm larva cosmetic base oil is less, and this may be relevant with composition with the composition of barley worm larva cosmetic base oil; Barley worm larva cosmetic base oil contains more short chain fatty acid; Known according to pertinent data, the olive oil viscosity is in the 81cP left and right, and barley worm larva cosmetic base oil viscosity is 62.1cP, this shows that barley worm larva cosmetic base oil viscosity is less than vegetables oil, is added in makeup and may makes skin feel salubriouser.
These are only the preferred embodiment that the present invention is cited, not in order to limit the scope of the invention, the those of ordinary skill in affiliated technical field uses the equivalence that the present invention does modify or change, all with belonging to scope of patent protection of the present invention.
Claims (10)
1. the preparation method of a barley worm larva cosmetic base oil is characterized in that: comprise the following steps:
1) sterilizing and drying and dehydrating: the barley worm larva that will screen and clean is laid on the travelling belt of microwave dryer and carries out sterilizing and drying and dehydrating, after the barley worm larva after drying and dehydrating utilizes plastic sealing bag to seal up for safekeeping, at the temperature of 0-5 ℃, stores;
2) oil is carried in squeezing:
2.1) preheat: the barley worm larva of storage is laid on the travelling belt of microwave dryer and is preheated;
2.2) the hydraulic pressure squeezing: the barley worm larva after preheating is packed into rapidly in the cavity of hydraulic oil press to pressurised extraction 2-15min;
3) clarifying grease:
3.1) dregs of fat separation: the temperature that the hydraulic pressure squeezing is obtained is passed through flame filter press at once at the crude oil of 50-80 ℃, carries out dregs of fat separation to obtain thick oil;
3.2) the de-flavor of decolouring: the thick oil obtained directly is preheating to 40-80 ℃, add and the synthermal sorbent material of oil, stir while adding, churning time is 20-90min, stirring velocity is 60-200r/min, get the top absolute oil after staticly settling 30-40 minute after stirring, obtain described barley worm larva cosmetic base oil.
2. preparation method according to claim 1, is characterized in that: step 1) density of putting of described barley worm larva is 10-40 bar/square decimeter; The service rating of described microwave dryer is 1-18KW.
3. preparation method according to claim 1, is characterized in that: step 1) the travelling belt travelling speed of described microwave dryer is 2-10mm/s, the travelling belt width is 40-120cm.
4. preparation method according to claim 1, is characterized in that: step 1) water content of barley worm larva polypide after described drying and dehydrating is 3-9%, surface color is without crossing thermogenetic coke black.
5. preparation method according to claim 1, is characterized in that: step 2) density of putting of described barley worm larva is 10-30 bar/square decimeter; The service rating of described microwave dryer is 1-10KW.
6. preparation method according to claim 1, is characterized in that: step 2) the travelling belt travelling speed of described microwave dryer is 5-15mm/s, the travelling belt width is 40-120cm.
7. preparation method according to claim 1, is characterized in that: step 2) described pre-warmed temperature is 50-80 ℃, the polypide temperature after described preheating is 50-80 ℃.
8. preparation method according to claim 1, is characterized in that: step 2) cavity volume of described hydraulic oil press is 2-20L, and squeeze pressure is 10-50MP, and cavity temperature is 60-90 ℃.
9. preparation method according to claim 1, is characterized in that: step 3) the filter screen particle diameter of described flame filter press is the 30-60 order; Consisting of of described sorbent material: 60-100 purpose silicon-dioxide or atlapulgite 50-80wt%; The fat-soluble silica gel 10-30wt% of 100-200 purpose; 100-200 purpose aluminum oxide 10-20wt%.
10. a barley worm larva cosmetic base oil, it is characterized in that: described barley worm larva cosmetic base oil makes by the described preparation method of claim 1-9 any one.
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| CN105456155A (en) * | 2015-11-23 | 2016-04-06 | 太仓安佑生物科技有限公司 | Method for preparing cosmetic raw materials from Hermetia illucens larvas and application of method |
| CN106833865A (en) * | 2016-12-28 | 2017-06-13 | 武汉工程大学 | A kind of method of non-solvent formula high efficiency extraction energy insect oils |
| CN107858201A (en) * | 2017-11-28 | 2018-03-30 | 湖北聚注通用技术研究有限公司 | A kind of mantis oil and its application in pet skin care products |
| CN108283670A (en) * | 2018-04-13 | 2018-07-17 | 张爱丽 | A kind of pharmaceutical composition and preparation method thereof for treating burn and scald |
| CN112691053A (en) * | 2021-01-22 | 2021-04-23 | 广东绿金生物科技有限公司 | Formula for repairing and removing scars of burned and scalded skin and preparation method |
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| CN107858201A (en) * | 2017-11-28 | 2018-03-30 | 湖北聚注通用技术研究有限公司 | A kind of mantis oil and its application in pet skin care products |
| CN108283670A (en) * | 2018-04-13 | 2018-07-17 | 张爱丽 | A kind of pharmaceutical composition and preparation method thereof for treating burn and scald |
| CN112691053A (en) * | 2021-01-22 | 2021-04-23 | 广东绿金生物科技有限公司 | Formula for repairing and removing scars of burned and scalded skin and preparation method |
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